Breakdown of oil films and formation of residual films

The breakdown processes of oil films under quasi-static loading have been investigated by using a newly developed steel-oil-mercury system. The relationship between the thickness and breakdown ratio of a hexadecane film is represented by a single master curve independently of the indentation speed, indentation load, and temperature. The master curve shows that the breakdown process of hexadecane includes two stages; one is the decrement of the thickness without breakdown and the other is the decrement of the thickness with a drastic progress of breakdown. By solving a small amount of fatty acid in hexadecane, the thickness increases and the breakdown ratio decreases noticeably; a multilayer residual film supporting normal load is formed between two metal surfaces. Experiments at different temperatures reveal a negative relationship between the temperature and thickness of residual film, which indicates that the residual film is organized by physical interaction rather than chemical interaction. At least under a lower concentration, the residual film appears to consist of not only fatty acid molecules but also hexadecane molecules.     

Oxyphilic cell variant of endometrioid adenocarcinoma

A case of oxyphilic cell variant of endometrioid adenocarcinoma is presented. To the best of our knowledge, there have been only three such cases reported in the English literature. The patient was a 35-year-old Japanese female (gravida 0, para 0). She was slightly obese with profuse vaginal bleeding. Histological examination of the resected uterus revealed endometrioid adenocarcinoma with an exclusive oxyphilic cell component. There was no evidence of myometrial invasion nor lymph node metastases. Reported cases of oxyphilic cell variant of endometrioid adenocarcinoma, including the present case, were stages 0-1 and grades 1-2. Although further study is necessary to evaluate this variant, oxyphilic cell variant seems to be an early stage of adenocarcinoma and should be differentiated from eosinophilic metaplasia and other types of adenocarcinoma of the endometrium.     

Pressureless low temperature sintering of nanocrystalline zirconia ceramics via dry powder processing

Pressureless sintering approaches provide a simple avenue to manufacture dense ceramic parts with minimal processing equipment, but current pressureless sintering techniques have yet to demonstrate capabilities of producing dense ceramics while maintaining sub-50 nm grain sizes. Nanocrystalline yttria stablized zirconia ceramics were process from 4 mol% yttria stablized zirconia (4YSZ) nanopowders with a crystallite size of 7.5 nm using dry cold isostatic pressing (CIP) where powders are dried immediately prior to green compact formation and CIP vacuum bagging. It is shown that CIP pressures >75 000 psi (517 MPa) effectively remove pores larger than 100 nm and that pressureless sintering occurs at reduced temperatures for green densities ≥50%. Though the sintering kinetics are shown to be similar to other zirconia nanopowder sintering studies, the small initial crystallize size and reduced sintering temperature allowed densities as high as 97.2%, while retaining a ceramic grain size at or below 40 nm. Produced nanocrystalline 4YSZ ceramics with a grain size of 30.3 nm and a density of 96.3% had Vicker's hardnesses as high as 14.2 GPa and Vicker's indentation fracture resistance of 3.43 MPa·, demonstrating that simple processing approaches can be refined to fabricate nanocrystalline ceramics while maintaining high hardness and indentation fracture resistance.     

A model for the complex permittivity of water at frequencies below 1 THz

Experimental permittivity data of liquid water, compiled from the open literature, were selectively applied to support a modeling strategy. Frequencies up to 1 THz and atmospheric temperatures are covered with an expression made up by two relaxation (Debye) terms. The double-Debye model reduces to one term when the high frequency limit is set at 100 GHz, and the model can be extended to 30 THz by adding two resonance (Lorentzian) terms. The scheme was carried out by employing nonlinear least-squares fitting routines to data we considered reliable.     

Compact and unified hardware architecture for SHA-1 and SHA-256 of trusted mobile computing

This paper presents a compact and unified hardware architecture implementing SHA-1 and SHA-256 algorithms that is suitable for the mobile trusted module (MTM), which should satisfy small area and low-power condition. The built-in hardware hash engine in a MTM is one of the most important circuit blocks and dominates the performance of the whole platform because it is used as a key primitive to support most MTM commands concerning to the platform integrity and the command authentication. Unlike the general trusted platform module (TPM) for PCs, the MTM, that is to be employed in mobile devices, has very stringent limitations with respect to available power, circuit area, and so on. Therefore, MTM needs the spatially optimized architecture and design method for the construction of a compact SHA hardware. The proposed hardware for unified SHA-1 and SHA-256 component can compute a sequence of 512-bit data blocks and has been implemented into 12,400 gates of 0.25 μm CMOS process. Furthermore, in the processing speed and power consumption, it shows the better performance in comparison with commercial TPM chips and software-only implementation. The highest operation frequency and throughput of the proposed architecture are 137 MHz and 197.6 Mbps, respectively, which satisfy the processing requirement for the mobile application.     

Substrate effect on the temperature coefficient of resistance of La0.7Ca0.3MnO3 thin films prepared by metal organic deposition

Epitaxial La_0.7Ca_0.3MnO₃ (LCMO) thin films were successfully prepared by the metal-organic deposition process on various (001) single-crystal substrates: MgO, LaAlO₃ (LAO), SrTiO₃ (STO), and (LaAlO₃)_0.3-(SrAlTaO₆)_0.7 (LSAT). The crystallinity and the epitaxial growth of the LCMO films were characterized by X-ray diffraction (θ − 2θ scans and pole-figure analysis). The temperature dependence of the resistance of the LCMO/LSAT, LCMO/STO and LCMO/LAO films exhibit typical characteristics with a transition from the paramagnetic-insulator state to the ferromagnetic-metallic state at a temperature peak (T _p ) ranging from 258 to 270 K. However, the LCMO/MgO films exhibited a semiconducting behavior without any transition. Based on the R(T) measurement, we calculated the temperature coefficient of resistance (TCR) for a bolometric application and we obtained 22%/K, 10.2%/K and 27.5%/K for the film grown on the LSAT, STO and LAO substrates, respectively. This difference in the TCR properties is related to the strain induced by the lattice mismatch between LCMO and the different substrates.     

The Effect of Curcuma phaeocaulis Valeton (Zingiberaceae) Extract on Prion Propagation in Cell-Based and Animal Models

Prion diseases are neurodegenerative disorders in humans and animals for which no therapies are currently available. Here, we report that Curcuma phaeocaulis Valeton (Zingiberaceae) (CpV) extract was partly effective in decreasing prion aggregation and propagation in both in vitro and in vivo models. CpV extract inhibited self-aggregation of recombinant prion protein (PrP) in a test tube assay and decreased the accumulation of scrapie PrP (PrP^Sc) in ScN2a cells, a cultured neuroblastoma cell line with chronic prion infection, in a concentration-dependent manner. CpV extract also modified the course of the disease in mice inoculated with mouse-adapted scrapie prions, completely preventing the onset of prion disease in three of eight mice. Biochemical and neuropathological analyses revealed a statistically significant reduction in PrP^Sc accumulation, spongiosis, astrogliosis, and microglia activation in the brains of mice that avoided disease onset. Furthermore, PrP^Sc accumulation in the spleen of mice was also reduced. CpV extract precluded prion infection in cultured cells as demonstrated by the modified standard scrapie cell assay. This study suggests that CpV extract could contribute to investigating the modulation of prion propagation.     

Analysis of license inconsistency in large collections of open source projects

Free and open source software (FOSS) plays an important role in source code reuse practice. They usually come with one or more software licenses written in the header part of source files, stating the requirements and conditions which should be followed when been reused. Removing or modifying the license statement by re-distributors will result in the inconsistency of license with its ancestor, and may potentially cause license infringement. In this paper, we describe and categorize different types of license inconsistencies and propose a method to detect them. Then we applied this method to Debian 7.5 and a collection of 10,514 Java projects on GitHub and present the license inconsistency cases found in these systems. With a manual analysis, we summarized various reasons behind these license inconsistency cases, some of which imply potential license infringement and require attention from the developers. This analysis also exposes the difficulty to discover license infringements, highlighting the usefulness of finding and maintaining source code provenance.     

Studies on relationship between activity and electron density on carbonyl oxygen in sex pheromone mimics of the American cockroach,part XI

From the relationship between structures of the 2-substituents of verbanyl analogs and their sex pheromone activities to the American cockroach, electron density of the carbonyl oxygen atom in the substituent, as estimated by the [¹⁷O]NMR chemical shift, was estimated to be an important factor which influenced the activity, in addition to length of the substituent and the position of the carbonyl group. (+)-Verbanyl methylcarbonate (XX), possessing the highest electron density on the carbonyl oxygen atom, showed the strongest activity among the analogs.For Part X, see Manabe et al., 1983. J. Chem. Ecol. 9:533–549.     

High temperature coefficients of resistance of VO2 films grown by excimer-laser-assisted metal organic deposition process for bolometer application

With bolometer application in mind, we prepared VO₂ films on TiO₂ (001) substrates by an excimer-laser-assisted metal organic deposition process at 300 °C or less. A metal-to-insulator transition of VO₂ is expected to induce high temperature coefficient of electrical resistance (TCR) useful for high-performance infrared sensors, but the practical use of crystalline VO₂ films has been prevented due to the accompanied wide hysteresis. In this study, by forming the epitaxial phase only near the substrate interface, the transition of the film was successfully broadened and the hysteresis disappeared. The maximum TCR of the film was more than -10%/°C near room temperature, and the temperature range in which TCR was higher than -4%/°C was very wide (280-320 K).