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排序方式: 共有294条查询结果,搜索用时 171 毫秒
1.
Khalil Faghihi 《应用聚合物科学杂志》2006,102(5):5062-5071
Six new flame‐retardant poly(amide‐imide)s (PAIs) 9a–f with high inherent viscosities containing phosphine oxide and hydantoin moieties in main chain were synthesized from the polycondensation reaction of N,N′‐(3,3′‐diphenylphenylphosphine oxide) bistrimellitimide diacid chloride 7 with six hydantoin derivatives 8a–f by two different methods such as solution and microwave assisted polycondensation. Results showed that the microwave assisted polycondensation, by using a domestic microwave oven, proceeded rapidly, compared with solution polycondensation, and was completed in about 7–9 min. All of the obtained polymers were fully characterized by means of elemental analysis, viscosity measurements, solubility test, and FTIR spectroscopy. Thermal properties and flame retardant behavior of the PAIs 9a–f were investigated using thermal gravimetric analysis (TGA and DTG) and limited Oxygen index (LOI). Data obtained by thermal analysis (TGA and DTG) revealed that these polymers showed good thermal stability. Furthermore, high char yields in TGA and good LOI values indicated that these polymers are capable of exhibiting good flame retardant properties. These polymers can be potentially utilized in flame retardant thermoplastic materials. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 5062–5071, 2006 相似文献
2.
Trimellitic anhydride was reacted with 4,4′‐diaminodiphenyl ether in a mixture of acetic acid and pyridine (3 : 2) at room temperature and was refluxed at 90–100°C, and N,N′‐(4,4′‐diphenylether) bistrimellitimide (3) was obtained in a quantitative yield. 3 was converted into N,N′‐(4,4′‐diphenylether) bistrimellitimide diacid chloride (4) by a reaction with thionyl chloride. Then, six new poly(amide imide)s were synthesized under microwave irradiation with a domestic microwave oven through the polycondensation reactions of 4 with six different derivatives of 5,5‐disubstituted hydantoin in the presence of a small amount of a polar organic medium such as o‐cresol. The polycondensation proceeded rapidly and was completed within 7–10 min, producing a series of new poly(amide imide)s in high yields with inherent viscosities of 0.27–0.66 dL/g. The resulting poly(amide imide)s were characterized by elemental analysis, viscosity measurements, differential scanning calorimetry, thermogravimetric analysis, derivative thermogravimetry, solubility testing, and Fourier transform infrared spectroscopy. All the polymers were soluble at room temperature in polar solvents such as N,N‐dimethylacetamide, N,N‐dimethylformamide, dimethyl sulfoxide, tetrahydrofuran, and N‐methyl‐2‐pyrrolidone. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 92: 3447–3453, 2004 相似文献
3.
Sarband Ebrahim Mokallaf Araghinejad Shahab Attari Jalal 《Water Resources Management》2020,34(2):447-462
Water Resources Management - In water resource management, assessing water resource allocation scenarios (WRASs) is an important multi-attribute decision making (MADM) problem. It involves... 相似文献
4.
Tsung-Liang Wu Chaw-Wu Tseng Chen-Chi Lin Shahab Hatam-Tabrizi I. Y. Shen 《Microsystem Technologies》2010,16(1-2):9-17
This paper is to study how stray magnetic forces encountered in a long seeking process affect position errors of a hard disk drive after it finishes the seek and settles. The study consists of three parts: analysis of stray magnetic forces, numerical modeling, and analysis of numerical results. In the analysis of stray magnetic forces, we lump the stray magnetic forces into three components D1, D2 and D4. Specifically, D1 is a pair of stray magnetic forces in the plane of the voice coil. The two forces act on the two equal legs of the voice coil. In addition, the two forces point to and away from the pivot center, respectively. D2 is a pair of stray magnetic forces out of the plane of the voice coil. The two forces are equal in magnitudes but opposite in directions. The two force components also act on the two equal legs of the voice coil. D4 is identical to D2, except that the two force components in D4 act in the same direction. In the numerical study, we adopt a numerical model that includes a spinning spindle motor, a spinning disk pack with multiple disks, a stationary base plate with a top cover, and a slewing head-stack assembly. Moreover, multiple bearings are present in the model to connect the multiple components. In particular, fluid-dynamic bearings connect the rotating spindle and disk pack with the base plate, pivot bearings connect the base plate with the head-stack assembly, and air bearings connect the spinning disk pack with head sliders located at the tip of the slewing head-stack assembly. Also, the numerical model assumes that the head-stack assembly seeks according to a user-specified seeking profile. Numerical simulations show two major conclusions. First, stray magnetic force component D1 does not lead to significant position errors when the head-stack assembly settles. Stray magnetic force components D2 and D4, however, can affect the position errors by significantly exciting torsion and bending modes of the head-stack assembly. Second, a flex cable can significantly increase position errors below 1 kHz during settling. 相似文献
5.
6.
Tumuluru Jaya Shankar Shahab Sokhansanj Sukumar Bandyopadhyay A. S. Bawa 《Food and Bioprocess Technology》2010,3(4):498-510
In the present study, response surface method (RSM) and genetic algorithm (GA) were used to study the effects of process variables like screw speed, rpm (x 1), L/D ratio (x 2), barrel temperature (°C; x 3), and feed mix moisture content (%; x 4), on flow rate of biomass during single-screw extrusion cooking. A second-order regression equation was developed for flow rate in terms of the process variables. The significance of the process variables based on Pareto chart indicated that screw speed and feed mix moisture content had the most influence followed by L/D ratio and barrel temperature on the flow rate. RSM analysis indicated that a screw speed?>?80 rpm, L/D ratio?>?12, barrel temperature?>?80 °C, and feed mix moisture content?>?20% resulted in maximum flow rate. Increase in screw speed and L/D ratio increased the drag flow and also the path of traverse of the feed mix inside the extruder resulting in more shear. The presence of lipids of about 35% in the biomass feed mix might have induced a lubrication effect and has significantly influenced the flow rate. The second-order regression equations were further used as the objective function for optimization using genetic algorithm. A population of 100 and iterations of 100 have successfully led to convergence the optimum. The maximum and minimum flow rates obtained using GA were 13.19?×?10?7 m3/s (x 1?=?139.08 rpm, x 2?=?15.90, x 3?=?99.56 °C, and x 4?=?59.72%) and 0.53?×?10?7 m3/s (x 1?=?59.65 rpm, x 2?=?11.93, x 3?=?68.98 °C, and x 4?=?20.04%). 相似文献
7.
Theoretical calculation simulation studies of ABV nuclear reactor coupled with desalination system
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Salah Ud‐Din Khan Syed Noman Danish Sajjad Haider Shahab Ud‐Din Khan 《国际能源研究杂志》2015,39(11):1554-1563
In this paper, research has been conducted on the floating type nuclear power plant named as ABV reactor which is designed for district heating, power, and sea water desalination by OKBM facility at Russia. This reactor was tested under different thermal loads during the designing phase, and three modules have been investigated. Theoretical calculations and simulation studies have been performed on these three modules having specifications as ABV‐6M with 47MWth, ABV‐6 with 38MWth, and ABV‐3 with 18MWth.The results obtained from these modules have been calculated mathematically and verified by simulation. We have compared the originally derived data of ABV desalination system with our theoretical and simulation analysis. The results from two desalination techniques including RO and RO + MED have been calculated and are presented in this paper with details. The results obtained from both analysis show that the efficiency of ABV nuclear reactor desalination system increases with the decrease in corresponding water cost ratio. Copyright © 2015 John Wiley & Sons, Ltd. 相似文献
8.
In this paper, a novel system has been developed for plasma disruption conditions followed by downward vertical displacement. During the disruption, size and orientation of plasma decreases, which gives the halo current circulated around each contacting point in radial as well as in poloidal directions. Therefore, a new mathematical model has been developed, which gives the interaction forces of halo current, vertical, and radial plasma dynamical behavior (linear and nonlinear). This theoretical approach showed that the tokamak plasma has two connecting points in order to distinguish between the stable and unstable position. This model can particularly give the magnetic field change points and changing of flux, which are more convenient in order to discuss the static and tilting position of plasma behavior. Numerical techniques have been calculated in terms of plasma dynamical behavior, that is, Electromagnetic/plasma, Vertical Displacement Event (VDE) stages, and initial interaction between the forces under specific time interval. The objective of the research is to developed theoretical and computational model in order to investigate the dynamical behavior of plasma under disruption conditions. This is the novel method, and no work has been reported so far. Copyright © 2015 John Wiley & Sons, Ltd. 相似文献
9.
Fereydoon Aflaki Vanik Ghoulipour Nader Saemian Shahab Sheibani 《Food Analytical Methods》2014,7(3):713-720
A rapid, sensitive, and reproducible high-performance liquid chromatographic procedure for the determination of nine biogenic amines in non-alcoholic beers was developed by an optimized benzoylation procedure. A Plackett–Burman factorial design was used in order to screen the statistically significant variables. The significant factors of biogenic amine benzoylation, reagent volume and pH, were optimized by a complete factorial response surface design, and optimal reaction conditions were generated. The optimized method showed good linearity (correlation coefficients > 0.997) and good recoveries (from 88.6 to 104.7 %). The repeatability and reproducibility of method were >3.9 and >4.6 %, respectively. Moreover, the detection limits of biogenic amines were calculated between 0.05 and 0.15 μg/ml in wine samples. The optimized method has been applied to the determination of biogenic amine contents of non-alcoholic beers consumed in Iran. Their values ranged from 0 to 2.56 mg/l, no significant differences (p?>?0.05) were observed between the analyzed samples, and none of these samples surpass the toxic levels reported in the literature. 相似文献
10.