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排序方式: 共有970条查询结果,搜索用时 15 毫秒
1.
Kumari Asha Neeraj Kumar Biswas Sakshi Saxena Vibha Rani Satsangi Rohit Shrivastav Rama Kant Sahab Dass 《International Journal of Hydrogen Energy》2021,46(40):20858-20870
The present study attempts quantitative determination of changes in the morphological surface features viz. fractal dimension, lower and upper cut off length scale through Power Spectral Density analysis prior to and after irradiation of 100 KeV Ar+ ion beam at incidence angles of 0°, 40° and 60° on ZnO thin films. All the unirradiated and irradiated samples are subjected to photoelectrochemical characterization and a correlation between photoelectrochemical performance and morphological parameters is established. Sample irradiated at 40° angle at the fluence of 5 × 1016 ions/cm2 is found to possess maximum fractal dimension of 2.72, lower and upper cut off length scale of 3.16 nm and 63.00 nm respectively. This sample exhibits maximum photocurrent density of 3.19 mA/cm2 and applied bias photon-to-current efficiency of 1.12% at 1.23 V/RHE. Hydrogen gas collected for duration of 1 h for the same sample was ~4.83 mLcm?2. 相似文献
2.
Mani Balamurugan Hui‐Yun Jeong Venkata Surya Kumar Choutipalli Jung Sug Hong Hongmin Seo Natarajan Saravanan Jun Ho Jang Kang‐Gyu Lee Yoon Ho Lee Sang Won Im Venkatesan Subramanian Sun Hee Kim Ki Tae Nam 《Small (Weinheim an der Bergstrasse, Germany)》2020,16(25)
The electrochemical reduction of carbon dioxide (CO2) to hydrocarbons is a challenging task because of the issues in controlling the efficiency and selectivity of the products. Among the various transition metals, copper has attracted attention as it yields more reduced and C2 products even while using mononuclear copper center as catalysts. In addition, it is found that reversible formation of copper nanoparticle acts as the real catalytically active site for the conversion of CO2 to reduced products. Here, it is demonstrated that the dinuclear molecular copper complex immobilized over graphitized mesoporous carbon can act as catalysts for the conversion of CO2 to hydrocarbons (methane and ethylene) up to 60%. Interestingly, high selectivity toward C2 product (40% faradaic efficiency) is achieved by a molecular complex based hybrid material from CO2 in 0.1 m KCl. In addition, the role of local pH, porous structure, and carbon support in limiting the mass transport to achieve the highly reduced products is demonstrated. Although the spectroscopic analysis of the catalysts exhibits molecular nature of the complex after 2 h bulk electrolysis, morphological study reveals that the newly generated copper cluster is the real active site during the catalytic reactions. 相似文献
3.
4.
Effect of boron on the low-cycle fatigue behavior and deformation structure of INCONEL 718 at 650 °C
L. Xiao M. C. Chaturvedi D. L. Chen 《Metallurgical and Materials Transactions A》2004,35(11):3477-3487
Symmetrical push-pull low-cycle fatigue (LCF) tests were performed on INCONEL 718 (IN718) containing 12, 29, 60, and 100 ppm
B at 650 °C. The results showed that all the alloys experienced a relatively short period of initial cyclic hardening at low
strain amplitudes, followed by a regime of saturation or slightly continuous cyclic softening. The initial cyclic hardening
phase decreased with increasing strain amplitudes, and disappeared at the high strain amplitudes. A serrated flow was observed
in the plastic regions of cyclic stress-strain hysteresis loops. The saturated cyclic stress amplitude at a given strain amplitude
was highest for the alloy with 60 ppm B, and lowest for the alloy with 12 ppm B. The LCF lifetime increased with increasing
B concentration up to 60 ppm, and then decreased as the B content increased from 60 to 100 ppm. Fractographic analysis suggested
that the fracture mode changed from intergranular to transgranular cracking as the B concentration increased. The characteristic
deformation microstructures produced by LCF tests at 650 °C, examined via transmission electron microscopy, were regularly spaced arrays of planar deformation bands on {111} slip planes in all four
alloys. A ladderlike structure was observed in some local regions in the alloy with 12 ppm B. Heavily deformed planar deformation
bands were observed in the fatigued specimens with 100 ppm B. The mechanism of improvement in the LCF life of IN718 due to
B addition is discussed. 相似文献
5.
6.
Shubneesh Batra Nanseng Jeng Akif Sultan Kyle Picone Surya Bhattacharya Keun-Hyung Park Sanjay Banerjee David Kao Monte Manning Chuck Dennison 《Journal of Electronic Materials》1993,22(5):551-554
When dopants are indiffused from a heavily implanted polycrystalline silicon film deposited on a silicon substrate, high thermal
budget annealing can cause the interfacial “native” oxide at the polycrystalline silicon-single crystal silicon interface
to break up into oxide clusters, causing epitaxial realignment of the polycrystalline silicon layer with respect to the silicon
substrate. Anomalous transient enhanced diffusion occurs during epitaxial realignment and this has adverse effects on the
leakage characteristics of the shallow junctions formed in the silicon substrate using this technique. The degradation in
the leakage current is mainly due to increased generation-recombination in the depletion region because of defect injection
from the interface. 相似文献
7.
8.
Hou V.T. Kant K. Ramaswami V. Wang J.L. 《Selected Areas in Communications, IEEE Journal on》1994,12(3):456-467
Motivated by field data which showed a large number of link changeovers and incidences of link oscillations between in-service and out-of-service states in common channel signalling (CCS) networks, a number of analyses of the link error monitoring procedures in the SS7 protocol were performed by the authors. This paper summarizes the results obtained thus far and include the following: (a) results of an exact analysis of the performance of the error monitoring procedures under both random and bursty errors; (b) a demonstration that there exists a range of error rates within which the error monitoring procedures of SS7 may induce frequent changeovers and changebacks; (c) an analysis of the performance of the SS7 level-2 transmission protocol to determine the tolerable error rates within which the delay requirements can be met; (d) a demonstration that the tolerable error rate depends strongly on various link and traffic characteristics, thereby implying that a single set of error monitor parameters will not work well in all situations; and (e) some recommendations on a customizable/adaptable scheme of error monitoring with a discussion on their implementability. These issues may be particularly relevant in the presence of anticipated increases in SS7 traffic due to widespread deployment of advanced intelligent network (AIN) and personal communications service (PCS) as well as for developing procedures for high-speed SS7 links currently under consideration by standards bodies 相似文献
9.
10.
Planning collision-free trajectories in time-varying environments: a two-level hierarchy 总被引:1,自引:0,他引:1
We propose a two-level hierarchy for planning collision-free trajectories in time varying environments. Global geometric algorithms for trajectory planning are used in conjunction with a local avoidance strategy. Simulations have been developed for a mobile robot in the plane among stationary and moving obstacles. Essentially, the robot has a global geometric planner that provides a coarse global trajectory (the path and velocity along it), which may be locally modified by the low-level local avoidance module if local sensors detect any obstacles in the vicinity of the robot. This hierarchy makes effective use of the complementary aspects of the global trajectory planning approaches and the local obstacle avoidance approaches. 相似文献