A new method for manufacturing nanostructured electrodes on glass substrates

The present paper describes a new method for manufacturing a nanostructured porous layer of TiO₂ on a conducting glass substrate for use in a dye-sensitized photoelectrochemical cell. The method involves deposition of a layer of semiconductor particles onto a conducting substrate and compression of the particle layer to form a mechanically stable, electrically conducting, and porous nanostructured film at room temperature. Photoelectrochemical characteristics and morphology of the resulting nanostructured films are presented. The potential use of the new manufacturing method in the future applications of nanostructured systems is discussed.     

Synthesis and thermal stability of ball-milled and melt-quenched amorphous and nanostructured Al-Ni-Nd-Co alloys

In this work the Al₈₅Ni₉Nd₄Co₂ alloy was used as a starting point for examining the possibility of forming bulk glassy Al-based materials by combining rapid quenching and ball milling techniques. Fine glassy powders were obtained by ball milling melt-spun amorphous ribbons using a severe cryogenic processing regime. The thermal stability data of the powders as obtained by constant-rate heating and isothermal DSC experiments together with viscosity measurements are discussed with respect to feasible consolidation conditions. The powder compaction was done by two methods (uni-axial hot pressing and extrusion) at 513 K for up to 15 min. Only the uni-axial hot pressing led to bulk Al₈₅Ni₉Nd₄Co₂ samples with similar glassy structure and Vickers microhardness values comparable to those of the initial melt-spun ribbons.     

School psychologists' acceptability of behavioral and traditional assessment procedures for externalizing problem behaviors.

A national survey of school psychologists' acceptability of psychological assessment techniques in the area of externalizing problem behaviors was examined. School psychologists' ratings of 2 procedures, Behavioral Assessment (BA) and Traditional Assessment (TA), were compared using an analog case study methodology. Using a random sample of 500 National Association of School Psychologists members from the 1991–1992 membership directory, 339 Ss completed the Assessment Rating Profile after reading a hypothetical case summary describing a student with suspected externalizing problem behaviors. Results indicated statistically significant differences between assessment methods and ratings of acceptability. BA procedures were found to be more acceptable than TA procedures. Implications related to the acceptability of psychological assessment techniques, as well as implications for school psychology practitioners are discussed. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Rotating magnetic field-driven flows in conductive inhomogeneous media: Part I—Numerical study

This paper presents a numerical study of the Lorentz force and fluid flow induced by a rotating magnetic field in a medium with a nonhomogeneous electric conductivity placed in a cylindrical vessel with insulated walls. The nonhomogeneity is modeled by the presence of a solid and a liquid phase of different electrical conductivity. The solid phase is located orthogonally to the axis of rotation, which corresponds to the case of unidirectional solidification. The simulations were performed for different locations of the solid front and different ratios of the electrical conductivity, σ _s /σ _l =0.2... 10. Here σ _s and σ _l are the electric conductivity of the solid and liquid phases, respectively. The results showed that the difference between electrical conductivity of solid and liquid phases has a noticeable effect on the mean-time Lorentz force and the velocity: namely, the presence of the solid phase (σ _s >σ _l ) leads to an increase of the Lorentz force and fluid flow in the cylinder.     

Crystallographic electron microscopy

We present a family of techniques for the transmission electron microscope that generate surface zone-axis patterns. These patterns display the variation of the diffracted-beam intensity as a function of the angle of the incident electrons. The conditions of the experiments are those of reflection high-energy electron diffraction at near grazing incidence. The techniques are: surface convergent-beam diffraction, a surface analogue of the Tanaka method and a modified double-rocking scheme. Experimental results are presented for diffraction from surfaces of MgO and MoS₂. We anticipate that surface zone-axis patterns (surface ZAPs) will become established as an important tool for surface characterization, especially when used in conjunction with high-resolution surface imaging and surface energy loss spectroscopy; surface ZAPs may be expected to play, in surface analysis, a role analogous to that played by convergent-beam diffraction in normal transmission electron microscopy.     

Putting it all together – Formal verification of the VAMP

In the verified architecture microprocessor (VAMP) project we have designed, functionally verified, and synthesized a processor with full DLX instruction set, delayed branch, Tomasulo scheduler, maskable nested precise interrupts, pipelined fully IEEE compatible dual precision floating point unit with variable latency, and separate instruction and data caches. The verification has been carried out in the theorem proving system PVS. The processor has been implemented on a Xilinx FPGA. A shorter version of this article with the title “Instantiating uninterpreted functional units and memory system: functional verification of the VAMP” appeared in [8]. The work reported here was done while all the authors were with Saarland University.     

Al-Cu-Fe QUASICRYSTALLINE PHASE FORMATION BY MECHANICAL ALLOYING

Al-Cu-Fe alloys were prepared from elemental powders in a high-energy planetary ball mill. A sequence of solid state reactions resulting in quasicrystal (QC) phase formation takes place during heating of the as-milled powder. These reactions were studied by both differential scanning calorimetry and x-ray diffraction methods. Mechanically alloyed powders were consolidated by cold and hot pressing, as well as by explosive compaction. After annealing at sufficiently high temperatures, the consolidated samples are single-phase QC, except the ones consolidated by explosion. The high reactivity of the as-milled alloys causes the appearance of high porosity of the consolidated samples after the annealing.     

Langzeitiges Kriechrißverhalten kennzeichnender Kraftwerksstähle

Long Term Creep Crack Behaviour of Typical Power Plant Steels The creep crack behaviour of the steels was investigated in a wide loading range up to a test duration of 40 000 h and down to a creep crack growth rate of 2 · 10^?5 mm/h with specimens of different shape and size. For steels of type l%Cr-l%Mo-0.6%Ni-0.3%V, 1%Cr-0.9%Mo-0.7%Ni-03.%V, 12%Cr-1%Mo-0.3%V-0.22%C and 12%Cr-l%Mo-0.3%V-0.20%C tested at 550°C, the creep crack growth rate could be described by the parameter C₂* with significantly smaller scatter bands than by the parameter C₁* or the stress intensity factor K_I. For steel 12%Cr-2%Ni-1%Mo tested at 450°C, parameter K_I leads to the smallest scatter band. The creep crack initiation can be described in a two-criteria diagram based on nominal stress and stress intensity factor. However the method is assumed to be over-conservative in case of increasing specimen size. As a result of several aperiodic creep fatigue crack tests, precracking under fatigue conditions gave a weak increase of the creep crack growth rate whereas by precracking under creep conditions the fatigue crack rate was strongly decreased.     

Test of the deterministic conjecture for the instantaneous time phase fluctuations of an oscillator

The fluctuations observed by recording the picosecond pulses of a mode-locked laser with a synchroscan streak camera are due to the laser jitter and to the variations of the zero crossing of the synchronization. By means of a simple model, it is shown that the dispersions measured when the synchronization is generated from the mode-locker oscillator reflect the instantaneous time phase fluctuations of this oscillator. From the study of the experimental recordings with methods of time series analysis it results that the phase noise of the electronic oscillator is consistent with an underlying low-dimensional strange attractor.