Simple chemical syntheses of TAG monohydroperoxides

For the purpose of synthesizing standards to be used in the quantification of TAG hydroperoxides, three TAG (1,2-dioleoyl-3-palmitoylglycerol, 1-oleoyl-2-linoleoyl-3-palmitoylglycerol, and triolein) monohydroperoxides were chemically synthesized as authentic specimens. TAG were prepared by using a simple condensation in pyridine of glycerol and the corresponding acid chlorides. These TAG were then converted into monohydroperoxides by a photosensitized peroxidation. The synthesized monohydroperoxides were analyzed by normal-phase and RP-HPLC. The results of normal-phase HPLC analysis showed that monohydroperoxides from a corresponding TAG were a mixture of regioisomers. In RP-HPLC, however, the regioisomers of monohydroperoxides were not separated and gave a single peak, which may improve the sensitivity for the detection of TAG monohydroperoxides. In this study TAG monohydroperoxide standards were synthesized; these will be useful for the study of yet unknown biological and pathological roles of TAG hydroperoxides.     

定子无磁轭模块化轴向磁通永磁电机研究进展综述

定子无磁轭模块化(yokeless and segmented armature,YASA)轴向磁通永磁电机具有功率密度和转矩密度高、效率高、轴向结构紧凑、易于维修的优点,在电动汽车、风力发电等领域有广阔的应用前景,已有大量文献对YASA电机进行分析研究。该文基于国内外对YASA电机已开展的研究工作,介绍该类电机的典型拓扑结构,并从电机电磁特性计算方法与性能优化、损耗分析与抑制技术、温升与散热研究、齿槽转矩削弱技术、结构强度校核与制造偏差分析,以及定子铁心材料选取等方面进行综述,并对该类电机当前的应用情况进行整理。最后,基于YASA电机的研究现状,对未来研究的发展趋势进行展望。     

Clinical application of single-shot echo-planar diffusion-weighted imaging with compressed SENSE in prostate MRI at 3T: preliminary experience

Magnetic Resonance Materials in Physics, Biology and Medicine - Image quality (IQ) of diffusion-weighted imaging (DWI) with single-shot echo-planar imaging (ssEPI) suffers from low signal-to-noise...     

一种改进型surendra背景更新算法的FPGA实现

针对现有的动态背景提取运动目标物体算法复杂且难以在硬件上实现的问题,研究了改进型surendra背景更新算法原理的特点,提出了改进型surendra背景更新算法的硬件结构,并对硬件结构进行综合、仿真后,在FPGA芯片上实现.     

基于Pocket PC的分布式程序设计

本文介绍了实现Pocket PC与PC之间的分布式程序设计的原理．并用实例详细介绍了进行分布式程序设计的主要方法。     

Wide Color Variation in SiNO Thin Films Dispersed with Precipitated TiN Nano Particles

Amorphous thin films of Ti_1?ySi_y(N,O) with y ≥ 0.38 were prepared by reactive sputter deposition in a nitrogen atmosphere. Thermal annealing of the films in an ammonia flow above 800°C yielded Si(N,O) amorphous thin films dispersed with precipitated TiN nanosized particles. The film color changed with Si content y and the annealing conditions, from carrot orange to cream yellow in the as‐deposited films due to their oxynitride nature, and from dark green to canary yellow and from iron blue to horizon blue at respective annealing temperatures of 800°C and 900°C due to metallic nature of the TiN nanosized particles precipitated in the annealing.     

16.9－28 10PR R7农业轮胎的设计

介绍16.9-28 10PR R7农业轮胎的设计。结构设计:外直径1 427 mm,断面宽408 mm,行驶面宽度386 mm,行驶面弧度高32 mm,胎圈着合直径716 mm,胎圈着合宽度381 mm,断面水平轴位置(H_1/H_2)0.665,花纹深度39 mm,花纹饱和度25.2%,花纹周节数28。施工设计:胎面采用两方四块结构,胎体采用4层高强度1400dtex/2V_1锦纶6浸胶帘布,缓冲层采用2层930dtex/2锦纶6浸胶帘布,采用LCX-4B型成型机成型、立式硫化罐硫化。成品轮胎试验结果表明,轮胎的外缘尺寸和物理性能均满足设计及国家标准要求。     

Fracture behaviour and numerical study of resistance spot welded joints in high-strength steel sheet

Cross tension tests of resistance spot welded joints with varying nugget diameter were carried out using 980 MPa high strength steel sheet of 1.6 mm thickness. In proportion, as nugget diameter increased from 3√t to 5√t (where t is thickness), cross tension strength (CTS) increased while fracture morphology simultaneously transferred from interface fracture to full plug fracture. In cases of interface fracture, circumferential crack initiation due to separation of the corona bond arose at an early stage of loading. The crack opening process without propagation was recognized until just before fracture and then the crack propagated to the nugget immediately in a brittle manner around CTS. In full plug fracture, main ductile crack initiation from the notch-like part at the end of sheet separation occurred with the sub-crack initiated at an early stage. The ductile crack propagated toward the HAZ and base material to form full plug fracture. The mode I stress intensity factor was considered as a suitable fracture parameter because the circumferential crack behaved pre-crack for brittle fracture in the nugget region at the final stage. Based on the FE analysis, the mode I stress intensity factor was calculated as 116 MPa √m at CTS as fracture toughness for the nugget. With respect to full plug fracture, ductile crack initiation behaviour from the notch-like part was expressed by concentration of equivalent plastic strain. On the assumption that the ductile crack arose in critical value of equivalent plastic strain, the value was calculated as 0.34 by FE analysis. Reasonable interpretation for interface fracture and full plug fracture in the resistance spot welded joint was proposed due to first crack initiation by stress concentration, brittle fracture by using mode I stress intensity factor, and ductile crack initiation by using equivalent plastic strain.     

Additive Sintering,Postannealing, and Dielectric Properties of SrTaO2N

The maintaining of the chemical composition and electrical insulativity of SrTaO₂N ceramics was investigated during sintering and annealing, using powders prepared by the nitridation of Sr₂Ta₂O₇. Due to the low thermal stability of SrTaO₂N, the partial loss of SrO and nitrogen induced the formation of a TaO_0.9 impurity after heat‐treating at above 1100°C. The sintering additive SrCO₃ and postannealing in NH₃ were employed to compensate for the loss of SrO and nitrogen to obtain ceramics with the original chemical composition. The as‐sintered SrTaO₂N ceramics with various relative density (RD) were annealed in NH₃ to observe the recovery of color and electrical insulativity. It was found that the inner part of the well‐sintered samples with RD = 95.1% could not be recovered by annealing, and continued to exhibit semiconducting behavior and a black color. On the other hand, for the as‐sintered SrTaO₂N ceramics with RD < 84%, both the nitrogen content and electrically insulating behavior were completely recovered after annealing. The postannealed SrTaO₂N ceramics (RD = 83.3%) possessed a relatively large dielectric constant of 450 with a low dielectric loss of less than 0.1 at 100 Hz, almost independent of frequency and temperature.