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2.
Uma Maheswar Rao S. S. M. S. Abdul Majeed C. Venkataseshaiah R. Sarathi 《Bulletin of Materials Science》2002,25(6):473-475
In the present work, tracking phenomena has been studied with silicone rubber material under the a.c. and d.c. voltages following
IEC-587 standards. The surface condition of the tracked zone was analysed using wide angle X-ray diffraction (WAXD) and thermogravimetric
differential thermal analysis (TG-DTA) studies. The tracking time was different for a.c. and d.c. voltages. 相似文献
3.
Recently an unstable trinucleotide CTG repeat, located within the 3' untranslated region of a gene on 19q13.3 was discovered in kindreds with myotonic dystrophy (DM). The age-of-onset/severity of DM shows a good correlation with CTG repeat size, and pedigrees and data reported to date have shown a striking trend toward amplification of the size of the CTG repeat during transmission from parent to child. The amplification has been accepted as the biological explanation for anticipation in the clinical severity observed in many families with DM. In this paper we report on 3 families where CTG amplification decreased during transmission from parent to child. In one case there was a gene conversion event, while in the remaining 2 there was a simpler reduction in the size of the repeat length. The changes appear to have been accompanied by a reduction in clinical severity in the child when compared to the parent. These observations are discussed in terms of their clinical implications and the biases that may exist in much of the reported data. 相似文献
4.
Girendra N. Kulsrestha Uma Shankar Jaipal S. Sharma Jasvinder Singh 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1991,50(1):57-65
Liquid-phase oxidation of cyclohexane with Co(III) catalyst and gaseous oxygen was found to be influenced by reaction temperature, catalyst concentration and the duration. Maximum adipic acid product selectivity (77%) with about 85% cyclohexane conversion was attained at 100°C using catalyst: cyclohexane molar ratio 0·08. Under these conditions more than 80% cyclohexane was converted in the first hour, although selectivity to adipic acid continued to increase for the next 5 h. Cyclohexyl acetate and cyclohexyl monoadipate were identified as important intermediates. This study supports the mechanism proposed by Schultz, J. G. D. and Opchenko, A., J. Org. Chem., 38 (21) (1973) 3729. 相似文献
5.
Amorphous inorganic ion exchangers zirconium phosphate, zirconium molybdate and zirconium phosphomolybdate have been prepared
and characterized by elemental analysis, TGA, FTIR and surface area measurements. The protonic conductivity in these materials
were determined at various temperatures and compared. It was found that the mixed material zirconium phosphomolybdate showed
maximum conductivity at all temperatures. 相似文献
6.
Long-period fibre gratings in specially designed birefringent few-mode fibres are used to demonstrate spectrally flat polarisers with bandwidths of 10 nm and polarisation extinction levels of 20 dB. This is enabled by the special dispersive properties of few-mode fibres, yielding fibre polarisers with performance approaching that of bulk-optic devices. 相似文献
7.
Lakshmi Ramachandran Nanjangud C. Narendra Karthikeyan Ponnalagu 《Service Oriented Computing and Applications》2012,6(4):283-302
Cloud-based systems promise an on-demand service provisioning system along with a ??pay-as-you-use?? policy. In the case of multi-tenant systems this would mean dynamic creation of a tenant by integrating existing cloud-based services on the fly. Presently, dynamic creation of a tenant is handled by building the required components from scratch. Although multi-tenant systems help providers save cost by allocating multiple tenants to the same instance of an application, they incur huge reconfiguration costs. Cost and time spent on these reconfiguration activities can be reduced by re-constructing tenants from existing tenant configurations supported by service providers. Multi-tenant cloud-based systems also lack the facility of allowing clients to specify their requirements. Giving clients the flexibility to specify requirements helps them avoid spending an excessive amount of time and effort looking through a list of services, many of which might not be relevant to them. Moreover, dynamic provisioning in the cloud requires an integrated solution across the technology stack (software, platform and infrastructure) combining functional, non-functional and resource allocation requirements. Existing research works in the area of web service matching, although numerous, still fall short, since they usually consider each requirement type in isolation and cannot provide an integrated solution. To that end, in this paper we investigate the features needed for dynamic service provisioning on the cloud. We propose a novel User Interface-Tenant Selector-Customizer (UTC) model and approach, which enables cloud-based services to be systematically modeled and provisioned as variants of existing service tenants in the cloud. Our approach considers functional, non-functional and resource allocation requirements, which are explicitly specified by the client via the user interface component of the model. To the best of our knowledge, ours is the first such integrated approach. We illustrate our ideas using a realistic running example, and also present a proof-of-concept prototype built using IBM??s Rational Software Architect modeling tool. We also present experimental results demonstrating the applicability of our matching algorithm. Our results show significant reduction in matching time with the help of an elimination process that reduces the search space needed for performing matching. 相似文献
8.
V. S. Ramachandran 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1972,22(11):1125-1138
The hydration characteristics of 3CaO.SiO2 or β2CaO.SiO2 are studied by an addition of 0.0, 0.1, 0.5 or 1.0% triethanolamine. The amount of Ca(OH)2 found at 1, 3, 7 or 28 days was in the order C3S + 0% TEA > C3S +0.1% TEA > C3S + 0.5% TEA > C3S+1.0% TEA, irrespective of whether lime was estimated by X-ray, DTA, TGA or chemical analysis. The rate of hydration, in terms of the disappearance of 3CaO.SiO2, showed that hydration proceeded faster in the presence of TEA after 1 day. Additions of TEA increase the induction period, promote the formation of a C-S-H with higher CaO/SiO2 ratio, increase the formation of non-crystalline Ca(OH)2 and enhance the surface area of the hydrated silicate product. 相似文献
9.
Uma Chatterjee 《Polymer》2005,46(5):1575-1582
ATRP of several methacrylates viz. methyl methacrylate (MMA), ethyl methacrylate (EMA), n-butyl methacrylate (nBMA), t-butyl methacrylate (tBMA), benzyl methacrylate (BzMA) and (N,N-dimethylamino)ethyl methacrylate (DMAEMA) has been studied in neat as well as aqueous (up to 12 vol% water) acetone at 35 °C using CuCl/bipyridine (bpy) catalyst and ethyl 2-bromoisobutyrate as the initiator. Addition of water significantly enhances the rate of polymerization without losing control. Unlike CuCl/bpy the CuBr/bpy catalyst gives poor control which is attributed to the lower solubility and consequent heterogeneity in the latter case. Of the other ligands used with the CuCl catalyst viz. o-phenanthroline (o-phen), 1,1,4,7,7-pentamethyldiethylenetriamine (PMDETA), 1,1,4,7,10,10-hexamethyltriethylenetetramine (HMTETA), Me6TREN only o-phen offers reasonably good control. The CuCl/bpy catalyst system has been used also in preparing some di- and tri-block copolymers with reasonably low polydispersity index (PDI) at ambient temperature (35 °C) using aqueous acetone as the solvent. The following block copolymers have been prepared PMMA-tBMA, PMMA-b-tBMA-b-MMA, PMMA-DMAEMA, by this method. 相似文献
10.
Fred N. Tebbe Patricia A. Morris Roger H. French Uma Chowdhry Robert L. Coble 《Journal of the American Ceramic Society》1988,71(4):204-C
Aluminum hydroxide obtained by hydrolysis of triethylaluminum is free of uranium and thorium at detection limits of 1 to 9 parts per billion (ppb). Other impurities commonly associated with aluminum oxides are present at low levels (Fe, ∼ 1 ppm; Si, 3 to 6 ppm). When the organoaluminum is intentionally contaminated with an iron salt, purity is restored by a simple distillation. 相似文献