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del del Valle M. A. Ugalde L. Díaz F. R. Bodini M. E. Bernède J. C. Chaillou A. 《Polymer Bulletin》2003,51(1):55-62
Summary The influence of electrolyte and monomer concentration on
properties and morphology of electrochemically obtained
polyselenophene films doped and undoped with hexafluorophosphate
and tetrafluoroborate anions was analyzed. The films were
deposited on SnO2-coated glass in a
classical three-electrode cell from the monomer and the
electrolyte in anhydrous acetonitrile.The electrochemical growth of polyselenophene thin films
was studied by X-ray photoelectron spectroscopy (XPS), electron
probe microanalysis (EPMA), and scanning electron microscopy
(SEM). The morphology study revealed different three-
dimensional (3D) and bidimensional (2D) growth, depending on
monomer and electrolyte concentration. 相似文献
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Unai Diaz-Orueta Aitziber Etxaniz Mari Feli Gonzalez Cristina Buiza Elena Urdaneta Javier Yanguas 《Universal Access in the Information Society》2014,13(1):89-97
The complexity of new information technologies (IT) may limit the access of elderly people to the information society, exacerbating what is known as “the digital divide,” as they appear to be too challenging for elderly citizens regardless of the integrity of their cognitive status. This study is an attempt to clarify how some cognitive functions (such as attention or verbal memory) may determine the interaction of cognitively impaired elderly people with technology. Twenty participants ranging from mild cognitive impairment to moderate Alzheimer’s disease were assessed by means of a neuropsychological and functional battery and were asked to follow simple commands from an avatar appearing on a TV by means of a remote control, such as asking the participant to confirm their presence or to respond Yes/No to a proposal to see a TV program. The number of correct answers and command repetitions required for the user to respond were registered. The results show that participants with a better cognitive and functional state in specific tests show a significantly better performance in the TV task. The derived conclusion is that neuropsychological assessment may be used as a useful complementary tool for assistive technology developers in the adaptation of IT to the elderly with different cognitive and functional profiles. Further studies with larger samples are required to determine to what extent cognitive functions can actually predict older users’ interaction with technology. 相似文献
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Global sensitivity analysis of the blade geometry variables on the wind turbine performance 下载免费PDF全文
The need for implementing efficient blade designs gains relevance as wind turbine developments require longer blades. The design of blade geometry, traditionally divided in 2D airfoils and spanwise distributions, is usually addressed as an optimization problem. A correct identification of the design variables is crucial to avoid unnecessary computational cost or insufficient exploration of the design space. This paper deals with the identification of the design variables that affect the wind turbine performance. First, the number of design variables for an accurate airfoil representation is resolved. A methodology, based on statistical hypothesis testing applied to the airfoil approximation errors, is presented to assess the accuracy of types of B‐splines. Second, the study is extended to chord and twist distributions besides airfoil geometry with the purpose of assessing the sensitive blade variables in the wind turbine performance. Global sensitivity analysis as multi‐variable linear regressions and variance‐based methods are used. Latin hypercube sampling is applied to generate efficient inputs. MATLAB‐based code is developed to obtain outputs: annual energy production, maximum blade tip deflection, overall sound power level and blade mass. As result of the study, a list of non‐affecting variables is deduced. These variables can be avoided in the optimization without loss of gain in the performance. The method is a powerful tool to analyse in a preliminary phase a design problem involving a high amount of variables and complex physical relations by means of combining different multi‐disciplinar calculation codes and performing statistical treatments. Copyright © 2017 John Wiley & Sons, Ltd. 相似文献
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Unai Iriarte‐Velasco Irene Sierra Emilio Atilano Cepeda Raquel Bravo Jose Luis Ayastuy 《Coloration Technology》2015,131(4):322-332
Bone is an inorganic template containing organic material inside which can be converted into hydroxyapatite‐rich material by pyrolysis. Nowadays, there is a growing research interest in the use of hydroxyapatite, the chemical formula of which is Ca10(PO4)6(OH)2. In the present work, pork bone, an abundant biomass source and food waste, has been converted into structured porous hydroxyapatite by a three‐step process including precharring under mild conditions, chemical activation, and thermal activation. The investigated activating agents were NaOH, KOH, K2CO3, H2SO4, and H3PO4. A thorough investigation of the influence of different activating protocols on the chemical and textural properties of the produced material was carried out by nitrogen adsorption–desorption at 77 K, potentiometric titrations, Fourier transform infrared, and X‐ray diffraction techniques. Chemical activation with NaOH, K2CO3, and H2SO4 increased the specific surface area up to 53%. H3PO4 reduced both surface area and pore volume, and KOH showed little influence on the pore structure. The produced materials were evaluated by methylene blue adsorption tests and showed significant improvement as a result of chemical activation. As a main effect, acid treatment increased methylene blue adsorption kinetics, probably owing to an increase in micropororosity, whereas alkali activation enhanced the adsorption capacity of the resultant biochar. 相似文献
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Unai De La Torre Beñat Pereda-Ayo Manuel Romero-Sáez Asier Aranzabal M. Pilar González-Marcos José A. González-Marcos Juan R. González-Velasco 《Topics in Catalysis》2013,56(1-8):215-221
The NOx NH3-SCR performance of several Cu and Fe catalysts supported on BETA and ZSM-5 zeolites has been studied in single SCR and double NSR–SCR configuration, and the activity related to the nature and reducibility of metal species on the catalyst surface. Intermediate ammonia formed in NSR improved greatly NOx conversion at the exit of the double NSR–SCR configuration, which was practically totally converted to N2. 相似文献
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M. Pilar González-Marcos Beñat Pereda Unai De La Torre Juan R. González-Velasco 《Topics in Catalysis》2013,56(1-8):352-357
The three-way activity under complex feed-streams of a series of Pt/Ce0.68Zr0.32O2 catalysts, either fresh or submitted to different ageing treatments, both before and after reduction, has been studied and related to the species present on the catalysts in view of their characteristics and TPR behaviour. 相似文献