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排序方式: 共有496条查询结果,搜索用时 31 毫秒
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Summary The synthesis and thermal degradability of poly (DL-lactide) were investigated. Key factors affecting the polymer molecular weight were found to be monomer recrystallization, initiator concentration and the vacuum level during drying/sealing of the polymerization reaction ampoule. It was found that poly (DL-lactide) is thermally unstable above its melting temperature. Monomer recrystallization, polymer precipitation and a low initiator content of the polymer significantly inhibited the rate and extent of thermal degradation. 相似文献
4.
Urs E. Gattiker 《Behaviour & Information Technology》1988,7(4):345-359
Organizational adjustment to technological change and its impact upon human resources should be based on an understanding of employee perceptions and behavioural responses to such developments. An analytic framework which relates strategic choice to internal labour market and employee determinism is derived from the methods employed by organizational theorists and psychologists to generate a set of typologies. The framework divides variables in four classes: (1) natural selection, with minimum choice and adaptation or selection out; (2) differentiation, with high choice and high employee determinism and adaptation within constraints; (3) strategic choice, with maximum choice and adaptation by design; and (4) undifferentiated choice, with incremental choice and adaptation by chance. Useful in reconciling previously inconsistent or incompatible theories of technological change, the framework is offered as a co-ordination device to integrate the results of divergent approaches to technological adaptation studies. 相似文献
5.
Urs E. Gattiker 《Journal in Computer Virology》2007,3(2):149-161
The Bologna process has resulted in the re- structuring of undergraduate and graduate education across Europe. This paper outlines what these changes mean for acquiring degrees in information security and how various universities have tried to respond to these demands. What is unclear at this stage is how the offering of continuous master degrees at Polytechnic and Applied Science Universities will affect the content and curriculum being taught in computer science and information security in particular. This question must be addressed since polytechnics are more industry focused and less research oriented than their university-counterparts. What seems to be clear at this stage is that continuous type master programs in computer science demand a greater level of mathematical knowledge than specialized masters. Moreover, due to the amount of credits that must be acquired, graduates of these types of programs will bring a deeper knowledge about the specialization such as, information security or malware, they acquired at university. This movement toward greater convergence in post secondary education may not have made things easier for recruiters, who are trying to hire graduates in information security or anti-virus experts. In fact, as this paper shows while the Bologna process may have eliminated the obvious differences, countless intricate and not so obvious differences have been added making it sometimes obscure for a bystander. 相似文献
6.
D Del Bufalo C Cucco C Leonetti G Citro I D'Agnano M Benassi T Geiser G Zon B Calabretta G Zupi 《Canadian Metallurgical Quarterly》1996,74(3):387-393
We investigated the effect of c-myb antisense phosphorothioate oligodeoxynucleotides [(S)ODNs] and cisplatin (CDDP) combination on the human colon carcinoma cell line LoVo Dx both in vitro and in nude mice bearing LoVo Dx solid tumour. We show that antisense (S)ODN treatment decreases c-myb mRNA and protein expression, induces growth arrest in the G1 phase of the cell cycle, and inhibits cell proliferation. In vivo treatment with c-myb antisense (S)ODNs results in a reduction in tumour growth. A greater inhibition of cell proliferation in vitro and a higher increase of tumour growth inhibition and growth delay in vivo were obtained with the combination of (S)ODNs and CDDP than when the two agents were administered separately. This comparative study, using the same tumour cell line in vitro and in vivo, suggests that c-myb antisense (S)ODNs might be useful in the therapy of colon cancer in combination with antineoplastic drugs. 相似文献
7.
Roland Gauch Urs Leuenberger und Urs Müller 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1989,188(1):36-38
Zusammenfassung Es wird eine Methode zur Bestimmung von Glyphosat und dessen Hauptmetabolit Aminomethylphosphonsäure (AMPA) in Trinkwasser beschrieben, die es erlaubt, den in der Schweiz geforderten Toleranzwert von 0,1 g/1 zu erreichen (Nachweisgrenze 0,02 g/l). Die Wasserprobe wird dabei direkt mit 9-Fluorenylmethyl-chloroformaat (FMOCCI) versetzt, um extrahierbare und gleichzeitig fluorescierende Derivate zu erhalten. Diese werden nach Ausschütteln mit einem organischen Lösungsmittelgemisch durch HPLC mit Fluorescenzdetektor bestimmt. In bisher 151 untersuchten Trinkwasserproben des Kantons Bern konnten weder Glyphosat noch AMPA nachgewiesen werden.
Determination of glyphosate herbicide and its main metabolite aminomethylphosphonic acid (AMPA) in drinking water by HPLC
Summary A method for the determination of glyphosate and its major metabolite aminomethylphosphonic acid (AMPA) is described. With a detection limit of 0.02 g/l, the method suitably fulfills the requirements of the Swiss legislation (tolerance value of 0.1 g/l water). The compounds are derivatized directly in the original water sample with 9-fluorenylmethyl chloroformate (FMOCCI) in order to obtain extractable and fluorescent derivatives. These are extracted with organic solvents and determined by HPLC using a fluorescence detector. Neither of the compounds could be detected in 151 tap water samples from the Canton of Berne.相似文献
8.
Urs T. Gonzenbach ré R. Studart David Steinlin Elena Tervoort Ludwig J. Gauckler 《Journal of the American Ceramic Society》2007,90(11):3407-3414
Direct foaming of colloidal suspensions is a simple and versatile approach for the fabrication of macroporous ceramic materials. Wet foams produced by this method can be stabilized by long-chain surfactants or by colloidal particles. In this work, we investigate the processing of particle-stabilized wet foams into crack-free macroporous ceramics. The processing steps are discussed with particular emphasis on the consolidation and drying process of wet foams. Macroporous alumina ceramics prepared using different consolidation and drying methods are compared in terms of their final microstructure, porosity, and compressive strength. Consolidation of the wet foam by particle coagulation before drying resulted in porous alumina with a closed-cell structure, a porosity of 86.5%, an average cell size of 35 μm, and a remarkable compressive strength of 16.3 MPa. On the other hand, wet foams consolidated via gelation of the liquid within the foam lamella led to porous structures with interconnected cells in the size range from 100 to 150 μm. The tailored microstructure and high mechanical strength of the macroporous ceramics can be of interest for the manufacture of bio-scaffolds, thermal insulators, impact absorbers, separation membranes, and light weight ceramics. 相似文献
9.
Prediction of the biologically active sites in eclosion hormone from the silkworm, Bombyx mori 总被引:1,自引:0,他引:1
Kikuchi T; Okamoto M; Geiser M; Schmitz A; Gohda K; Takai M; Morita T; Horii K; Fujita N 《Protein engineering, design & selection : PEDS》1997,10(3):217-222
The structure-activity relationship of eclosion hormone from the silkworm,
Bombyx mori, was analyzed. First, the probable active residues in silkworm
eclosion hormone and also tobacco hornworm eclosion hormone were predicted
by the average distance map method. To examine the contributions of those
residues to the activity of silkworm eclosion hormone, Gly-substituted
mutants for those predicted residues were produced by site-directed
mutagenesis and their activities were evaluated by a bioassay. Finally,
Glu12, Met24 and Phe25 were estimated to be the crucial residues for the
eclosion hormone activity. The possibility of the development of a blocker
of an eclosion hormone receptor on the basis of the present work is also
discussed.
相似文献
10.
Ennoblement of stainless steel (SS) by microbially deposited manganese oxides can lead to pitting corrosion at low chloride concentrations, causing unexpected material failures. We exposed 316L SS to manganese oxidizing bacteria Leptothrix discophora under well-defined laboratory conditions, and then placed the ennobled coupons in a 0.5 M sodium chloride solution until pitting developed. Using time-of-flight secondary ion mass spectroscopy we demonstrated that the pits and their immediate vicinity associated with microbial influenced corrosion had different chemical signatures than those associated with electrochemically induced pitting, suggesting a possibility that the microorganisms were directly involved in pit initiation. Based on the differences in the chemical signatures we were able to distinguish the microbially induced pits from those induced by anodic polarization. 相似文献