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1.
Development of an octocalcium phosphate cement 总被引:2,自引:0,他引:2
O. Bermúdez M. G. Boltong F. C. M. Driessens J. A. Planell 《Journal of materials science. Materials in medicine》1994,5(3):144-146
From previous studies it is known that alpha-tertiary calcium phosphate and dicalcium phosphate form a cement upon mixing with water. In this study this cement was optimized in terms of the milling of the constituents, their molar ratio, the amount of hydroxyapatite added and the water/powder ratio. The optimum Ca/P molar ratio of the cement mixture was 1.36±0.03. X-ray diffraction showed the reaction product to be octocalcium phosphate. Addition of precipitated hydroxypatite of over 3% diminished the final strength of the cement significantly. However, admixtures of only 2% of precipitated hydroxyapatite (a) kept the final compressive strength at 30±5 MPa after soaking in Ringers solution at 37°C, (b) diminished the initial setting time from 27.5 to 10 min and the final setting time from 65 to 40 min, (c) diminished the time in which the final strength was reached from 36 to less than 14 h. The tensile strength of this cement is 19±1% of its compressive strength. The optimum water/powder ratio as found in this study was 0.30 g/g. 相似文献
2.
E. E. Vicente S. Bermúdez A. Esteban R. Tendler B. Arcondo H. Sirkin 《Journal of Materials Science》1991,26(5):1327-1332
Invariant three- and four-phase equilibria in the magnesium-rich corner of the Mg-Cu-Sn ternary system have been studied by differential thermal analysis, optical microscopy, electron probe microanalysis and X-ray diffraction. The L(Mg) + Mg2 Cu + Mg2Sn ternary eutectic reaction was found to be at 467 °C and at Mg–13.5 at % Cu–4.4 at% Sn. The LMg2Cu + Mg2Sn pseudo-binary eutectic reaction is tentatively located at 522°C and at Mg–26.0 at % Cu–7.7 at % Sn. 相似文献
3.
J. Saúl García-Pérez Sara P. Cuéllar-Bermúdez Alejandra Arévalo-Gallegos José Rodríguez-Rodríguez Hafiz M. N. Iqbal Roberto Parra-Saldivar 《International journal of molecular sciences》2016,17(9)
Supercritical fluid extraction (SFE) is a sustainable technique used for the extraction of lipophilic metabolites such as pigments and fatty acids. Arnica plant is considered a potential candidate material with high antioxidant and antimicrobial activities. Therefore, in this study, a locally available Heterotheca inuloides, also known as Mexican arnica, was analyzed for the extraction of high-value compounds. Based on different pressure (P), temperature (T), and co-solvent (CoS), four treatments (T) were prepared. A maximum 7.13% yield was recovered from T2 (T = 60 °C, P = 10 MPa, CoS = 8 g/min), followed by 6.69% from T4 (T = 60 °C, P = 30 MPa, CoS = 4 g/min). Some bioactive sesquiterpenoids such as 7-hydroxycadalene, caryophyllene and δ-cadinene were identified in the extracts by GC/MS. The fatty acid profile revealed that the main components were palmitic acid (C16:0), followed by linoleic acid (C18:2ω6c), α-linolenic acid (C18:3ω3) and stearic acid (C18:0) differing in percent yield per treatment. Antibacterial activities were determined by the agar diffusion method, indicating that all the treatments exerted strong antibacterial activity against S. aureus, C. albicans, and E. coli strains. The antioxidant capacity of the extracts was also measured by three in vitro assays, DPPH, TEAC and FRAP, using Trolox as a standard. Results showed high antioxidant capacity enabling pharmaceutical applications of Mexican arnica. 相似文献
4.
Loss of stature in certain elderly subjects can be attributed to diseases such as osteoporosis, as well as to age and generational effects. In addition, many elders cannot stand straight for accurate measurement. For these cases, total height can be estimated with regression equations based on knee height. The aims of this study were, firstly, to evaluate the applicability of regression equations based on knee height for estimation of stature and, secondly, to document the differences between measured and estimated height in a group of elderly Hispanics with postural problems (n = 166) in comparison with a group of elderly Hispanic without postural problems (n = 270). Using both, estimated and measured height, we also calculated the body mass index (BMI) of both groups of elders. Statistical analyses were done with paired t-tests, within sex and study group. Within the group with postural problems, estimated height was higher than the measured height for both men (p < or = 0.001) and women (p < or = 0.001). There were no significant differences between measured and estimated height in the group without postural problems. Furthermore, in the group with postural problems, BMI values calculated with estimated height were lower than those estimated with the measured height, and these differences were also significant for both men (p < or = 0.001) and women (p < or = 0.001). With the aging of the Latin American population, there is a need for more nutrition and health research among elders. In order to do this we need to develop and use methods and criteria appropriate for each population. 相似文献
5.
6.
Microwave heating can be used to promote heterogeneous reactions with carbon materials, mainly because of the heating mechanism involved in microwave radiation and the phenomenon known as microplasmas. This work presents photographic evidence of plasma formation when different carbon materials are subjected to microwave heating. Two different kinds of plasmas were observed: ball lightning and arc discharge plasmas. The intensity of the plasmas in the less ordered carbon was significantly higher at the beginning of the process. 相似文献
7.
José María Desantes Vicente Bermúdez Antonio García Waldemar G. Linares 《Aerosol science and technology》2013,47(10):1161-1175
Control strategies such as variations in injection pressure and timing have been used by researchers to reduce in-cylinder exhaust emissions and meet legislation standards. Postinjection has been studied for several years and is now well known as an efficient strategy for reducing soot emission. Diesel gaseous and particle mass emissions have been progressively reduced over the last twenty years as a consequence of increasingly restrictive emission legislation and the application of aftertreatment devices. The main objective of this work is to better understand the effect of postinjection on particle size distribution in diesel exhaust. The approach uses a modern, well-instrumented research engine test cell equipped with a flexible high pressure fuel injection system. The results of this work provide guidelines for developing strategies to reduce particle size distribution in diesel engines. A major improvement in particle size distribution was found in the accumulation mode by using a close postinjection of a small quantity of fuel. For reduction in nucleation mode, a relationship was found with close postinjections of large quantities of fuel. 相似文献
8.
This paper deals with the numerical simulation of unsteady aerodynamics effects in horizontal-axis wind turbines. In particular, an unsteady three-dimensional potential method is presented whose aim is to predict time-dependent forces and moments on wind turbines operating in a field environment. The algorithm structure is such that the wake is not prescribed; instead, its shape and motion are obtained self-consistently from the solution of the problem. Flow separation effects are not considered. Once the mathematical formulation is discussed, the results of the solver validation campaign, including a parametric sensitivity study of the solutions, are presented. Then, the solver is applied to a practical case involving a wind turbine specifically constructed to collect unsteady aerodynamics data. It is found that the comparison between experimental data and computed results shows a good agreement. Finally, conclusions are drawn. 相似文献
9.
R. Mazzei G. García Bermúdez A. Fernández N. Betz 《Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms》2008,266(6):937-943
The present work is part of a systematic study that involves different polymeric substrates and monomers with the purpose to induce grafting on etched tracks. The residual active sites produced by heavy ion beams, remaining after the etching process, were used to start the grafting process. In order to produce tracks on foils of poly(vinylidene fluoride) (PVDF) they were irradiated with 208Pb of 25.62 MeV/n or with 115 MeV Cl ions. Then, they were etched and grafted with N-isopropylacrylamide (NIPAAm) monomers. Experimental curves of grafting yield as a function of fluence with the etching time as a parameter were measured. Also, the grafting yield as a function of the grafting and etching time was obtained. The replica method allowed the observation of the shape of the grafted tracks using transmission electron microscopy (TEM). In addition NIPAAm grafted foils were analyzed using Fourier transform infrared spectroscopy (FTIR). 相似文献
10.
Bruno Almeida Dr. Jesús Joglar María Jesús Luque Rojas Juan Manuel Decara Francisco Javier Bermúdez‐Silva Dr. Manuel Macias‐González Dr. Montserrat Fitó Miguel Romero‐Cuevas Dr. Magí Farré Dr. María Isabel Covas Dr. Fernando Rodríguez de Fonseca Dr. Rafael de la Torre 《ChemMedChem》2010,5(10):1781-1787
A series of fatty acid amides of 3,4‐methylenedioxymethamphetamine (MDMA) catechol metabolites were synthesized in order to evaluate their biological activities. Upon administration, all synthesized compounds resulted in negative modulation of food intake in rats. The most active compounds have affinity for the CB1 receptor and/or PPAR‐α; part of their biological activity may be caused by these double interactions. 相似文献