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AgCuV合金导电滑环在进行超声检测时发现有内部缺陷的存在。采用化学成分分析、超声检测、金相检验、扫描电镜及能谱分析等方法对缺陷产生的原因进行了分析。结果表明:AgCuV合金导电滑环经超声检测发现的内部缺陷是裂纹,脆性的含钒第二相与AgCu合金基体的结合力弱并且易碎,在应力集中处产生了微裂纹,微裂纹沿着第二相与基体结合力弱的部位扩展,最终导致AgCuV合金导电滑环内部缺陷的产生。 相似文献
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The ZrO_2 ceramic was successfully jointed to stainless steel by vacuum brazing with active filler metal. The AgCuTi active filler metal was used and the joining was performed at a temperature of 850 ℃ for 10 min. The microstructures of the joints were characterized by metallographic microscopy,scanning electron microscopy( SEM),and energy dispersive spectroscopy( EDS).Metallographic microscopy analysis shows that the morphology of the cross section was a sandwich structure and the Ti O is observed in the surface of ZrO_2/stainless steel. The diffusion and enrichment of the elements are the key roles in the brazing of ZrO_2 ceramic and stainless steel. The formation of TiCu compounds inhibited the further diffusion of titanium into stainless steel or the ZrO_2 ceramic to form TiO compound. In the experimental conditions,the average tensile strength is 80 MPa for the joint of ZrO_2 ceramic/Ag Cu Ti/stainless steel systems. A complete joint is formed between the ZrO2 ceramic and stainless steel with the leakage rate at the degree of 10~(-12) Pa·m~3/s. 相似文献
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为研究混合稀土元素在金银铜合金内部的分布状态以及混合稀土元素的添加对金银铜合金硬度的影响,使用真空中频感应炉制备了Au-35Ag-5Cu、Au-35Ag-5Cu-1RE合金,并对铸态合金进行不同变形量的轧制加工,探讨了稀土元素的添加、变形量对合金组织及维氏硬度的影响。使用EDS进行了稀土元素分布检测、DSC分析固液相线温度并进行维氏硬度的测量等。结果表明,稀土元素La、Ce、Pr、Nd占据了Au、Ag元素的位置,改变了AuAg两种元素的分布,与Cu固溶效果较好,对Cu元素分布没有显著影响。稀土元素的添加降低了Au-35Ag-5Cu的液相线温度和固相线温度,增大了液相线温度和固相线的温度差。混合稀土元素的添加有助于提高铸态及轧制态金银铜合金的耐磨性。 相似文献
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研究了Sn元素对Ag-Cu-In合金钎料加工及钎焊性能的影响。结果表明:Ag-Cu-In合金钎料中加入一定量的可以有效降低钎料的熔化温度,当8%Sn元素加入Ag-Cu-In合金中,其熔化温度降低为575~620 ℃,可以加工为0.10 mm厚的带材,钎焊性能良好;随着合金中Sn元素含量的增加,合金钎料中的脆性相增多、变大,导致合金的加工性能变差,不能成型。 相似文献
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Zhang Guoqing, Feng Xingmei, Feng Zhanying, Tang Chao, Wang Feng and Qi Yuefeng
Effect of mixed rare earth and Sr on microstructure and brazability of Al-20Cu-5Si-2Ni filler metal
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The objective of this study is to investigate the influence of adding tiny amount of mixed rare earth ( La, Ce) and Sr to Al-20Cu-5Si-2Ni filler metal, by analyzing the microstructure, wettability and mechanical properties of brazed joints. The results show that with the addition of mixed rare earth ( La, Ce) into Al-20Cu-5Si-2Ni alloy, the α-Al solid solution as well as CuAl2 ( Ni) intermetallic compound phase significantly reduced, while more Al-Si eutectic phase and Al-Si-Cu ternary eutectic phase were produced. And as mixed rare earth ( La, Ce) added in, the wettability of Al-20Cu-5Si-2Ni filler metal decreased, while the shear strength of the brazed joints increased. The addition of Minor Sr modificated Al 20Cu-5Si-2Ni filler metal, further reduced the CuAl2 ( Ni) intermetallic compound phase, which was partially replaced Al-Si-Cu ternary eutectic phase. As a result, the tensile strength as well as the wettability of the filler metal was improved. 相似文献
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通过在Ag-26Cu-5Ti钎料中添加21. 5%In,设计开发了一种新型Ag Cu In Ti合金钎料,用于实现Al2O3陶瓷与无氧铜的活性连接,同时改善流动性,提高活性。对钎料的固液相温度与润湿铺展性能进行分析,并测试了Al_2O_3/Ag Cu In Ti/Cu试验件抗拉强度和气密性。通过金相显微镜、扫描电子显微镜观察试验件微观界面组织,进一步探究Ag Cu In Ti合金钎料的活性连接反应机理。结果表明,Ag Cu In Ti合金钎料在750℃实现了对陶瓷和金属的真空活性连,降低了钎焊温度,满足分级钎焊和补焊的需求,且形成结合紧密的反应界面,证明其对陶瓷具有良好的润湿性;钎焊过程中合金钎料中的Ti元素向Al_2O_3陶瓷界面富集,形成多个界面产物,而合金钎料中Ag元素、Cu元素、In元素与无氧铜发生溶解扩散,生成新的化合物相,最终实现陶瓷与金属的冶金结合。 相似文献
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通过差热分析、扫描电镜显微组织分析、真空钎焊等手段,对不同Pd含量Ag-Cu-Pd钎料的熔化特性以及在无氧铜和镍上铺展性进行研究,并对铸态组织和钎焊界面组织进行分析.结果表明,随着Pd含量增加,Ag-Cu-Pd钎料的固相线温度、液相线温度有明显提高,固液相线温度间隔也随之增大;当Pd含量为10 %和20 %时钎料铺展性良好,且随着Pd含量增加,钎料合金铺展性降低,但当Pd增加到30 %时,钎料铺展性变差且有轻微侵蚀迹象;铸态Ag-Cu-Pd合金中Pd元素主要存在于富铜相中;Ag-28Cu-20Pd钎料焊接无氧铜板时的钎焊界面,形成连续的金属间化合物(IMC)层,钎料中Pd元素主要分布在IMC层上. 相似文献
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