Oxime-Modified Aluminum(III) Isopropoxide: A Promising Sol–Gel Precursor for Corrosion Resistive Nano-Alumina Coating on an Aluminum Alloy

Protection of Metals and Physical Chemistry of Surfaces - Dense alumina coatings were fabricated over aluminum alloy via dip coating method using oxime-modified aluminum(III) isopropoxide as a...     

Simultaneous three-dimensional step-height measurement and high-resolution tomographic imaging with a spectral interferometric microscope

A noncontact, nonmechanical scanning, wide-field spectral interference microscope is developed for simultaneous measurement of three-dimensional step-height of discontinuous objects and tomographic imaging. A superluminescent diode (SLD) is used as a broadband light source and a liquid-crystal Fabry-Perot interferometer (LC-FPI) as a frequency-scanning device. By means of changing the injection current to the SLD, the spectral profile of the SLD is equalized, and a constant light input to the interferometer is achieved over the entire frequency-scan range. The Fourier-transform technique is used to determine both the amplitude and the phase of spectral fringe signals. Three-dimensional height distribution of a discontinuous object is obtained from the phase information, whereas optically sectioned images of the object are obtained either from the amplitude information alone or from the combination of both the amplitude and phase information. Experimental results with submicrometer resolution are presented for both step-height measurement and tomographic sectioning.     

Spectral interferometric microscope with tandem liquid-crystal Fabry-Perot interferometers for extension of the dynamic range in three-dimensional step-height measurement

The maximum measurable range of a spectral interference microscope depends on the coherence length of the light transmitted by its tunable spectral filter. To achieve a large range in step-height measurement we have developed a new tunable spectral filter that uses tandem liquid-crystal Fabry-Perot interferometers (LC-FPIs), which can simultaneously attain both a high spectral resolution and a large tuning range. Fringe visibility measurements were carried out, and it was found that the coherence length of the light transmitted through tandem LC-FPIs is two times larger than that transmitted through a single LC-FPI. Using this novel tunable spectral filter, we developed a new spectral interference microscope for the measurement of three-dimensional shapes of discontinuous objects. Experimental results of step-height measurements both with a single LC-FPI and with tandem LC-FPIs are presented for a combination of standard steel gauge block sets with 1-, 99-, and 100-microm steps. A large range (1-100 microm) of measurement with submicrometer resolution was achieved with tandem LC-FPIs that was not possible with our previous system in which a single LC-FPI was used.     

Spectral interference Mirau microscope with an acousto-optic tunable filter for three-dimensional surface profilometry

A nonmechanical scanning Mirau-type spectral interference microscope has been developed for the measurement of three-dimensional surface profiles of discontinuous objects. An acousto-optic tunable filter (AOTF) is used as a high-resolution spectral filter, which scans the optical frequency of the broadband light emitted from a superluminescent diode. To generate spectral fringes that make full use of the limited coherence length of the filtered light we unbalanced the Mirau interferometric system by positioning the reference mirror nearly halfway between the top and the bottom of the step height. When the frequency of the broadband light source is scanned by an AOTF, the interference fringes move in opposite directions on the top and the bottom of the object. To uniquely determine the sign of the fringe movement over the large area of the object, we developed a three-dimensional Fourier-transform technique, and from the detected sign of the fringe movement and phase information, we determined the three-dimensional step height. Experimental results of the measurement of 100-microm step height are presented. The main advantages of the proposed system are that it provides nonmechanical scanning and a large measurement range without ambiguity in the sign of the phase.     

High-resolution full-field optical coherence microscopy using a Mirau interferometer for the quantitative imaging of biological cells

In this paper quantitative imaging of biological cells using high-resolution full-field optical coherence microscopy (FF-OCM) is reported. The FF-OCM was realized using a swept-source system, a Mirau interferometer, and a CCD camera (a two-dimensional detection unit). A Mirau-interferometric objective lens was used to generate the interferometric signal. The signal was analyzed by a Fourier analysis technique. Optically sectioned amplitude images and a quantitative phase map of biological cells such as onion skin and red blood cells (RBCs) are demonstrated. Further, the refractive index profile of the RBCs is also presented. For the 50× Mirau objective, the experimentally achieved axial and transverse resolution of the present system are 3.8 and 1.2 μm, respectively. The CCD provides parallel detection and measures enface images without X, Y, Z mechanical scanning.     

Visualization of internal energy flows in optical fields carrying a pair of fractional vortices

The internal energy flows resulting from the azimuthal component of optical currents in beams carrying a pair of fractional vortices during propagation have been experimentally detected in a knife edge test. Two optical vortices of fractional charge in a beam pair up by means of a connecting dark intensity line between intensity zeros of the vortices. Independent of the polarity of the fractional vortices, this pairing up process occurs. This is in contrast to the isolated intensity null points of vortices of integer charges and thus calls for a study on the internal energy flows in such beams.     

Controlled modulation of laser beam and dynamic patterning of colloidal particles using optical tweezers

We present controlled generation of complex-structured beam profiles using diffractive optical element and demonstrate multiple dynamic trapping of colloidal particles. The phase element is programmed to generate various tailored optical fields having structures, similar to that of number three, spiral, and circle but in a tractable manner. Thus, the generated spatially tailored optical fields are confined to focal volume in optical tweezers. This enabled real-time trapping of multiple microscopic objects whereby its transverse organization was controlled in a dynamic manner from one structure to another with the help of spatial light modulator. Such a controlled beam shaping finds potential applications in biophotonics, super resolution imaging, and measurement of biophysical parameters, cell sorting, and micro-manipulation of colloidal particles.     

Laser speckle reduction by multimode optical fiber bundle with combined temporal, spatial, and angular diversity

We report significant speckle reduction in a laser illumination system using a vibrating multimode optical fiber bundle. The optical fiber bundle was illuminated by two independent lasers simultaneously. The beams from both lasers were first expanded and collimated and were further divided into multiple beams to illuminate the fiber optic bundle with normal and oblique incidence. Static diffusers were also placed at the input and output faces of the fiber bundle, thus introducing the spatial as well as angular diversity of illumination. Experiments were carried out both in free space and in imaging geometry configuration. Standard deviation, speckle contrast and signal-to-noise ratio of the images were computed, and the results were compared with those of white light illumination. Speckle contrast close to that of white light was obtained using a vibrating fiber bundle with combined temporal, spatial, and angular diversities of the illumination.     

Two-wavelength Talbot effect and its application for three-dimensional step-height measurement

The phenomenon of Talbot self-image shift by changing the wavelength of the illuminating light is described and demonstrated experimentally. A periodic grating is illuminated by light with wavelengths lambda1 and lambda2 generated by two lasers, and the Talbot self-images are recorded along the longitudinal direction at individual wavelengths. The Talbot self-image shift due to the change in the wavelength of light is implemented for the measurement of the three-dimensional step height of a large discontinuous object without any phase ambiguity problem. Fourier-transform fringe analysis was used to determine the maximum contrast of the high-visibility bands for the measurement of the step height of the object. The main advantages of the proposed system are nonmechanical scanning, high stability because of its common path geometry, compactness, and a wide range of measurement as compared to interferometric three- dimensional profilers.