H2S optimization for lignite liquefaction

Two lignite samples, Beulah No. 3 and Big Brown No. 1, were liquefied at 420 °C using H₂ and synthesis gas to determine the optimum beneficial amount of H₂S in the batch autoclave reactor. Under the conditions employed, 50–100 psi partial pressure of H₂S, nominally 4–10 wt% of daf lignite, was optimum for both samples. Synthesis gas outperformed H₂ with and without H₂S for the liquefaction of the two coals.     

链烷烃的表面张力与内压

对Ｄａｖｉｓ和Ｒｏｓｓｅｉｎｓｋｙ提出的关系检验表明，液体的表面张力σ与Ｐ１Ｖｍ１／３之比不仅取决于温度，还与液体的种类有关，据此，建立了一个能由链烷烃的分子结构准确预测其表面张力的方法。     

电子商务中SET协议的安全缺陷研究

目前SET协议在电子商务交易中应用越来越广泛,因此,对SET协议的安全性的要求就越来越高。论文在SET协议的交易流程基础上,分析了其安全机制采用的技术和优点,指出了SET协议安全性存在的一些问题。     

冷库地坪防冻臌机械通风的传热计算

设计手册中关于使用机械通风防止冷库地坪冻臌的参数（风道直径、间距及长度）仅是推荐值，它忽略了地坪结构、土壤温度和外界空气温度对通风系统节能的影响，因而造成地基土壤的热损失和冷库负荷的增大。从冷库节能和冷库建筑安全使用出发，对采用机械通风防止地坪冻臌进行了传热分析，提出了在传热计算中参数的合理选择和通风系统的设计方法。     

摩擦诱发高铬铸铁相变的透射电镜研究

利用透射电子显微镜研究了高铬铸铁在摩擦过程中的显微组织变化。结果表明：奥氏体基体在摩擦应力的作用下发生相变。摩擦表面形成α‘Ｍ。次表层形成γ与α’Ｍ共存区；γ与．ε共存区；γ位错丛聚区。     

离子镀铝青铜膜的XTEM研究

本文利用透射电镜对离子镀铝青铜膜进行横截面显微组织研究结果表明:整个膜层分为细等轴晶、细纤维状及柱状晶三种不同形态的生长区并且柱状晶主要以孪晶方式生长膜中存在NiAIl Cu_9Al_4合金相,与基体取向关系为:讨论了膜层成核和生长过程发现气相沉积膜层中存在生长条纹     

Covalent Adaptable Microstructures via Combining Two-Photon Laser Printing and Alkoxyamine Chemistry: Toward Living 3D Microstructures

Manufacturing programmable materials, whose mechanical properties can be adapted on demand, is highly desired for their application in areas ranging from robotics, to biomedicine, or microfluidics. Herein, the inclusion of dynamic and living bonds, such as alkoxyamines, in a printable formulation suitable for two-photon 3D laser printing is exploited. On one hand, taking advantage of the dynamic covalent character of alkoxyamines, the nitroxide exchange reaction is investigated. As a consequence, a reduction of the Young´s Modulus by 50%, is measured by nanoindentation. On the other hand, due to its “living” characteristic, the chain extension becomes possible via nitroxide mediated polymerization. In particular, living nitroxide mediated polymerization of styrene results not only in a dramatic increase of the volume (≈8 times) of the 3D printed microstructure but also an increase of the Young's Modulus by two orders of magnitude (from 14 MPa to 2.7 GPa), while maintaining the shape including fine structural details. Thus, the approach introduces a new dimension by enabling to create microstructures with dynamically tunable size and mechanical properties.     

基于SoPC的SD卡控制器IP核的设计

针对目前在嵌入式平台中使用SD卡控制器专用芯片价格昂贵、软件模拟SPI时序控制读写速度较慢的问题,提出了一种基于SoPC技术的SD卡控制器IP核设计的架构方案.采用VHDL语言设计SD卡控制器IP核,利用自定义模块技术将其添加到SoPC中,利用Nios Ⅱ IDE编写SD卡的基础读写驱动软件并移植μC/FS文件系统,实...