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排序方式: 共有212条查询结果,搜索用时 15 毫秒
1.
Kenzo Kitayama 《Journal of the American Ceramic Society》1992,75(6):1447-1451
Phase equilibria in the Ta-Co-O and Nb-Co-O systems have been studied at 1200°C at oxygen partial pressures from 10−0.68 to 10−13.50 atm for the former and from 10−0.68 to 10−13.30 atm for the latter. In both systems, M2 CoO6 and M2 Co4 O9 are stable ternary compounds under the experimental conditions, and a new phase, Nb5 Co2 O14 , has been identified. The Ta-Co-O system is simple, whereas the Nb-Co-O system is somewhat more complicated because of the extra phase. The lattice constants of the ternary compounds have been determined and compared with previous values. The standard Gibbs energies of reactions have been determined using oxygen partial pressures in equilibrium with three solid phases. 相似文献
2.
We observed change in distance between two droplets in each step after application of large multi-step shear strains. Experiments were performed using a sliding plate apparatus. Large step shear strains were applied to two polyisobutylene droplets in poly(dimethyl siloxane) matrix in the same plane between the plates. The distance between the two droplets decreases with increasing the total shear strain, which is given by the product of the step strain magnitude and the number of application of the step strains. The two droplets coalesce when the distance becomes less than the diameter of the droplets. The slope for plots of the distance versus the total strain is independent of the step strain magnitude. This indicates that the effect per unit strain on the distance is the same, irrespective of the strain magnitude. It is suggested that a stronger hydrodynamic interaction between the droplets is the main cause for the droplet approach. 相似文献
3.
Hiromasa Higasa Ryoichi Takahata Hiroshi Imaizumi Kenzo Miya 《Electrical Engineering in Japan》1996,116(3):96-106
A high-temperature superconductor YBa2Cu3O7-x with strong pinning force has allowed stable magnetic suspension with no control to be developed. Two types of superconducting magnetic bearings (SMB) using YBCO and permanent magnet were assembled. The two types are radial and axial. The dynamic stiffness of each SMB as it was cooled down under a magnetic field by liquid nitrogen was measured both radially and axially. As a result, it was found that the spring constants of these SMBs were almost as large as a practically desirable value; however, their damping coefficients were lower than the practical level. These findings are useful as one of the data bases for development of an optimum SMB design to support the weight of rotors in an axial direction. 相似文献
4.
The UV-stabilizing ability and thermal loss from the polystyrene film of novel UV absorbers, 2-[(3-hydroxy-4-benzoyl) phenoxy] pentachlorocyclotriphosphazene (HBPC) and hexakis[ (2-hydroxy-4-benzoyl) phenoxy] cyclotriphosphazene (HBPP), were investigated. The UV-stabilizing ability of HBPC estimated by the formation of carbonyl groups in polystyrene was comparable to that of 2,4-dihydroxybenzophenone (DHB), suggesting that the phosphazene moiety does not affect the efficiency of the stabilizing ability of DHB units. No significant difference of efficiency per stabilizing units between HBPC and HBPP was observed. HBPC and HBPP are noteworthy for their low thermal losses from the polystyrene film, i.e., the thermal loss of HBPP was completely suppressed and the diffusion coefficient of HBPC at 160°C was two orders of magnitude smaller than that of DHB. The thermogravimetric analysis and differential scanning calorimetry measurement showed that HBPC and HBPP are nonvolatile and stable up to 230 and 300°C, respectively. © 1993 John Wiley & Sons, Inc. 相似文献
5.
Kenzo Sato 《Journal of Infrared, Millimeter and Terahertz Waves》1986,7(9):1361-1416
We have investigated the IR reflectional properties of the three-hold cytrogical surface layer (kutchikura layer on silicate layer n(SiO2) on silicate cellulose layer C6H10SixOy) and that of chlorophyll, a(C55H72MgN4O5) etc., present in bladder's cells by using our experimental method. From analysis of three set of anisotropical reflection spectra assigned as due to CO, SiO and NC surface oscillators contained in the cytrogical cells and measured at 2500 2200 cm?1, 1200 700 cm?1 and at 700 200 cm?1 regions, we have confirmed some important results. One is their quantized directional distributions that of the numbers of fine step spectrum and that of the reflection integrals of these spectra. Here, that of the NC oscillators were found to distribute in pentagonal directions relating to the molecular structure of chlorophyll. Second, we confirmed the pecularity of eight fine step-series measured in these sensitive spectra comparing with that of bamboo's seven series. Third, from analysis of the stepnized variation of the “reflection integrals”, we estimated the origin of this effect as which is presumably due to statistical, transfer of the 2p4 valence electrons etc. in the oxygen atoms from C=O, Si=O double bonding side upto the shallower quantized states, E(N,J) which were formed softly around the and surface oscillators. And these surface oscillators were confirmed as to make photo-chemical reaction process by receiving energy higher than ~24 m eV especially under the illumination of sunshine etc. 相似文献
6.
Annadanam V. Sesha Sainath Takashi Inoue Yoshiharu Hatakeyama Masahiro Shishido Kenzo Okamoto Seigou Kawaguchi Takashi Kuriyama Kiyohito Koyama 《大分子材料与工程》2004,289(3):264-268
Summary: Polyacrylonitrile (PAN) particles with micro‐size ranges (0.15–2 μm) were prepared by emulsion and dispersion polymerizationa and in supercritical carbon dioxide media. The PAN particles were blended with Nylon 6 (PA6) at 220 °C by using a miniature mixer; it was found that melt‐mixing was possible for PAN‐rich compositions as high as 70 wt.‐%. Blends were characterized by scanning electron microscopy, IR, viscosity measurements, differential scanning calorimetry, and dynamic mechanical thermal analysis (DMTA). The size and shape of original PAN particles were retained in PAN/PA6 blends. The useful range to blend PAN particles size was less than 1 μm in terms of shape retention of the PAN particles in blends. Blends with 40 wt.‐% PAN content were found to be melt‐processable. The elastic modulus was higher for PAN/PA6 blends than pure PA6.
7.
Saburo Komori Mitsuo Okahara Kenzo Okamoto 《Journal of the American Oil Chemists' Society》1960,37(10):468-473
Summary Since the long-chain fatty acid sucrose diesters inevitably produced in the synthesis of monoesters are only slightly soluble
in water, no important use can be found for them at the present time except as oilsoluble emulsifying agents.
In order to exploit new uses we have attempted to improve their solubility in water by introducing oxyethylene radicals into
the molecule.
The addition reaction of ethylene oxide with the sucrose diesters was carried out in an autoclave in the presence of alkaline
catalysts. With the reaction temperature maintained between 100–130° the pressure decreased as the reaction proceeded, and
one to two hours were required to consume the ethylene oxide used.
The addition products are yellow or orange oily materials soluble in water. Aqueous solutions showed good surface-active properties. 相似文献
8.
Kenichi Yokoyama Toshio Ogawa Kenzo Asaoka Junichi Sakai 《Journal of Alloys and Compounds》2005,400(1-2):227-233
The hydrogen absorption properties of Ti–0.2 mass% Pd (Ti–0.2Pd) alloy in 2.0% and 0.2% acidulated phosphate fluoride (APF) and neutral 2.0% NaF solutions (25 °C) has been evaluated by hydrogen thermal desorption analysis. During the early stage of immersion (120 h) in the 2.0% APF solution, the amount of absorbed hydrogen was lower than 500 mass ppm. A thermal desorption of hydrogen primary appearing with a peak at 500–600 °C and a broad desorption ranging from 100 to 400 °C were observed. In the 0.2% APF solution, the amount of absorbed hydrogen saturated at 100–200 mass ppm; the thermal desorption of hydrogen appeared with a single peak at 550 °C. In the 2.0% NaF solution, hydrogen absorption was negligible even after 1000 h of immersion, although corrosion pits were observed. The results of the present study suggest that the hydrogen absorption of Ti–0.2Pd alloy, as compared with commercial pure titanium, is suppressed in fluoride solutions. 相似文献
9.
Optimal impedance control based on body inertia for a hydraulically driven hexapod robot walking on uneven and extremely soft terrain 总被引:1,自引:0,他引:1
This paper presents the implementation of impedance control for a hydraulically driven hexapod robot named COMET‐IV, which can walk on uneven and extremely soft terrain. To achieve the dynamic behavior of the hexapod robot, changes in center of mass and body attitude must be taken into consideration during the walking periods. Indirect force control via impedance control is used to address these issues. Two different impedance control schemes are developed and implemented: single‐leg impedance control and center of mass‐‐based impedance control. In the case of single‐leg impedance control, we derive the necessary impedance and adjust parameters (mass, damping, and stiffness) according to the robot legs' configuration. For center of mass–based impedance control, we use the sum of the forces of the support legs as a control input (represented by the body's current center of mass) for the derived impedance control and adjust parameters based on the robot body's configuration. The virtual forces from the robot body's moment of inertia are adapted to achieve optimal control via a linear quadratic regulator method for the proposed indirect attitude control. In addition, a compliant switching mechanism is designed to ensure that the implementation of the controller is applicable to the tripod sequences of force‐based walking modules. Evaluation and verification tests were conducted in the laboratory and the actual field with uneven terrain and extremely soft surfaces. © 2011 Wiley Periodicals, Inc. 相似文献
10.
Small unmanned aerial vehicles (UAVs) are becoming popular among researchers and vital platforms for several autonomous mission systems. In this paper, we present the design and development of a miniature autonomous rotorcraft weighing less than 700 g and capable of waypoint navigation, trajectory tracking, visual navigation, precise hovering, and automatic takeoff and landing. In an effort to make advanced autonomous behaviors available to mini‐ and microrotorcraft, an embedded and inexpensive autopilot was developed. To compensate for the weaknesses of the low‐cost equipment, we put our efforts into designing a reliable model‐based nonlinear controller that uses an inner‐loop outer‐loop control scheme. The developed flight controller considers the system's nonlinearities, guarantees the stability of the closed‐loop system, and results in a practical controller that is easy to implement and to tune. In addition to controller design and stability analysis, the paper provides information about the overall control architecture and the UAV system integration, including guidance laws, navigation algorithms, control system implementation, and autopilot hardware. The guidance, navigation, and control (GN&C) algorithms were implemented on a miniature quadrotor UAV that has undergone an extensive program of flight tests, resulting in various flight behaviors under autonomous control from takeoff to landing. Experimental results that demonstrate the operation of the GN&C algorithms and the capabilities of our autonomous micro air vehicle are presented. © 2009 Wiley Periodicals, Inc. 相似文献