Preparation of Silver Nanowires via a Rapid,Scalable and Green Pathway

Rapid synthesis of silver nanowires(Ag NWs) with high quality and a broad processing window is challenging because of the low selectivity of the formation of multiply twinned particles at the nucleation stage for subsequent Ag NWs growth.Herein we report a systematic study of the water-involved heterogeneous nucleation of Ag NWs with high rate(less than 20 min) in a simple and scalable preparation method.Using glycerol as a reducing agent and a solvent with a high boiling point,the reaction is rapidly heated to 210 ℃ in air to synthesize Ag NWs with a very high yield in gram level.It is noted that the addition of a small dose of water plays a key role for obtaining highly pure Ag NWs in high yield,and the optimal water/glycerol ratio is0.25%.After investigating a series of forming factors including reaction temperature and dose of catalysts,the formation kinetics and mechanism of the Ag NWs are proposed.Compared to other preparation methods,our strategy is simple and reproducible.These Ag NWs show a strong Raman enhancement effect for organic molecules on their surface.     

弱导光纤的标量衍射光束特性分析

仿照罗兰圆光学系统构造罗兰球光学系统 ,在罗兰球中简化电磁波的瑞利 索末菲标量衍射积分公式 ,推导出折射率阶跃分布的弱导光纤LP模衍射场分布和空间频谱的计算公式。提出LP0 1模远场衍射分布存在类似于平面波圆孔夫琅禾费衍射艾里斑的中央亮斑概念 ,并给出中央亮斑角半宽度的计算公式。     

^60Coγ射线对刚地弓形虫缓殖子感染性的影响

应用不同剂量的~(60)Coγ射线照射含NT株弓形虫包囊的鼠脑匀浆后,以0.4％胰蛋白酶液消化,使弓形虫缓殖子从包囊中释放出来,并用生理盐水作连续10倍稀释,使成为含不同数量缓殖子的悬液,将此悬液接种小鼠,用生物检测方法确定其感染性。另设未经照射处理的缓殖子悬液感染小鼠的对照组。结果表明,γ射线0.55kGy剂量为控制鼠脑中NT株弓形虫感染性的最小有效剂量。γ射线0.1kGy剂量对弓形虫缓殖子感染性无明显影响,而0.45kGy照射后,其感染性较前者下降了10~4倍。     

Evaporated Thin Films of CdS and CdTe: Optimization for Photovoltaic Applications

Thin films of cadmium sulphide and cadmium telluride have been prepared by thermal evaporation under various conditions of deposition. These films have been characterized optically. electrically and for structure determination. The results of these characterizations along with the initial results of all thin film CdS/CdTe solar cells are presented in this paper     

木犀科植物花粉的扫描电镜研究

植物花粉的形态特征具有种属特异性。本文用扫描电子显微镜观察了木犀科(Oleaceae)的六属八种植物花粉的形态特征。结果表明,除迎春有个别四萌发沟外,其它花粉都是三沟型,外壁纹饰均为网状。但各种植物花粉的细微形态仍有明显差异。因此,用扫描电镜观察研究植物花粉的亚微形态特征,可为植物分类提供一些必要的形态依据。     

构筑企业级信息系统安全体系

本文以跨地区公司为例,探讨企业级信息系统安全体系的构筑,所述的原则和做法可以实现在外部网-内部网-主机-用户体系上,形成多道防线,使企业计算机网络具有相当程度的安全性,从而达到企业信息系统的安全目标。     

ER流体特性及其研究现状

本文简要介绍了ER流体现象及其力学和电学性能,给出了描述ER流体行为的一般理论,提出了ER流体应用中目前存在的主要问题。     

GB 19865 & GB 6675 ANNEX A.A——SAFETY OF ELECTRICAL TOYS Differences Between the new and old Chinese National Standards

This article anlayzes the different requirements for electrical toys safety between GB 6675-2003 and GB19865-2005. This information is summed up in table form to make it easy for toy designers and manufacturers to grasp the new standard.     

A NEW METHOD FOR DETERMINATION OF FRACTURES OF METALS UNDER SEM

本文提出了一种在扫描电镜中应用体视学原理定量研究金属脆性断口的方法.利用这种方法,图象上的小晶面的晶向、成分及两点间距都可以测定.     

高炉用氮化硅结合碳化硅制品化学分析方法的研究

确定了高氧化铝含量（０．５％－２０％）的高炉用氮化硅结合碳化硅制品中Ｓｉ３Ｎ４、ＳｉＣ、ｆＳｉ、ＳｉＯ２、Ｆｅ２Ｏ３、Ａｌ２Ｏ３六种化学成分的化学分析方法试验条件．并按条件试验选择了分析方法，进行了精密度、准确度和实际工作的考核，证明了本分析方法可靠、切实可行，能满足科研工作和生产的要求。