药用植物白芍愈伤组织中产芍药双苷的研究(英文)

In order to facilitate the preparation of paeoniflorin (PF) and albiflorin (AF), two chief bioactive constituents in Paeonia lactiflora Pal (PL), induction and culture of callus from PL were studied. With a modified woody plant medium supplemented with 0.5 mg·L?1 6-benzylaminopurine, 1.0 mg·L?1 naphthylacetic acid, 0.1 mg·L?1 thidiazuron and 30 g·L?1 sucrose, callus was induced from four kinds of explants:leaf, stems, petiole, and root. The potency to form callus varies between different explants and leaf explants exhibits the highest capacity (100%). On the other hand, root-derived cal us (R-callus) produces the highest level of total amount of PF and AF, 31.8 mg·g?1 dry mass, which is higher than the corresponding level in the root of field cultivated PL. Further-more, the time needed is only 40 days, remarkably shorter than the cultivation time of PL, about 4–5 years. Higher accumulation levels of PF and AF with shorter production time indicate that cal us culture of PL is a promising powerful tool for production of PF and AF in the future.     

酿酒葡萄籽的化学成分及综合利用

本文就酿酒葡萄副产物葡萄籽的化学成分:油脂(亚油酸)、多酚物质(原花青素、单宁及白藜芦醇等)以及葡萄籽功效成分的提取与综合利用进行了综合评述.     

还原剂水合肼对LiNi0.5Mn1.5O4结构及性能的影响

在用二次干燥共沉淀法制备锂离子电池正极材料LiNi0.5Mn1.5O4的前驱体时,加入还原剂水合肼,对前驱体进行还原处理,进而对比还原处理与不加还原剂的样品在结构和电化学方面的区别。实验结果发现,还原处理的前驱体所制备的LiNi0.5Mn1.5O4的充放电比容量远高于不加还原剂的样品,而且还原处理的前驱体所制备的正极材料在高温条件下(55℃)电化学性能保持较好,50次充放电循环后容量保持率更高。X粉末衍射(XRD)和扫描电镜测试结果表明,用还原剂水合肼处理的前驱体所合成的样品具有较好的结晶度,晶粒呈规则的八面体形貌,杂质含量很少;而未处理的前驱体所合成的样品则含有少量的杂质,结晶度较差。研究结果表明,添加还原剂水合肼对所制备的LiNi0.5Mn1.5O4正极材料的结构和性能有较好的促进作用,对进一步的改性研究具有重要的指导意义。     

低温共熔盐法制备LiNi_(0.8)Co_(0.2)O_2的结构与电化学性能

低温共熔盐0.434LiNO3-0.266LiOH·H2O-0.3CH3COOLi·2H2O在80～90℃范围实现很好的熔融态。采用这种低温共熔盐制备出了锂离子电池正极材料LiNi0.8Co0.2O2,XRD检测显示材料结晶度高,具有规整的层状α-NaFeO2结构,SEM扫描显示样品形貌均一,颗粒大小均匀。充放电测试表明,材料具有良好的电化学性能,在2.8～4.3V电压范围0.2C首次放电比容量为174.1mAh/g,循环20次后容量保留95%。     

普洛迪药物主要成分及其结合形式的质谱分析

In order to explain the reason why the clinical effects of “Puluodi” are better than those of cerebroprotein hydrolysate and troxerutin injections used individually, the components of “Puluodi” were analysed by electrospray ionization mass spectrometry, liquid chromatography-mass spectrometry and cold-spray ionization mass spectrometry, as well as amino acid analysis. The existing state of the main components such as the interaction between amino acids and troxerutin was studied emphatically.