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以双(2,4,5-三氯-6-正丁烷氧羰基苯基)草酸酯(简称CPPO)和红色荧光剂罗丹明B组成的过氧草酸酯类化学发光体系为研究对象,从粒径、用量和种类的角度讨论了分散剂云母等对体系发光效率的影响.结果表明,添加30μm云母50mg后,体系的发光寿命、强度均显著增加,发光效率较高。 相似文献
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Study on Luminescence Properties and Crystal-Lattice Environment of Eu^2+ in Sr4-xMgxSi3O8Cl4:Eu^2+ Phosphor 总被引:1,自引:0,他引:1
According to the Van Uitert experimental equation, crystal-lattice environment of Eu^2 in the Sr4Si3O8C14 crystal was discussed. By adding Mg^2 to the host lattice, Sr4-xMgxSi3O8C14:Eu^2 was synthesized and the emission peak shifted from blue-green (488nm) to blue-violet (411nm) with the increase of amount of the magnesium which replaced the strontium. By analyzing the spectra of Sr4-xMgxSi3O8C14:Eu^2 the two Eu^2 emission centers were found because of the change of crystal-lattice environment in the host and the crystal structure was obtained by X-ray diffraction data. 相似文献
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钴-钛系列随角异色功能颜料的制备及性能研究 总被引:2,自引:0,他引:2
采用具有干涉色的云母钛作为基质材料,通过湿化学法制备随角异色功能颜料.用XRD、多角度色度仪、X-Rite MA-86Ⅱ5角度分光光度仪对颜料进行分析表征.考察实验条件对颜料随角异色效果的影响,分析了角度变化对颜料明度和颜色变化趋势的影响.结果表明,在具有干涉色的云母钛表面包覆氧化钴膜,能够制得变色效果较好的随角异色颜料,制备此种颜料的最佳反应条件是:反应温度70~80℃,pH9.5~10.5之间,加料速度2~3滴/min,煅烧温度900℃,煅烧时间60min,改变云母钛的干涉色可以制得多种颜色的随角异色颜料,随着观察角度的增加,颜料的明度增加,颜料呈现3种颜色变化. 相似文献
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通过使用离子交换法和水热法,简单制备了一系列不同含量的Co~(2+)和Ni~(2+)共掺杂锐钛矿型TiO_2纳米带.使用X射线衍射(XRD)、扫描电镜(SEM)、透射电镜(TEM)、X射线光电子能谱(XPS)、傅里叶红外(FTIR)和振动样品磁强计(VSM)等各种测试技术对这些样品进行了表征.结果表明,Co~(2+)和Ni~(2+)皆掺入TiO_2晶格中,没有发现任何钴或镍金属簇或金属纳米粒子存在,也未发现有它们的氧化物第二相存在.磁性测试结果证实,所有掺杂样品皆有室温铁磁性,但所表现的磁性行为很复杂,同时具有铁磁性和顺磁性. 相似文献
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The non-grinding long afterglow material SrAl2O4:Eu^2+ , Dy^3+ was prepared by combustion method in home mierowave oven direetly, after dispersant, frother, eomburent, and mineralizer were added into the reacting system. XRD analysis showed that the powders were nearly pure SrAl2O4 phase with few other phases, and the size of the grain was 41.1 nm. Fluoreseenee speetrum results indieated that there were 2 exeitation peaks loeated at 345 and 400 nm, and the emission peak loeated at 516 nm, afterglow lasted up to 30 min or more. The mierowave eombustion method has advantages of less time, low temperature and no grinding process, and the material made by the method has good luminescent property. 相似文献
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煤的芳烃化学研究进展 总被引:2,自引:0,他引:2
当世界上的石油资源逐渐枯竭之后,煤能否成为21世纪化学工业的原材料?科学家们正面临极富感染力的挑战,即寻找和发展一条利用液化煤中的芳烃化合物合成有机化学品的新途径。近期研究表明,新兴的煤化学工业具有很大的发展潜力。本文主要讨论和介绍煤的非燃料利用问题,研究发展由煤制取芳烃化学品和材料的可能途径。综述有关文献26篇。 相似文献