Pd-Ag-Sn-In-Zn合金时效强化机制研究

通过硬度测试、X射线衍射（XRD）分析、扫描电镜（SEM）观察研究了Pd-Ag-Sn-In-Zn合金时效强化行为及相关的微观结构变化，从而很好地解释了该合金的时效强化机制。结果表明，时效前期合金硬度的增加与在晶界处形成中间过渡相有关。通过扫描电镜观察，可以清楚地看到基体相以及等温时效过程中在晶界处有类似珠光体的析出相。随着稳定第二相的长大，硬度持续下降。     

基于SCE-UA算法新安江模型在沣河流域的应用

为了探索人工试错法和基于SCE-UA算法的自动优选法这两种方法在混合产流地区的拟合效果,选取新安江模型对半湿润半干旱地区陕西沣河流域进行参数优化。探讨基于SCE-UA算法的新安江模型在沣河流域的适用性,重点分析了参数的变化情况,发现两种方法模拟的次洪参数SM、CS变化较大。研究结果表明:基于SCEUA算法的新安江模型在沣河流域适用性较好,相对人工试错法参数取值更加合理,提高了优化速度与模拟精度,具有简便、高效的特点。     

Microstructure and mechanical properties of Nb-B bearing low carbon steel plate: Ultrafast cooling <Emphasis Type="Italic">versus</Emphasis> accelerated cooling

The microstructure and mechanical properties of low carbon bainite high strength steel plate were studied via different cooling paths at the pilot scale. There was a significant increase in mechanical properties, and notably, the yield strength, tensile strength, and toughness at -40 °C for the tested steel processed by ultra-fast cooling were 126 MPa, 98 MPa and 69 J, respectively, in relation to steel processed by accelerated cooling. The ultra-fast cooling rate not only refined the microstructure, precipitates, and martensiteaustenite (M/A) islands, but also contributed to the refinement of microstructure in thick plates. The large size M/A constituents formed at lower cooling rate experienced stress concentration and were potential sites for crack initiation, which led to deterioration of low-temperature impact toughness. In contrast, the acicular ferrite and lath bainite with high fraction of high-angle grain boundaries were formed in steel processed by ultra-fast cooling, which retarded cleavage crack propagation.     

基于性能预测的并行软件模块设计研究

并行计算软件库,如scalapack和plapack,通过提供大量并行计算子过程来提高并行计算软件开发效率。为方便用户使用并行软件库,该文提出了一种基于性能预测技术来开发并行计算软件库的方法,这是一种隐藏并行计算细节的有效途径。并就构成该软件库的神威超级计算机系统并行软件开发工具,并行线性代数软件库的数据自动分布的方法和供用户调用并行软件库的接口设计技术进行了讨论。实验结果表明,这种技术能有效提高并行计算软件效率。     

气敏元件电极引线Au-Pt合金材料

分析Au - 2 3 5Pt合金的显微组织 ,考查其物理力学化学特性 ,与纯Pt丝比较 ,表明可取代纯Pt丝作气敏元件的电极引线 ,有良好效益。     

总α和总β放射性测定方法研究

研究了各种常见核素α、β放射性在BH-1216低本底α、β测量仪上的计数效率与其射线能量之间的关系,以241Am和40K分别作为总α和总β的标准物质,计算了常见核素的总α和总β放射性计数效率E相对于标准物质计数效率Esd的等效因子ρ(ρ=E/Esd),用于比较已知核素活度浓度样品的总放射性估算值与测量值间的一致性。研究还发现,放射性活度与计数率的比值,即活度-计数率比K,与待测放射源的质量厚度之间存在良好的线性关系。用活度-计数率比代替计数效率作"效率校正",计算方便、精度较高。基于上述研究建立了适用于食品和环境样品中总α和总β放射性的测定方法。     

几种亚热带速生乡土阔叶树种的制浆特性评价

选择10种具有发展前景的速生阔叶树，通过材质材性和CMP制浆性能的测定分析，并结合造林学特性评价，筛选出适宜于南方山地大规模种植的闹叶树种。结果显示，马褂木和光皮桦是非常优异的纸浆阔叶木，其木材密度中等，纤维细长，综纤维素含量高而木质素含量低。马褂木和光皮桦CMP的裂断长和撕裂指数都明显高于马尾松TMP。通过综合评价，四川桤木、闽粤栲和翅荚木等可作为次等重要的纸浆阔叶树种来考虑，而木荷、枫香、乳源木莲和山杜英等因其木材密度偏大或木质素、抽出物含量偏高等固有缺陷不适宜作为纸浆树种发展。     

CuO含量对yCuO/CuxCe1-xOδ催化剂脱除痕量CO性能影响

采用柠檬酸络合-浸渍相结合的方法制备yCuO/CuxCe1-xOδ催化剂,通过XRD、BET、H2-TPR等手段研究了载体掺杂CuO含量（x值）、表面负载CuO含量（y值）对yCuO/CuxCe1-xOδ催化剂催化氧化CO性能的影响。结果表明,载体中掺杂的CuO能与CeO2产生协同作用,有利于负载的CuO在载体表面均匀分散,促进氧化-还原性能的提高,提升CO催化氧化活性。采用正交试验法,经DPS（Data Process System）软件对CuO含量进行逐步回归优化,优化得到16.40 %CuO/Cu0.05Ce0.95Oδ催化剂具有较优的催化氧化CO性能,该催化剂在50 ℃、3.0 MPa的工况条件下,可将液相丙烯中微量CO从1.0 × 10-5（φ,体积分数）降至3.0 × 10-8（φ）,达到聚合级烯烃对CO脱除深度的要求,连续反应1400 min,稳定性良好。     

Experimental assessment of textured tools with nano-lubricants in orthogonal cutting of titanium alloy

In this study, we investigated the effects of composite nano-Cu/WS₂ lubricating oil and single-point diamond indentation-textures on improving the cutting performance of YG8 cemented carbide tools, which is crucial for textures tool applications. The aims of the study were to improve wear resistance and reduce chip adhesion at the tool’s rake face in cutting of titanium alloys. Dot textures with different spacings were fabricated on the surface of YG8 cemented carbide tools through the single-point diamond indentation method, and composite nano-Cu/WS₂ lubricating oil was prepared. Orthogonal cutting tests were carried out under dry cutting and minimal quantity lubricated (MQL) conditions. Investigate the effect of different texture spacing on the cutting performance in the light of cutting forces, friction coefficient, the deformed chip thickness, tool adhesions, and chip morphology. The results show that the dot texture effectively improved the lubrication conditions in machining titanium alloys under the MQL conditions. The dot texture is effective at low speed in the dry cutting conditions. With the increase of cutting speed, the friction coefficient of dot texture tool is affected by texture spacing, and the friction coefficient of DT-200 tool is the smallest. In addition, composite nano Cu/WS₂ lubricating oil forms a lubricating film on the wear path by atomizing the lubricating oil and stores it in the dot texture, which enhances the anti-wear performance in the cutting process and reduces the cutting force and friction coefficient at the tool chip interface. By evaluating cutting force, friction coefficient, chip and tool morphology, it is concluded that DT-100 tool is more effective in improving lubrication conditions.

     

低度软锰矿制取硫酸锰的实验研究

以低度软锰矿为原料,采用还原焙烧—硫酸浸出法制取硫酸锰,研究了还原焙烧对浸出率的影响,及影响产品主含量达标的钙镁硫酸盐杂质的去除方法,探索出了3条工艺路线,可制得一水硫酸锰含量达98.5%以上的高品质硫酸锰产品。