A STUDY OF EXPERIMENTAL DESIGN OPTIMALITY FOR WIENER SYSTEMS

In the context of nonlinear dynamic system identification for Hammerstein systems, Rollins et al. (2003a) studied the information efficiency of the following two competing experimental design approaches: statistical design of experiments (SDOE) and pseudo-random sequences design (PRSD). The focus of this study is the Wiener system and evaluates SDOE against PRS under D-optimal efficiency. Three cases are evaluated and the results strongly support SDOE as the better approach.     

The effects of osmium tetroxide post‐fixation and drying steps on leafy liverwort ultrastructure study by scanning electron microscopy

Leafy liverwort is one of the most abundant and diverse plants in Indonesia. Their high variation and beneficial secondary metabolites contained in the oil bodies have attracted researchers' attention. The ultrastructural analysis of leafy liverworts is important as a means of species identification and also for further exploration of their oil bodies. However, the optimization of the preparation steps for observing leafy liverworts by SEM is necessary to avoid sample destruction. Fixation and drying play important roles in maintaining a sample's structure as close to its natural state as possible. Thus, in this study, we evaluated the effect of 4% Osmium tetroxide (OsO₄) and drying on leafy liverworts ultrastructure. Microlejeunea, Acrolejeunea, and Frullania were fixed with 2.5% glutaraldehyde. Some samples were then post‐fixed with 4% OsO₄, while the rest were directly dehydrated with an ethanol series and then subjected to different drying methods, i.e. air drying, freeze drying, and drying with hexamethyldisilazane (HMDS). According to the data obtained, post‐fixation with 4% OsO₄ could better maintain the integrity of the samples and enhance the contrast of leafy liverwort SEM images. In addition, samples dried with HMDS showed more detailed structures compared to those that were air dried. Different ultrastructure were found among the different leafy liverworts observed by SEM. Our data suggested the advantages of SEM in providing ultrastructure information on leafy liverworts as well as the optimum conditions to observe them with less deformation. OsO₄ post‐fixation could enhance the contrast of leafy liverwort SEM images and maintain the structure of the samples. Drying with HMDS provided a convenient way for rapid SEM preparation with less structural distortion.     

Glycerin‐Oxidation mit magnetisch abtrennbaren Nanokatalysatoren

Nanoparticle gold and gold‐platinum catalysts supported on magnetite particles were used in the aerobic glycerol oxidation. Transmission electron microscopy analysis confirmed an icosahedral morphology of the gold catalyst and a flower‐like structure for the gold‐platinum catalyst. Dynamic light scattering analysis confirmed a mean diameter of 30 nm for both catalysts. This particle size was relatively stable for more than one month. The catalysts were easily recoverable from the reaction medium by means of magnetic force. No metal leaching was observed and the successfully reused catalysts showed only slight alteration.     

A STUDY OF EXPERIMENTAL DESIGN OPTIMALITY FOR WIENER SYSTEMS

A weakly nonlinear theory of wave propagation in two superposed dielectric fluids streaming through porous media in the presence of vertical electric field and in the absence of surface charges at their interface is investigated in three dimensions. The method of multiple scales is used to obtain a dispersion relation for the linear problem and a Ginzburg-Landau equation with complex coefficients for the nonlinear problem, describing the behavior of the system. The stability of the system is discussed both analytically and numerically in both cases, and the corresponding stability conditions are obtained. It is found, in the linear case, that the stability criterion is independent of the medium permeability and that the medium porosity, surface tension, and dimension all have stabilizing effects the fluid viscosities, velocities, and depths have destabilizing effects, and the electric field has a dual role in the stability of the system. In the nonlinear analysis, it is found that the electric field has a stabilizing effect in two-dimensional disturbances and destabilizing effect in three-dimensional disturbances cases. The surface tension, fluid depths, and medium porosity have stabilizing effects in both two- and three-dimensional disturbance cases and the fluid viscosities, velocities, and medium permeability have destabilizing effects in both cases, and this stability or instability occurs faster for three-dimensional disturbance cases. It is found also that the system is unstable in the absence of fluid velocities or for nonporous media. Finally, the dimension was found to have a dual role (stabilizing as well as destabilizing) in the considered system, while it has a destabilizing effect in the case of nonporous media.     

Influence of Nanosilica Filler Content in LDPE Composites on Partial Discharge CharacteristicsEI北大核心CSCD

Partial discharges （PDs） due to artificial void in samples of LDPE nanocomposite sheet have been investiga- ted in this work. PDs may cause the degradation of insulating materials and may affect the lifetime of high-voltage ap- paratus. An experimental work using sphere ball-plane electrode system （CIGRE Method II） and a 1.0 mm LDPE composite sheet was carried out. Different weight percentages of nanosilica （0%, 2%, 4%, 6% and 8%） were used. PD experimental results, such as PD magnitude and PD number （both PD pulse polarities）, as functions of the ap- plied stress duration at a specified applied voltage were compared. The surface morphology of specimens was also presented and this conforms to the PD findings. The experimental results show that the PD characteristics of the LDPE generally improve with the introduction of nanosilica, the composite with the highest content of filler, namely the 8% （wt） nanosilica sample has the least partial discharge activities.