退火温度对冷轧态1235铝合金板材组织性能的影响

试验和讨论了退火处理对冷轧1235铝板的组织和力学性能的影响。确定了其再结晶温度范围。     

Fitting polynomial surfaces to triangular meshes with Voronoi squared distance minimization

This paper introduces Voronoi squared distance minimization (VSDM), an algorithm that fits a surface to an input mesh. VSDM minimizes an objective function that corresponds to a Voronoi-based approximation of the overall squared distance function between the surface and the input mesh (SDM). This objective function is a generalization of the one minimized by centroidal Voronoi tessellation, and can be minimized by a quasi-Newton solver. VSDM naturally adapts the orientation of the mesh elements to best approximate the input, without estimating any differential quantities. Therefore, it can be applied to triangle soups or surfaces with degenerate triangles, topological noise and sharp features. Applications of fitting quad meshes and polynomial surfaces to input triangular meshes are demonstrated.     

Electrochemical studies of bovine serum albumin immobilization onto the poly-o-phenylenediamine and carbon-coated nickel composite film and its interaction with papaverine

A biosensor based on bovine serum albumin (BSA) and poly-o-phenylenediamine (PoPD)/carbon-coated nickel (C-Ni) nanobiocomposite film modified electrode has been developed to study the interaction of BSA with papaverine (PAP). The well-dispersed C-Ni nanoparticles were dripped onto the glassy carbon electrode (GCE) surface firstly, and PoPD films were subsequently electropolymerized by cyclic voltammetry (CV) to prepare PoPD/C-Ni/GCE. Finally, the BSA was easily immobilized on the PoPD films via electrostatic adsorption. The morphology and the electrochemical properties of the fabricated composite electrodes were examined by scanning electron microscope (SEM) and electrochemical impedance spectroscopy (EIS), respectively. The interaction of PAP with BSA was monitored by differential pulse voltammetry (DPV), using PoPD as the electrochemical indicator. The binding constant (K), obtained by DPV, was 1.7 × 10⁴ L/mol, which was consistent with the fluorescence analysis. This constructed biosensor also exhibited a fine linear correlation with PAP concentration range of 2.5 × 10⁻⁹-4.5 × 10⁻⁵ mol/L and a detection limit of 8.3 × 10⁻¹⁰ mol/L was achieved by DPV.     

SHS法工艺参数对制备氮化硅粉体的影响

本文采用自蔓燃高温合成方法(Self-propagating High-temperature Synthesis)简称(SHS)合成氮化硅粉体,借助于XRD、SEM等检测方法,分析了自蔓燃高温合成氮化硅过程中氮气、温度、稀释剂与孔隙率等方面的影响。结果表明:只要最高燃烧温度不高于相应氮气压力下Si3N4的热分解温度,就可以用SHS方法合成Si3N4;氮气压力下硅粉的自蔓燃合成反应,必须要引入Si3N4稀释剂,来控制反应温度,以获得高α相含量的粉体。压坯气孔率控制在30%~70%,否则反应不能进行。研究发现SHS法可以制备纯度较高的氮化硅粉体。此法较传统方法合成的氮化硅设备简单,成本低廉,纯度高,填充性及烧结活性好。     

Tailored microstructure of zirconia and hafnia-based thermal barrier coatings with low thermal conductivity and high hemispherical reflectance by EB-PVD

Zirconia and hafnia based thermal barrier coating materials were produced by industrial prototype electron beam-physical vapor deposition (EB-PVD). Columnar microstructure of the thermal barrier coatings were modified with controlled microporosity and diffuse sub-interfaces resulting in lower thermal conductivity (20–30% depending up on microporosity volume fraction), higher thermal reflectance (15–20%) and more strain tolerance as compared with standard thermal barrier coatings (TBC). The novel processed coating systems were examined by various techniques including scanning electron microscopy (SEM), X-ray diffraction, thermal conductivity by laser technique, and hemispherical reflectance.     

Typoselectivity of Crude Geobacillus sp. T1 Lipase Fused with a Cellulose-Binding Domain and Its Use in the Synthesis of Structured Lipids

Typoselectivity of crude CBD-T1 lipase (Geobacillus sp. T1 lipase fused with a cellulose binding domain) was investigated. Multi-competitive reaction mixtures including a set of n-chain fatty acids (C8:0, C10:0, C12:0, C14:0, C18:1 n-9, C18:2 n-6 and C18:3 n-3) and tripalmitin-enriched triacylglycerols were studied in hexane. The crude CBD-T1 lipase discriminated strongly against C18:1 n-9 [competitive factor (α) = 0.23] and showed the highest preference for C8:0 (α = 1). Utilizing the catalytic properties of crude CBD-T1 lipase, acidolysis of soybean oil with C8:0 was selected as a model reaction to investigate the ability of the lipase to produce MLM-type (medium-long-medium) structured lipids. Several reaction parameters (added water amount, reaction temperature, substrate molar ratio and reaction time) examined for incorporating C8:0 into soybean oil, the optimum conditions were: 1:3 (soybean oil/C8:0) of molar ratio, 3 mL of hexane, 50 °C of temperature, 48 h of reaction time, 20 % of crude CBD-T1 lipase (w/w total substrates), and 7.5 % of water (w/w enzyme). Under these conditions, the incorporation of C8:0 was 29.6 mol%. The results suggest that crude CBD-T1 lipase, which showed different fatty acid specificity profiles, is a potential biocatalyst for the modification of fats and oils.     

创制杀菌剂啶菌恶唑生物活性及应用研究(Ⅰ)--番茄灰霉病

啶菌恶唑(试验代号:SYP-Z048)是一种结构新颖、作用方式独特的新型杀菌剂,具有保护、治疗效果及良好的内吸传导性。对子囊菌、担子菌和半知菌引起的多种植物病害具有良好的防治作用。啶菌恶唑对番茄灰霉病具有很高的离体杀菌活性和优异的田间防治效果。室内离体试验啶菌恶唑对番茄灰霉病(Botrytiscinerea )的EC50值为0.206 /ml;1998～2002年多点的田间小区试验结果表明:啶菌恶唑在处理剂量200～400 g a.i./hm2、施药2～3次、间隔期6～8d的条件下对番茄灰霉病有良好的防治效果,防效优于目前生产上推广使用的多菌灵、腐霉利、菌核净、嘧霉胺等常规杀菌剂。     

基于行为的移动协同感知模型研究

移动协同一般受到资源的限制和移动环境的干扰，影响协同工作的有效进行。基于行为（Activity）设计移动协同系统，以行为为中心构建系统，可以克服上述困难。其中，如何提供行为所围绕的感知信息是关键所在。文章提出了一个基于行为的移动协同感知模型，通过定义行动者实体、目标实体、行为阶段实体等一组感知实体对象及感知行为服务，来提供基于行为的感知信息，并在原型系统中进行了实现。模型提供了移动用户在协同工作行为中群组工作（Team Work）的所有感知要素，从而支持了用户有效完成协同工作。     

Fabrication and dynamic analysis of the electrostatically actuated MEMS variable capacitor

Future microwave networks require miniature high-performance tunable elements such as switches, inductors, and capacitors. In this paper, high performance variable capacitor was fabricated by simple microelectromechanical systems (MEMS) technology. The capacitance and quality (Q) factor at 1 GHz are 0.792 pF and 51.6. The pull-in voltage is 13.5 V and the tuning ratio of the capacitor is more than 1.31:1. A reduced-order model for the dynamic characteristics of the capacitor is established based on the equilibrium among the plate flexibility.     

Fast and Error-Bounded Space-Variant Bilateral Filtering

The traditional space-invariant isotropic kernel utilized by a bilateral filter (BF) frequently leads to blurry edges and gradient reversal artifacts due to the existence of a large amount of outliers in the local averaging window. However, the efficient and accurate estimation of space-variant kernels which adapt to image structures, and the fast realization of the corresponding space-variant bilateral filtering are challenging problems. To address these problems, we present a space-variant BF (SVBF), and its linear time and error-bounded acceleration method. First, we accurately estimate spacevariant anisotropic kernels that vary with image structures in linear time through structure tensor and minimum spanning tree. Second, we perform SVBF in linear time using two error-bounded approximation methods, namely, low-rank tensor approximation via higher-order singular value decomposition and exponential sum approximation. Therefore, the proposed SVBF can efficiently achieve good edge-preserving results. We validate the advantages of the proposed filter in applications including: image denoising, image enhancement, and image focus editing. Experimental results demonstrate that our fast and error-bounded SVBF is superior to state-of-the-art methods.