The effect of alkali metal oxide on the properties of borosilicate fireproof glass: Structure,thermal properties,viscosity, chemical stability

The purpose of the current work was to research the effect of alkali metal oxide on the structure, thermal properties, viscosity and chemical stability in the glass system (R₂O–CaO–B₂O₃–SiO₂) systematically. Because the glass would emulsify when Li₂O was added to the glass batch, this article did not discuss Li₂O. The results showed that when the amount of Na₂O was less than 4 mol.%, there was a higher interconnectivity of borate and silicate sub-networks in glass, as more mixed Si–O–B bonds were present in glass. The glass samples exhibited excellent thermal properties and chemical stabilities. As the amount of Na₂O exceeded 4 mol.%, the interconnectivity of borate and silicate sub-networks was weakened. The thermal properties and chemical stabilities of the glass samples were reduced. The connectivity of the silicate sub-network was weakened slightly as the Na/K ratio varied, and the coefficient of thermal expansion (CTE) of the glass samples gradually increased, and the resistance to thermal shock (RTS) value gradually decreased. Moreover, the viscosity of the glass samples decreased with the ratio of Na/Si and Na/K increased.     

Preparation and Characterization of a Chloroperoxidase-like Catalytic Antibody

The small molecule, meso-tetra(α,α,α,α-o-phenylacetamidophenyl) porphyrin (Mr1147.0) was used as complete antigen to elicit MAb through the immunization and cell fusion techniques. The MAb 1F2 obtained was demonstrated to be very pure by MALDI/TOFMS. The subtype of MAb 1F2 is IgG2a, which has a relative molecular weight of 156,678.8 Da.No significant change in the intensity of absorption peaks in UV and CD spectra was observed over a pH range between 6 and 12. The high stability of the abzyme and the tight binding between Fe porphyrin and antibody were also demonstrated. V_max, K_m, κcat, κcat/K_m for abzyme are 5.18 × 10⁻⁸ Ms⁻¹, 1.50 × 10⁻⁸ M, 0.518 s⁻¹, 3.45 × 10⁷ M⁻¹s⁻¹, respectively. The data obtained indicate that catalytic antibody has high catalytic activity. The chloroperoxidase activity of MAb 1F2-Fe porphyrin complex is stable from 10 °C to 60 °C.     

GPS失效时组合导航系统修正方法研究

针对采用低成本惯性元件的MEMS-IMU/GPS组合导航系统在GPS信号长时间失效后系统趋于发散的问题,在研究捷联航姿解算算法、加速计测量姿态角算法和磁传感器解算航向角算法的基础上,提出将航姿辅助修正算法引入组合导航系统中,一旦系统检测到无效信号出现,则能自动切换到辅助修正状态,使导航结果被抑制在0.5°左右;通过半实物仿真实验,证明了该方法能够有效解决GPS信号长时间失效后系统发散问题,满足了在低成本MEMS惯性元件基础上的高精度导航要求。     

Interfacial reaction during fabricating of full Cu3Sn joints in microelectronic packaging

Two copper substrates electroplated with Sn, both consisted of Cu/Sn?+?Sn/Cu structures, but they were bonded over different times in order to investigate the interfacial reaction. The growth morphologies of Cu₆Sn₅ and Cu₃Sn were analysed, respectively. The growth mechanisms for Cu₆Sn₅ and Cu₃Sn were investigated. The results show that the growth of Cu₆Sn₅ is primarily controlled by grain boundary-diffusion. However, the growth Cu₃Sn is controlled by the reaction of Cu-Cu₆Sn₅ at the beginning of the reaction, and then controlled by volume-diffusion as the thickness of the Cu₃Sn layer increases.     

日本持续照顾型养老社区的开发模式与实践

持续照顾型养老社区在养老机构中起着重要的作用。中国正在进一步加速老龄化且拥有超过1亿老年人口。本文将探讨日本持续照顾型养老社区相应的建筑设计层面和运营层面的经验及其在中国应用的可能。     

某型飞机航姿系统综合检查仪的研究与设计

简述了航姿系统综合检查仪的功能、工作原理以及整体设计方案;采用SDC/DSC模块来发送和接收同步器信号,解决了航姿系统中轴角转换的数字化问题,使检测仪的体积大大减小的同时提高了航姿系统检测精度;提出了小波去噪抗干扰技术,滤除了交流电源产生的噪声;应用改进的广义似然比法和Wald序惯概率比法（SPRT）实现了对系统软故障的检测;本检查仪精度高,操作简单,使用方便,满足机务维护的要求.     

液晶显示屏基板玻璃与盖板玻璃红外与拉曼光谱分析

基于液晶显示屏所用基板玻璃与盖板玻璃,以实验室熔制样品作为研究对象,通过傅里叶变换红外光谱(FTIR)与拉曼光谱对这两种玻璃进行了结构探索与对比分析.红外光谱表明,基板玻璃与盖板玻璃谱峰较为接近,中频区与高频区,基板玻璃的峰位处于更高的频率;而拉曼光谱结果表明,两种玻璃的Si-Onb非桥氧的存在形式均以Q2和Q3为主,且Q3比例大于Q2,而两种玻璃的Q0与Q1均很少,同时与红外光谱类似,基板玻璃在高频区的拉曼峰位比盖板玻璃处于更高的频率,且Q3/Q2值更高,表明基板玻璃网络结构中含有更高的桥氧比例,网络结构紧致度高于盖板玻璃.     

基于模糊滑模控制和两级滤波滑模观测器的PMSM改进控制策略

针对传统带有滑模观测器的永磁同步电机控制系统中转矩脉动大、抖振明显、反电动势估计精度差等问题,提出基于模糊滑模控制和两级滤波滑模观测器的PMSM改进控制策略.首先,在速度环提出基于双曲正弦函数的新型趋近率,结合模糊控制思想对趋近率参数实现自整定,设计了一种基于新型趋近率的模糊积分滑模速度环控制器,并且对新型趋近率的抖振抑制效果给出严格分析.其次,提出基于变截止频率低通滤波器和修正反电动势观测器的两级滤波结构,抑制反电动势中的高频分量和测量噪声,并对转子位置进行合理补偿,继而设计了两级滤波滑模观测器;通过Lyapunov判据对本文提出控制策略的稳定性进行了推导证明.仿真和实验结果表明,与传统滑模观测器相比,改进的控制器使电机在启动和受到外部扰动时系统响应良好,有效改善了转矩脉动、抖振、反电动势的估计精度等问题.     

非金属预弯开口减振结构响应特性及逆向设计

针对非金属减振结构动态响应特性易出现负刚度的现象,研究一种基于非金属材料的预弯开口减振结构。采用有限元法对该结构进行响应特性分析,明确各结构参数对减振结构响应状态的作用机理,并建立该减振结构响应特征曲线与各结构参数的关联关系,用实例验证此关联关系的准确性。结果表明：预弯开口减振结构的结构参数对其响应特性有较大影响,主截面尺寸变化主要影响特性曲线的接触变形期;预弯角大小主要影响特性曲线的平台期和接触变形期;开口尺寸大小影响特性曲线的平台期和接触变形期。具体体现在：预弯柱高度、开口高度和最短距离影响特征曲线中A点的上下变化,特征B点的上下左右变化;预弯柱宽影响特征曲线中A点的上下左右变化,特征B点的上下变化;预弯角影响特征曲线中A点和B点的上下左右变化;开口倒角影响特征B点的上下左右变化。所得成果可为该类型减振装置的优化设计提供新的参考。     

键合机引线框架夹持传送机构的设计与开发

在分析现有键合机引线框架传送机构的优缺点的基础上,根据整机设备的设计开发要求,利用伺服电机和气缸作为动力源的方式,研究开发了夹持传送机构,用于完成引线框架的夹持、松开、传送等动作,并成功地应用到整机设备开发中,满足了整机功能和性能的要求,目前该设备已投入实际生产运行.