Microstructure,wear and corrosion characteristics of multiple-reinforced (SiC–B4C–Al2O3) Al matrix composites produced by liquid metal infiltration

In this study, AA7075 aluminum matrix composites reinforced with the combination of SiC, Al₂O₃, and B₄C particles were fabricated by the liquid metal infiltration method. The effects of the relative ratio of B₄C and Al₂O₃ particles on the microstructural, wear, and corrosion features of the composite samples were analyzed using XRD, light metal microscopy, SEM, EDS, Brinell hardness, ball-on-disc type tribometer, and potentiodynamic polarization devices. It was determined that infiltration occurred more successfully, and homogenously distributed particles with reduced porosity were obtained as the amount of Al₂O₃ increased. Worn surface studies revealed that the specimens were predominantly worn by abrasion and adhesion. The increase in B₄C/Al₂O₃ ratio caused a decrease in the hardness and wear strength, whereas it increased the corrosion resistance.     

Antenna miniaturization for vehicular platforms using printed coupled lines emulating magnetic photonic crystals

A miniature printed antenna exploiting magnetic photonic crystal (MPC) modes is presented. The MPC mode is typically found in volumetric anisotropic materials and is realized here using a set of coupled printed transmission lines. The printed element is formed by a pair of unit cells, cascaded to realize a circularly periodic structure. To excite the nonreciprocal MPC mode, the coupled microstrip lines are printed on a uniform substrate with magnetic material inserts. A printed and slot (cavity-backed) version of the MPC-based element is designed and constructed. It is found that the cavity-backed version is better suited for reducing platform interactions, thus, avoiding detuning when installed on smaller platforms. Tunable magnetic biasing is also explored to improve functionality. The paper concludes by providing the in situ performance of the cavity-backed and recessed MPC antennas.     

Effect of Deep Cryogenic Treatment on Wear Resistance of AISI 52100 Bearing Steel

In this study, the effects of deep cryogenic treatment (DCT) on the wear resistance of AISI 52100 bearing steel were investigated. For this purpose, a number of bearing steel samples were held for different times (12, 24, 36, 48, 60 h) at deep cryogenic temperatures (?145 °C). The wear experiments were carried out in a ball–disk arrangement, by applying loads of 10 and 20 N and a sliding velocity of 0.15 m/s. After conducting the experimental studies, 36 h was found to be the optimal holding time. At this holding time, the wear rate and friction coefficient were decreased, while the hardness reached to maximum values. It was observed that DCT led to significant microstructural changes, which resulted in improved tribological properties.     

Compact Thermal Model for the Transient Temperature Prediction of a Water-Cooled Microchip Module in Low Carbon Emission Computing

This article presents a compact computational model for the rapid determination of the junction temperature of a chip cooled with a heat sink, exploring the concept of hot water cooled electronics as a strategy to reduce the carbon footprint of data centers. The model aims at rapid simulations of variations of the chip, as well as the heat sink outlet water temperatures during transient heat loads. The model is validated by experimental tests with a water-cooled manifold microchannel (MMC) heat sink, which is designed to cool the processors of state-of-the-art servers. The chip temperature is determined subject to periodic heat loads as large as 100 W with frequencies in the range from 1 to 10 Hz. The results show that to calculate 1 s of real temperature variation requires less than 20 s of computational time on a Quad-Core AMD Opteron 2350, 2 GHz desktop PC with 4 GB RAM. The thermal response of the heat sink to real-time power traces with durations up to 200 s is modeled for different flow rates. The simulations indicate that application of a flow-control feedback loop could achieve more than 50% reduction in water flow rate, without compromising the maximal chip temperatures.     

The performance of ceramic and cermet cutting tools for the machining of austempered ductile iron

In this study, the machinability of austempered ductile iron (ADI) having a ferritic structure was examined. For this purpose, three types of ductile iron materials (as cast, ADI-250, ADI-375) and two different types of cutting tool materials (ceramics and cermet) were used. To emphasize the role of austempering process, ductile iron (DI) specimens are first austenitized in salt bath at 900°C for 120 minutes after which they are quenched in salt bath at 250°C (ADI-250) and 375°C (ADI-375) for 120 min. Machining tests were carried out at various cutting speeds (100–500 m/min) under the constant depth of cut and feed rate. The performance of both ceramic and cermet tools were evaluated based on the workpiece surface roughness and flank wear. Wear conditions of the cutting tools were characterized by scanning electron microscope. The results point out that the lower austempering temperature results in increasing of the cutting forces, while better surface roughness is obtained. Additionally, the results indicate that the tool wear occurs mainly on the flank face. However, higher cutting speed results in chipping formation in cermet cutting tool.     

Fabrication and characterization of anisotropic dielectrics for low-loss microwave applications

New magneto-photonic assembly designs for high-gain antennas require dielectrics with a significant anisotropy and low loss at GHz frequencies. This paper describes an approach to fabricate such dielectrics from ceramic laminates. These laminates consist of two ceramics with largely different permittivities and low dielectric losses. Alternating layers of commercially available α-Al₂O₃ and Nd-doped BaTiO₃ were laminated using organic adhesives. Equivalent permittivity tensors and loss tangents were characterized using a resonant cavity-based approach, which was coupled with a finite-element method full-wave solver. Measured permittivity values were in good agreement with mean field predictions; a minimum loss tangent 1.1 × 10^?3 was obtained when using one-component epoxy (Loctite^®-3982) adhesive. Application of two-component epoxy (M-bond 610) adhesive results in a slightly higher loss but better mechanical properties and machinability. These laminates were used to demonstrate high gain in a prototype antenna with 6 misaligned anisotropic dielectric layers.     

tert-Butylhydroquinone as a spectroscopic probe for the superoxide radical scavenging activity assay of biological samples

As a more convenient and less costly alternative to electron spin resonance (ESR) and nonspecific nitroblue tetrazolium (NBT) and cytochrome c assays of superoxide radical (SR, O(2)(?-)) detection, a novel probe, tert-butylhydroquinone (TBHQ), is introduced for SR nonenzymatically generated in the phenazine methosulfate-β-nicotinamide adenine dinucleotide (PMS-NADH) system. SR attacks both TBHQ and SR scavengers incubated in solution for 30 min where scavengers compete with TBHQ for the O(2)(?-) produced. TBHQ, but not its O(2)(?-) oxidation product, tert-butyl-1,4-benzoquinone (TBBQ), is responsive to the CUPRAC (cupric reducing antioxidant capacity) spectrophotometric assay. The CUPRAC absorbance of the ethyl acetate extract of the incubation solution arising from the reduction of Cu(II)-neocuproine reagent by the remaining TBHQ was higher in the presence of O(2)(?-) scavengers (due to less conversion to TBBQ), the difference being correlated to the SR scavenging activity (SRSA) of the analytes. With the use of this reaction, a kinetic approach was adopted to assess the SRSA of amino acids, vitamins, and plasma and thiol antioxidants. This assay, applicable to small-molecule antioxidants and tissue homogenates, proved to be efficient for cysteine, uric acid, and bilirubin, for which the widely used NBT test is nonresponsive. Thus, conventional problems of NBT assay arising from formazan insolubility and direct reduction of NBT by tested scavengers were overcome.     

(2S,12Z)-2-Acetoxy-12-heptadecene: Major Sex Pheromone Component of Pistachio Twig Borer, Kermania pistaciella

The sex pheromone of the pistachio twig borer, Kermania pistaciella (Lepidoptera: Oinophilidae), one of the most important insect pests of pistachio, Pistacia vera, in Turkey and Iran, was identified. In gas chromatographic-electroantennographic detection (GC-EAD) and GC-mass spectrometric analyses of pheromone gland extracts of female K. pistaciella from Turkey, (2S,12Z)-2-acetoxy-12-heptadecene was identified as the major candidate pheromone component. In field experiments in Turkey, lures containing synthetic (2S,12Z)-2-acetoxy-12-heptadecene attracted large numbers of male moths. Its attractiveness was significantly reduced by the presence of the R-enantiomer or of either enantiomer of the corresponding alcohol. (2S,12Z)-2-Acetoxy-12-heptadecene is the first pheromone component identified in the Oinophilidae and the first secondary acetate pheromone component identified in the Lepidoptera. An erratum to this article can be found at     

Investigation of dual phase transformation of commercial low alloy steels: Effect of holding time at low inter-critical annealing temperatures

Dual phase steels are a class of steels characterized by a microstructure consisting of a soft ferrite matrix with hard martensite islands at the grain boundaries. The temperature in the dual phase (α + γ) region and the holding time are two important parameters in the intercritically annealing process. In this study, different grades of commercial low alloy steels have been heat treated to a constant annealing temperature by changing the holding time. It is observed that the effect of holding time is dependent on the steel composition. In this context, a microstructural examination has been carried out using optical, scanning electron microscope and electron probe micro-analysis and hardness values have been determined.