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1.
Synthesis of hydrous SnO2 and SnO2-coated TiO2 powders by the homogeneous precipitation method and their characterization 总被引:1,自引:0,他引:1
Hydrous SnO2 and SnO2-coated TiO2 powders were synthesized by the homogeneous precipitation method using urea and the products were characterized by X-ray diffraction, thermogravimetry, differential thermal analysis, scanning electron microscopy and energy- dispersive X-ray microanalysis. Electrical conductivities were measured with an impedance analyser. Hydrous SnO2 powder prepared under conditions without SO
4
2–
ions was a bulky product containing 75 wt% of water. The addition of SO
4
2–
ions to the solution changed bulky hydrous SnO2 to a dense product; approximately spherical particles were obtained with an average particle size of 0.14 ± 0.03 m. with 13.5 wt % of absorbed water. Antimony-doped hydrous SnO2 prepared under conditions with SO
4
2–
ions consisted of approximately spherical particles with an average particle size of 0.17 ± 0.04 m with 15.0 wt % of absorbed water. Hydrous SnO2-coated TiO2 powders with a good dispersion state and with various Sn/Ti ratios were prepared under conditions with SO
4
2–
ions. All the as-prepared coated powders were white, but the products doped with Sb3+ ions were turned to pale blue by heat treatment at 600° C for 1 h and their electrical conductivities increased by orders of about 3.0 in comparison with those of the other two. 相似文献
2.
Yoshihiro Kubota Yusuke Nishizaki Hisanori Ikeya Masami Saeki Tetsunari Hida Sachiko Kawazu Michitaka Yoshida Hidekazu Fujii Yoshihiro Sugi 《Microporous and mesoporous materials》2004,70(1-3):135-149
Two types of organic–inorganic hybrid base catalysts are prepared. Organic-functionalized molecular sieves (OFMSs), particularly “amine-immobilized porous silicates”, are designed based on common idea to immobilize catalytic active sites on silicate surface. Silicate–organic composite materials (SOCMs), such as “ordered porous silicate–quaternary ammonium composite materials”, are the precursors of ordered porous silicates obtained during the synthesis. Both the OFMS and the SOCM are used as the catalysts for Knoevenagel condensation. Among the OFMSs, there is clear tendency that the use of molecular sieve with larger pore volume and/or surface area gives the product in higher yield. Aminopropylsilyl (AP)-functionalized mesoporous silicates such as AP-MCM-41 gives the product in high yield under mild conditions. No loss of activity is observed after repeated use for three times. The SOCMs are also active for the same reaction. The precursors of the mesoporous silicates are more active than those of microporous silicates. This material can be repeatedly used without significant loss of activity. High activity is not due to the leached species. The active sites of the SOCM catalysts are considered to be SiO− moieties located on the pore-mouth. Activity of the SOCM increases when the reaction is carried out without solvent, whereas decrease in activity of the OFMS is observed in the solvent-free system. 相似文献
3.
Hui-suk Yun Haoshen Zhou Itaru Honma 《Journal of Inorganic and Organometallic Polymers and Materials》2006,16(2):169-173
Self-standing transparent submillimeter-thick (∼0.34 mm) mesoporous titania films were prepared using the evaporation-induced
self-assembly (EISA) of a triblock copolymer template and titanium tetraethoxide. Performing EISA at low temperature and low
humidity improved the transparency and continuity of the films. As synthesized films had a well-defined hexagonal mesostructure
and the existence of both amorphous titania and anatase nanocrystallites (2 nm) was confirmed. The films that were calcined
at 400°C were composed of anatase nanocrystallites (14–16 nm) and had a BET surface area of 90 m2 g−1 with 13-nm pores. The films were characterized using XRD, FE-SEM, TEM, and N2 adsorption–desorption measurements.
An erratum to this article can be found at 相似文献
4.
Miyahara Daiki Ueda Itaru Hayashi Yu-ichi Mizuki Takaaki Sone Hideaki 《International Journal of Information Security》2021,20(5):729-740
International Journal of Information Security - Card-based cryptography is an attractive and unconventional computation model; it provides secure computing methods using a deck of physical cards.... 相似文献
5.
K. Yoshida Y. Maeno S. Nishizaki S. Ikeda T. Fujita 《Journal of Low Temperature Physics》1996,105(5-6):1593-1598
We have investigated the normal-state conduction of superconducting Sr2RuO4 (Tc 1K), which is isostructural to La2–xSrxCuO4. The resistivity of single crystals shows a crossover at TM130K from 3D metallic conduction at lower temperatures to 2D one at higher temperatures. Concerning the temperature dependence of the out-of-plane resistivity, we present a systematic interpretation based on competition between the life time of the quasiparticles and the time for the quasiparticles to travel between the adjacent RuO2 planes. 相似文献
6.
Yoshihiro Sagisaka Itaru Ishibashi Tamotsu Nakamura Masahiro Sekizawa Yuh Sumioka Masahiro Kawano 《Journal of Materials Processing Technology》2012,212(9):1869-1874
The authors proposed double-layer-type environmentally friendly lubricants, which were composed of an undercoat, superior in adhering to a material, and an overcoat, superior in reducing the friction between the material and the die. The performance of these lubricants for cold forging was evaluated by the ring compression test, the combined forward rod-backward can extrusion-type friction test and the combined forward conical can-backward straight can extrusion-type friction test. The double-layer-type lubricants showed comparable friction characteristics and anti-pick-up properties to a conversion coating lubricant, when the film thickness and surface treatment before coating were improved. In a practical application by cold multistage forging, the double-layer-type lubricants showed a similar performance to a conversion coating lubricant. 相似文献
7.
Junying Liu Rui Zhang Itaru Osaka Sarada Mishra Anna E. Javier Detlef‐M. Smilgies Tomasz Kowalewski Richard D. McCullough 《Advanced functional materials》2009,19(21):3427-3434
New solution processable 4‐(2‐hexyldecan)‐4H‐bisthieno[2,3‐d:3′,2′‐b]pyrrole and 4,4′‐dialkyl‐2,2′‐bithiazole‐based copolymers (PBTzDTPs) are synthesized with excellent FET performance. These novel copolymers have considerable potential in printable electronics as they have high charge carrier mobilities, excellent air stability, good solution processibility, and no requirement for post‐deposition thermal annealing, all requirements for this field of application. The thin film transistors fabricated from PBTzDTPs achieve field effect mobilities as high as 0.14 cm2 V?1 s?1 with current on/off ratios up to 106 without thermal annealing. In addition, the devices exhibit stable performance in air, showing no significant degradation over 60 days. Moreover, the polymers described here provide an excellent example of the systems in which higher mobility performance does not require higher crystalline, long‐range ordered structures. Such a system appears to be particularly promising for rapid fabrication techniques, where kinetic conditions usually prevent the development of long‐range order. 相似文献
8.
9.
Tamotsu Nakamura Hiroyuki Saiki Naoki Ikeuchi Nkk Itaru Ishibashi 《Lubrication Science》1995,11(4):287-294
In the present paper, some solid lubricants were tested in backward extrusion friction tests with flat-headed punches using aluminium at room temperature. The results showed that anti-seizure ability was improved when wax was added to the solid lubricant samples. In addition, a water-based graphite lubricant and an ultrahigh molecular weight polyethylene (UHMW-PE) lubricant were tested using aluminium workpieces heated to 500°C. The lubricity of the UHMW-PE lubricant was found to be superior to that of the graphite lubricant. 相似文献
10.
Goto S Takahashi H Kawasaki S Kimura B Fujii T Nakatsuji M Watanabe I 《Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan》2004,45(1):25-28
To simplify the labor-intensive conventional routine testing of samples to detect Leuconostoc at a meat processing plant, we developed polymerase chain reaction (PCR) primers specific for Leuconostoc from 16S rRNA gene sequences. These primers did not detect other common lactic acid bacteria such as Lactobacillus plantarum, Lact. sake, Lact. fermentum, Lact. acidophilus and Weissella viridescens. PCR with this primer detected all Leuconostoc species tested (Leu. mesenteroides subsp. mesenteroides, Leu. pseudomesenteroides, Leu. carnosum, Leu. lactic, Leu. citreum, Leu. amelibiosum, Leu. gelidum), except for Leu. fallax, and no other lactic acid bacteria on agarose gel electrophoresis. The method could identify areas contaminated with Leuconostoc in a large-scale industrial meat processing plant. Of 69 samples analyzed, 34 were positive for Leuconostoc according to the conventional culture method (isolation of LAB producing dextran) and PCR, whereas 29 were negative according to both. Six samples were culture-negative but positive by PCR. No false negative results were generated by PCR. The method is rapid and simple, is useful for routinely monitoring areas contaminated with Leuconostoc in meat processing plants, and could help to prevent the spoilage of meat products. 相似文献