Physical and chemical characteristics of butterfat fractions obtained by crystallization from molten fat

Both summer and winter butterfats were fractionated using a laboratory procedure which was designed to simulate a commercial fractionation process. The process is based on a slow, controlled cooling of the melted fat, a short stabilization time at the fractionation temperature, and separation of the crystals from the liquid oil by vacuum filtration using a stainless steel perforated disc. Fractionation temperatures of 29, 26, 23 and 19 C for winter butterfat and 29 and 19 C for summer butterfat were used to obtain solid and liquid fractions at each temperature. Three replications at each temperature showed good reproducibility of results. The fractions were characterized by their fatty acid and triglyceride compositions, melting and crystallization behavior, iodine value, peroxide value and melting point. Presented at the AOCS meeting in Philadelphia in May 1985.     

Interfacial hybridization kinetics of oligonucleotides immobilized onto fused silica surfaces

Fused silica optical fibers have been used in an intrinsic mode optical configuration as biosensors for fluorescence based detection of hybridization of nucleic acids. In this work, the kinetics of hybridization of single-stranded oligonucleotides that were covalently immobilized were studied. The probe DNA was dT₂₀, and the target was Fluorescein-labeled non-complementary (dT₂₀) or complementary (dA₂₀) oligonucleotide. Chronofluorimetric monitoring of the adsorption and hybridization processes was used to investigate oligonucleotide films of different density, in different salt concentrations, at temperatures of 25 and 40 °C, with the concentration of the target DNA being 0.005–0.1 μM. Mathematical models based on first- and second-order Langmuir adsorption have been examined to describe both the adsorption and the hybridization processes. Experimental data were processed using the models, and the hybridization kinetics were calculated. Hybridization kinetics on these optical fiber DNA sensors was found to be up to three orders faster than results presented for a number of other experiments using different immobilization chemistries.     

Stress Heterogeneity Effect on the Strength of Silicon Nitride

The experiments reported in this paper demonstrate the causes of the failure of monolithic ceramics. The specimens are made of silicon nitride and tested at room temperature. The stress field within the specimen is different for each of four series of tests that have been conducted. Fractographic observations have also been made to identify the causes of the failures. A size effect analysis is performed.     

Production of fungal enzymes and proteins from high salt cheese wheys

A fermentation procedure using wheys from buffalo milk, sweet rennet and salted wheys containing up to 15% NaC1, and based on the selection of salt-tolerant fungal cultures for production of microbial proteins and some economically important enzymes, is described. Certain strains of Aspergillus flavus, A. niger, A. ochraceus and A. terreus gave yields of mycelium ranging between 1.5 and 30 g on a dry weight basis. Strong proteolytic activities were exhibited by A. ochraceus, A. flavus and, to a lesser extent, by A. niger in the presence of salt up to 10% as final concentration. Powerful milk-clotting activities were also detected in culture supernatants of A. flavus and A. ochraceus. Extracellular β-galactosidases were released in to the culture fluids of these fungal strains with variable activities, depending upon the salt content of the growth medium. The application of the procedure is discussed.     

A 90-nm Wideband Merged CMOS LNA and Mixer Exploiting Noise Cancellation

This paper describes the design and implementation of a wideband merged LNA and mixer chip covering the frequency range from 0.1 to 3.85 GHz using 90-nm CMOS technology. Its high level of integration as well as its low power consumption makes it suitable for the rapidly growing software defined radio RF receivers. The chip performance achieves S11 below -10 dB along the entire band and a minimum single side band noise figure of 8.4 dB at IF frequency of 70 MHz. Power conversion gain is measured to be 12.1 dB while the input referred 1 dB compression point is measured to be -12.8 dBm. The chip core consumes only 9.8 mW from a 1.2 V supply with a die area, including the pads, of 0.88 mm²     

Absorbing surface impedances of lossy layers in the finite difference time-domain method

In this paper the time-domain surface impedances of an homogeneous absorber layer, are given for the vertical and horizontal polarizations, or respectively for the electric field perpendicular or parallel to the incidence plane. It turns out that the application of the concept in finite difference time-domain (FDTD) in absorbing surface impedances boundary conditions, gives results in good agreement with analytical Fresnel reflection coefficients.     

Thermal induced transformations in glassy chalcogenides SixTe60−xAs30Ge10

Temperature-induced transformations are considered to be interesting characteristic properties of amorphous materials including the Si _x Te_60–x As₃₀Ge₁₀ system, withx=5, 10, 12 and 20. Density (), X-ray diffraction and differential thermal analysis (DTA) were used to characterize the compositions. DTA traces of each glass composition at different heating rates from 5 to 30° C min^–1 were obtained and interpreted. Fast and slow cooling cycles were used to determine the rate of structure formation. Cycling studies of materials show no memory effect but only ovonic switching action. The compositional dependence of the crystallization activation energy (E) and the coefficient of glass-forming tendency (K _gl) have been calculated. The thermal transition temperatures and associated changes in specific heat have been examined as a function of the Te/Si ratio by differential scanning calorimetry. It was found that andE increase linearly with increasing tellurium content, while the heat capacity (c _p) andK _gl, decrease with increasing tellurium content.E=1.54 eV andc _p=0.246 J g^–1 K^–1 forx=20 whileE=2.74eV andc _p=0.22 J g^–1 K^–1 forx=5.