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Böttger PH Flage-Larsen E Karlsen OB Finstad TG 《The Review of scientific instruments》2012,83(2):025101
A versatile apparatus to measure the cross-plane Seebeck coefficient and the resistivity of bulk samples shaped as disks or thin plates, over a temperature range of 300 K-620 K with possible extension to higher temperatures, is presented. It is constructed from readily available equipment and instrumentation with parts that are easily manufactured. The Seebeck coefficient is measured over an average region of the sample under steady-state conditions. The sample resistance is measured using a four-point alternating current method and scaled to room temperature measurements with known geometry to calculate resistivity. A variety of sample shapes are supported. Most importantly, the support of the thin disk geometry allows for the very same samples to be used in a laser flash instrument. The design allows for rough vacuum, high vacuum, or purging with inert gases in the sample chamber. Measurements on thermoelectric ZnSb and a Ni reference material are presented. 相似文献
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Saccharomyces cerevisiae, Candida krusei, C. tropicalis, Geotrichum candidum, G. fermentans and Rhodotorula graminis were isolated during the fermentation of maize for ogi production. All the isolates except Geotrichum fermentans and Rhodotorula graminis were able to degrade phytate. All the yeasts strains exhibited lipase and esterase activities. Only S. cerevisiae (2.60%) and C. krusei (7.41%) exhibited amylase activities. Candida sp. produced wider zone of inhibition than the other yeasts strains tested during lipase activity while S. cerevisiae strains produced significantly wider zone of clearing as compared to the other yeasts for esterase activities. The study of inter-relationships between Lactobacillus plantarum and yeasts (C. krusei and S. cerevisiae) showed that the growth of the yeast strains were enhanced during fermentation by the presence of the lactic acid bacteria, but the growth of the L. plantarum strain was significantly enhanced especially by the C. krusei. 相似文献
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苏联动力工程的最新发展以及自动化在发电厂和变电站的应用,迫切需要有一种能够在帶負載情况下进行多次分合操作时(特別是在开断短路电流时)工作稳定并可以長期不需檢修触头的电器。 电器是否可以不需檢修触头而長期运行首先与制造該电器的触头材料有关。 大家知道,触头和接触联接因电器以及触头本身的工作条件,磨損特性及結構形狀等不同而有所区别。在高压电器中所采用的触头和接触联接主要可分为以下兩类: 相似文献
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The effects of dietary deficiencies of zinc and essential fatty acids (EFAs) or both on aspartate aminotransferase (AST) and alanine aminotransferase (ALT) were investigated in young growing rats. Four groups of albino rats were fed diets deficient in either EFA (4% hydrogenated coconut oil) or zinc (6 ppm) or both. The control diet was adequate in EFA (4% soybean oil) and zinc (100 ppm). The feeding trial lasted eight weeks and the activities of AST and ALT were determined in the liver and serum. EFA deficiency had no significant (p > 0.05) effect on liver AST. However, zinc and the double deficiencies depressed AST activity in the organ. Deficiencies of EFA, zinc and their combination depressed ALT activity in the liver significantly (p < 0.05) with a concomitant increase recorded in the serum. The data suggested alteration in endothelial permeability of the plasma membrane and thus leakage of membrane constituents in the tissue studied. It is therefore considered that these deficient diets may affect liver tissue negatively in view of the role of these enzymes in amino acid metabolism. 相似文献
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The optical constants of water ice have been determined in the near infrared from 4000 to 7000 cm(-1). Polycrystalline ice films with thickness as great as ~1164 mum were formed by condensation of water vapor on a cold silicon substrate at temperatures of 166, 176, 186, and 196 K. The transmission of light through the ice films was measured during their growth from 0 to 1164 mum over the frequency range of approximately 500-7000 cm(-1). The optical constants were extracted by means of simultaneously fitting the calculated transmission spectra of films of varying thickness to their respective measured transmission spectra with an iterative Kramers-Kronig technique. Equations are presented to account for reflection losses at the interfaces when the sample is held in a cell. These equations are used to reanalyze the transmission spectrum of water ice (358-mum sample at 247 K) recorded by Ockman in 1957 [Philos. Mag. Suppl. 7, 199 (1958)]. Our imaginary indices for water ice are compared with those of Gosse et al. [Appl. Opt. 34, 6582 (1995)], Kou et al. [Appl. Opt. 32, 3531 (1993)], Grundy and Schmitt [J. Geophys. Res. 103, 25809 (1998)], and Warren [Appl. Opt. 23, 1206 (1984)], and with the new indices from Ockman's spectrum. The temperature dependence in the imaginary index of refraction observed by us between 166 and 196 K and that between our data at 196 K and the data of Gosse et al. at 250 K are compared with that predicted by the model of Grundy and Schmitt. On the basis of this comparison a linear interpolation of the imaginary indices of refraction between 196 and 250 K is proposed. We believe that the accuracy of this interpolation is better than 20%. 相似文献
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Authenticity and traceability have been two of the most important issues in the food chain. Authenticity in particular, is closely related with both food quality and safety issues. Vegetables stand for a category of foods heavily affected by adulteration either in terms of geographic origin (national or international level) or production methods (organic or conventional production, fertilizers, pesticides, genetically modified vegetables). This review aims at addressing most of the currently applied methods for ensuring quality control of vegetables; a) instrumental: ion chromatography, high pressure liquid chromatography, atomic absorption spectrophotometry, electronic nose and mass spectroscopy and b) sensory analysis. The results of all the above mentioned methods were analyzed by means of multivariate analysis (principal component analysis, discriminant analysis, cluster analysis, canonical analysis, and factor analysis). All ensuing results and conclusions are summarized in eight comprehensive tables. 相似文献
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