Removal of imidacloprid and acetamiprid from tea infusions by microfiltration membrane

Removal of imidacloprid and acetamiprid in tea infusions by microfiltration membrane using dead‐end model was investigated in the present study. The results showed that microfiltration significantly promoted the removal of both pesticides (P < 0.05) in tea infusions. Furthermore, the extent of removal was strongly influenced by the pore size of membrane, operational pressure and the concentrations of tea infusions. The initial concentration of imidacloprid and acetamiprid showed no significant effect on their removal rates. The maximum removal rates were 79.7% for imidacloprid and 81.9% acetamiprid. The changes in major chemical components of tea infusions after microfiltration were evaluated. The results indicated that microfiltration caused no considerable changes in total polyphenols and total free amino acids, and small but statistically significant losses (6.3–18.0%) of eight catechins and three methylxanthines when filtration volume reached to 200 mL. The present study validated the application of microfiltration as a potentially feasible and promising method for the removal of imidacloprid and acetamiprid residues from tea infusions.     

基于状态空间法的电动机故障诊断和识别

电动机的初期故障信号一般较弱,不易辨别,而状态空间法在小信号的处理中灵敏度很高。为达到对电动机故障的诊断和识别,试图把状态空间法应用到对电动机的故障诊断中,先通过推导,从数学理论层面分析了状态空间法对于电动机故障信号的可辨别性,再使用Matlab软件搭建状态空间的辨别模型,把实验台测试的三组数据导入到模型中进行测试。测试的结果有力地证明了此方法的可行性,并能克服快速傅里叶变换(FFT)中数据采集量较大、分辨率不高的缺点。     

Effect of Fog and Clouds on the Image Quality in Millimeter Communications

The effect of fog and clouds in millimeter communication is discussed, and the attenuation caused by fog and clouds is reviewed. Signal-to-noise ratio (SNR) of image is derived using relating models of fog and clouds attenuation. According to the relation of image quality and its signal-to-noise ratio, the system behavior is forecasted theoretically. It is shown that the signal-to-noise ratio of receiver at certain transmitter power is inverse with radio wave frequency, from about 70dB at 10GHz to 48dB for fog and 49dB for clouds. The image quality of received signal at certain transmitter power is inverse with radio wave frequency, from about 7 grade at 10GHz to 5.27 grade for fog and 5.37 grade for clouds. The above calculated results are consistent with experimental results.     

A model for evaluation and administration of security inobject-oriented databases

The integration of object-oriented programming concepts with databases is one of the most significant advances in the evolution of database systems. Many aspects of such a combination have been studied, but there are few models to provide security for this richly structured information. We develop an authorization model for object-oriented databases. This model consists of a set of policies, a structure for authorization rules, and algorithms to evaluate access requests against the authorization rules. User access policies are based on the concept of inherited authorization applied along the class structure hierarchy. We propose also a set of administrative policies that allow the control of user access and its decentralization. Finally, we study the effect of class structuring changes on authorization     

低渗透油藏生产井关井测压时间的计算与应用

低渗透油藏的生产井压裂后，在单井试油试采过程中，压力恢复测试关井时间不同，其中有些井压力恢复曲线不能出现边界反应段，渗流不能反映地层中真实流动特征。针对这种情况，基于长庆绥靖油田塞39井区长：低渗透油藏大量试井和实际生产资料，利用现代试井解释理论，研究合理关井时间的界限及其计算方法。结果表明，当油井关井测压时间达到3倍地层径向流开始出现的时间后，利用此时的压力数据解释地层参数和地层压力，其结果的误差小于5％，同时能较准确地判断边界类型。计算的理论曲线和霍纳法解释值非常接近，对于塞39井区，若预先知道某生产井地层有效渗透率值，可从理论曲线查出压力恢复试井的关井时间，否则，建议按照该井区地层有效渗透率（大约在6mD左右），将不稳定试井测试时间控制在25d以上为宜。图4表3参14     

Effects of multiple weak interactions on the binding of phenolic compounds by polymeric adsorbents

To investigate the effects of multiple weak interactions on the binding of phenolic compounds by polymeric adsorbents, macroporous polystyrene (PS) resin and PS‐based adsorbents with different hydrogen‐bond acceptor atoms (PS CH₂( OCH₂CH₂)_n OCH₃, n = 0, 1, 2, and 3, denoted as PS‐EG₀, PS‐EG₁, PS‐EG₂, and PS‐EG₃) were prepared. The phenol adsorption strength order on these adsorbents was PS/PS‐EG₀ < PS‐EG₁ < PS‐EG₂ < PS‐EG₃, indicating that the adsorption on PS and PS‐EG₀ was driven by hydrophobic and π–π interactions, and the adsorption on PS‐EG₁, PS‐EG₂, and PS‐EG₃ was driven by a hydrogen bond in addition to hydrophobic and π–π interactions. PS‐EG₂ may adsorb a second phenol molecule on each binding site and PS‐EG₃ may adsorb second and third ones. The adsorption strength of resorcinol increased in the order of PS, PS‐EG₁, and PS‐EG₂, indicating that the adsorption was driven by 0, 1, and 2 hydrogen bonds in addition to hydrophobic and π–π interactions. Similarly, the adsorption of phloroglucinol on PS, PS‐EG₁, PS‐EG₂, and PS‐EG₃ was driven by 0, 1, 2, and 3 hydrogen bonds in addition to hydrophobic and π–π interactions because the adsorption strength increased in this order. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 4652–4658, 2006     

Computation of Microwave Attenuation on Coplanar Waveguide with Conformal ADI-FDTD Method

A novel Conformal Finite-Difference Time-Domain based on Alternating-Direction Implicit Method(ADI-CFDTD) used to calculate the microwave attenuation on coplanar waveguide(CPW) with complicated cross-section up to 200GHz is presented. This ADI-CFDTD algorithm is the combination of conformal algorithm dealing with the deformed cell with ADI-FDTD, and has unconditionally stable. The difference equations are derived from the Faraday's and Ampere's law. To validate its accuracy and efficiency, as an example, a CPW fabricated on lithium niobate is proposed. Numerical results demonstrate that this new ADI-CFDTD algorithm has more accuracy than that of quasi-static and CFDTD and shows good agreement with experiment data. When frequency is up to millimeter wave band the radiation loss is not negligible in total power loss.     

Study on the Intelligent System of Gear Pitch Deviation Measurement and Analysis

The intelligent controlling and data process of pitch error measurement is proposed. The whole system takes C++ as the development tool and takes advantages of object-oriented and visualization, having the advantages of easy operation and humanistic interface. In the meanwhile, the system can be complemented and improved according to the demand of user, having certain independence. The research of the system provides an efficient and reliable way to measure and analyze the gear pitch, which can be referenced in the future research.     

Transient aspects of inner wall temperatures at different spatial positions in fluidized bed evaporators

In this work, the instantaneous data of inner wall temperatures obtained at given axial positions but for different heated tubes or at various axial positions but at the same heated tube in a tube-bank fluidized bed evaporator with a vapor–liquid–solid external natural circulation flow were analyzed by employing linear and nonlinear time series analysis methods, including correlation dimension and Kolmogorov entropy analyses besides time domain, power spectrum and autocorrelation analyses. It is found that nonlinear characteristics of the wall temperature time series vary with spatial position in the evaporator at given operation conditions, and thus the multi-phase flow boiling behavior. However, the signals obtained at given axial position but different heated tubes in the evaporator exhibit more similar nonlinear evolution behavior, and those measured in the same heated tube but at different axial heights in the evaporator undergo more distinct nonlinear dynamic behavior. Multi-scale phenomena in different spatial positions are also found and discussed. These transient aspects of inner wall temperatures are closely related to the average holdup of solid particles and motion of vapor bubbles in vapor–liquid–solid flow. These results can provide some valuable information on the system modeling and controlling from the point of view of nonlinearity.