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O Prez‐Camacho S Sepúlveda‐Guzmn M Prez‐lvarez M García‐Zamora G Cadenas‐Pliego 《Polymer International》2005,54(12):1626-1631
New functionalized styrene–maleimide copolymers were prepared by free radical copolymerization of styrene (St) and N‐4‐carboxybutylmaleimide (NBMI) in chloroform, using 2,2′‐azobisisobutyronitrile (AIBN) as initiator. Monomer and copolymer characterization was carried out by 1H‐ and 13C‐NMR. Copolymer composition was determined by elemental analysis and Fourier‐transform infrared (FTIR) spectroscopy. The glass transition temperature (from DSC) and the thermogravimetric analysis (TGA) of the copolymers were consistent with the thermal behavior and stability observed for alternating St–maleimide copolymers. St–NBMI copolymers crosslinked with divinylbenzene (DVB) were also synthesized and their cation exchange properties evaluated in order to assess the capacity of the new copolymers to bind metallic ions. Copyright © 2005 Society of Chemical Industry 相似文献
3.
Antonio J. Jara Pablo Lopez David Fernandez Jose F. Castillo Miguel A. Zamora Antonio F. Skarmeta 《Personal and Ubiquitous Computing》2014,18(2):323-338
The application of Internet-enabled devices in the real world for the development of Smart Cities, environmental monitoring, bus tracking, and parking requires scalability, extensibility, and integration of emerging resources to reach a suitable ecosystem for data acquisition and interaction with citizens. Internet of things needs to offer efficient support for global communications and access to services and information. It needs to enable homogeneous and seamless machine-to-machine communication for different solutions and applications. This work presents an homogeneous and suitable mechanism for global resource discovery, device access for deployed smart objects in different scenarios, and sensors and devices from end users (participative sensing). The integration of legacy and sensors already available from smart buildings and smart objects is presented. For this purpose, a resolution infrastructure called “digcovery” is defined for maximizing efficiency and sustainability of deployments. Digcovery architecture offers the framework to allow users to register/include their own sensors into a common infrastructure and access/discover the available resources through mobile digcovery. Mobile digcovery exploits the context-awareness, geo-location, and identification technologies available in mobile platforms such as smartphones to discover, interact, and access the resources through its ElasticSearch engine. 相似文献
4.
Rosario?Zamora Gemma?Gómez Francisco?J.?HidalgoEmail author 《Journal of the American Oil Chemists' Society》2002,79(3):267-272
13C NMR spectra of oil fractions obtained chromatographically from 109 vegetable oils were obtained and analyzed to evaluate
the potential use of those fractions in the classification of vegetable oils and to compare the results with the NMR analysis
of complete oils. The oils included the following: virgin olive oils from different cultivars and regions of Europe and north
Africa; “lampante” olive, refined olive, refined olive pomace, hazelnut, rapeseed, high-oleic sunflower, corn, grapeseed,
soybean, and sunflower oils; and mixtures of virgin olive oils from different geographical origins. Oils were divided into
two sets of samples. The training set (98 samples) was employed to select the variables that resulted in significant discrimination
among the different oil classes. By using stepwise discriminant analysis, more than 98% of correct validated assignments were
obtained; these results were confirmed when applied to the test set (11 blind samples). Results suggest that the use of oil
fractions considerably increases the discriminating power of NMR in the analysis of vegetable oils. 相似文献
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Antonio J. Jara Miguel A. Zamora Antonio F. G. Skarmeta 《Personal and Ubiquitous Computing》2011,15(4):431-440
Diabetes therapy management in AAL environments, such as old people and diabetes patients homes, is a very difficult task
since many factors affect a patient’s blood sugar levels. Factors such as illness, treatments, physical and psychological
stress, physical activity, drugs, intravenous fluids and change in the meal plan cause unpredictable and potentially dangerous
fluctuations in blood sugar levels. Right now, operations related to dosage are based on insulin infusion protocol boards,
which are provided by physicians to the patients. These boards are not considering very influential factors such as glycemic
index from the diet, consequently patients need to estimate the dosage leading to dose error, which culminates in hyperglycemia
and hypoglycemia episode. Therefore, right insulin infusion calculation needs to be supported by the next generation of personal-care
devices. For this reason, a personal device has been developed to assist and consider more factors in the insulin therapy
dosage calculation. The proposed solution is based on Internet of things in order to, on the one hand, support a patient’s
profile management architecture based on personal RFID cards and, on the other hand, provide global connectivity between the
developed patient’s personal device based on 6LoWPAN, nurses/physicians desktop application to manage personal health cards,
glycemic index information system, and patient’s web portal. This solution has been evaluated by a multidisciplinary group
formed by patients, physicians, and nurses. 相似文献
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Diego Rocha-Parra Luciana León Bianchi Fernando Gentico David Garcia-Burgos María C. Zamora 《International Journal of Food Science & Technology》2021,56(8):3876-3884
The aim of the present study was to compare the information provided by a discrete and continuous data analysis of two emotions (disgust and joy), elicited by bitter-tasting beverages (coffee, yerba mate infusion and grapefruit juice) in two groups with different body mass index (BMI): overweight group (25 < BMI < 30), and healthy-weight control group (18.5 < BMI ≤ 25). Participants (n = 66; 34 females, 32 males) evaluated a total of three consecutive sips of the same beverage (taking one sip every 20 s and registering a continuous video for 60 s). The Wilcoxon test (continuous analysis) showed some changes generated as the drinks were being consumed. The biggest difference was the expression of disgust for coffee in the high BMI group, at the first sip (0–10 s). It represented 27% compared to 2% in normal BMI. The continuous analysis allowed to observe the periods where the differences were greater (0–10 and 40–50 s). 相似文献
9.
This work reports the study of four different carbon materials for their application as carbon material in microporous layers for high temperature proton exchange membrane fuel cells electrodes. The microporous layers were prepared with carbon black (a commercial one, Vulcan XC72), two different carbon nanofibers, CNF, (Ribbon and Platelet structure) and carbon nanospheres, all of them prepared in our lab. The microporous layers were characterized by XRD. The hydrophobicity, electrical conductivity, and permeability to different gases were also evaluated. The stability is an important issue to be overcome in the field of proton exchange membrane fuel cells. Thus, accelerated thermal and electrochemical degradation tests in phosphoric acid media were carried out to evaluate the stability of the different advanced materials tested under the same conditions. From all the performed essays, the carbon nanospheres were the best nano‐carbon materials because of the lower degradation degree shown by the microporous layer prepared with them and the good conductivity and permeability achieved, whereas CNF with a Platelet structure showed a low electrochemical stability due to their greater edge plane exposure which favors their corrosion. 相似文献
10.
Florence Bonnet-Magnaval Leïla Halidou Diallo Valrie Brunchault Nathalie Laugero Florent Morfoisse Florian David Emilie Roussel Manon Nougue Audrey Zamora Emmanuelle Marchaud Florence Tatin Anne-Catherine Prats Barbara Garmy-Susini Luc DesGroseillers Eric Lacazette 《International journal of molecular sciences》2022,23(1)