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1.
Habibeh Haddad Dabaghi Abdolmajid Bayandori Moghaddam Mahmood Kazemzad Rassoul Dinarvand Fezze Aryanasab Mohammad Reza Nabid 《Journal of Applied Electrochemistry》2008,38(3):409-413
Electrochemical treatment processes can significantly contribute to the protection of the environment through the minimization
of waste and toxic materials in effluents. From a pharmaceutical point of view and due to the existing resemblance between
the electrochemical and biological reactions, it can be assumed that the oxidation mechanisms on the electrode and in the
body share similar principles. In this paper, the application of electrochemical studies in the design of an environmentally
friendly method was delineated for the new hydrocaffeic acid (HCA, 3,4-dihydroxy hydrocinnamic acid) derivatives synthesis
at carbon electrodes in an undivided cell. In this cell, the EC mechanism reaction was involved, comprising two steps alternatively;
(1) electrochemical oxidation and (2) chemical reaction. In particular, the electro-organic reactions of HCA, an important
biological molecule, were studied in a water–acetonitrile (90:10 v/v) mixture in the presence of benzenesulfinic acid (3) and p-toluenesulfinic acid (4). The research included the use of a variety of experimental techniques, such as cyclic voltammetry, controlled-potential
electrolysis and product spectroscopic identification. 相似文献
2.
Khalid Mahmood Zia Mehdi Barikani Ijaz Ahmad Bhatti Mohammad Zuber Haq Nawaz Bhatti 《应用聚合物科学杂志》2008,109(3):1840-1849
A series of polyurethane (PU) elastomers was prepared by the reaction of poly(?‐caprolactone) and 4,4′‐diphenylmethane diisocyanate, which was extended with a series of chain extenders (CEs) having 2–10 methylene units in their structure. The completion of the reaction was confirmed by Fourier transform infrared spectroscopy. The chemical structures of the synthesized PU samples were characterized with Fourier transform infrared, 1H‐NMR, and 13C‐NMR spectroscopy, and the thermal properties were determined by thermogravimetric analysis, DSC, and dynamic mechanical thermal analysis techniques. The mechanical properties were also studied and are discussed. The thermogravimetric analysis and DSC analysis showed that CE length had a considerable effect on the thermal properties of the prepared samples. The dynamic mechanical thermal analysis and damping peaks were also affected by the number of methylene units in the CE length. The elastomer extended with 1,2‐ethane diol exhibited optimum thermal properties, whereas the elastomer based on 1,10‐decane diol displayed the worst thermal properties. Tensile strength and elongation at break decreased with increasing CE length, whereas hardness showed the opposite trend. The glass‐transition temperature moved toward lower temperatures with increasing CE length. The decrease in the glass‐transition temperature and tensile properties were interpreted in terms of decreasing hard segments and increasing chain flexibility. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
3.
We analyze nonlinear coupling of polarized solitons in the presence of initial frequency chirp on the basis of a theoretical model described by a coupled nonlinear Schrödinger equations. We also obtain a threshold condition for the bound state of two polarizations and show analytically that the threshold amplitude for soliton trapping can be controlled by varying the chirp parameter. 相似文献
4.
5.
On the free convection boundary layer on a vertical plate with prescribed surface heat flux 总被引:1,自引:0,他引:1
The free convection boundary layer on a vertical plate with a prescribed surface heat flux proportional to (1 +x
2)µ (µ a constant) is discussed. For µ > –12 the boundary-layer solution develops from a similarity solution valid forx small to the one valid forx large. However, with µ –12 the similarity equations forx large are not solvable and the behaviour for largex in this case is discussed. It is found that there are two cases to consider, namely µ < –12 and µ = –12. In both cases the leading-order problem is homogeneous involving an arbitrary constant which is determined from an integral property of the full boundary-layer problem. However, in the former case the asymptotic behaviour is algebraic, with the perturbation to the leading-order solution, arising from the heat flux boundary condition, being ofO[x
1+2µ]. The latter case also involves logarithmic terms, with the perturbation to be leading-order solution now being ofO[(logx)–1]. 相似文献
6.
Asim Muhammad Nabeel Ghani Muhammad Usman Ibrahim Muhammad Ali Mahmood Waqar Dengel Andreas Ahmed Sheraz 《Neural computing & applications》2021,33(11):5437-5469
Neural Computing and Applications - In order to provide benchmark performance for Urdu text document classification, the contribution of this paper is manifold. First, it provides a publicly... 相似文献
7.
Abbas Waseem Khan Muhammad Fakhir Taj Murtaza Mahmood Arif 《Neural computing & applications》2021,33(19):12921-12938
Neural Computing and Applications - Autonomous driving research is an emerging area in the machine learning domain. Most existing methods perform single-task learning, while multi-task learning... 相似文献
8.
Modeling guided wave propagation with application to the long-range defect detection in railroad tracks 总被引:2,自引:0,他引:2
Ivan Bartoli Francesco Lanza di Scalea Mahmood Fateh Erasmo Viola 《NDT & E International》2005,38(5):325-334
The aim of this work is to demonstrate the use of a commercial finite element package, ABAQUS EXPLICIT, to model ultrasonic guided waves in structural components. The particular application of interest is modeling the interaction of a broadband vertical bending mode with transverse-type defects in railroad tracks. This topic is part of a broader project on high-speed defect detection in rails by long-range ultrasonic inspections. Reflection coefficient spectra in the 20–45 kHz range are obtained for four different sizes and three different orientations of transverse head flaws. A preliminary study of Lamb waves in a free plate helps drawing modeling guidelines for the rail. 相似文献
9.
Image composition is widely used in television and film industry to create synthetic visual effects. It requires seamless integration of different parts of two or more images into a single image. Existing image composition techniques only change the local contents of the resulting image while in many cases local changes may also require some global effects as well. For example, if the image of sun from one image is transferred to another image, the global brightness pattern should also be transferred. Unfortunately existing techniques cannot handle global effects of local content manipulations. This paper describes a novel image composition technique which captures global effects associated with a specific local content from one image and incorporates in the second image. In our proposed technique, all images are transformed to the frequency domain. The composite image is created in frequency domain by mixing different frequencies from multiple images and then transformed back to the spatial domain. We have experimented the proposed technique to shift the image of sun along with its global brightness pattern, the global effects of rain and also for transferring global texture pattern from one image to the other. In most of the cases the results produced by our algorithm appear far close to real images than state of the art existing image composition techniques. 相似文献
10.
The adhesion and interfacial properties of polyurethane (PU) foams with thermoplastic (TP) materials were investigated using different techniques. The adhesion performance of PU foam with TP materials was evaluated using the peel test method, and the adhesion durability was checked after different climate treatments. X‐ray photoelectron spectroscopy (XPS), atomic force microscopy (AFM), and contact angle measurements were used to study the surface and interface morphology of PU foam and TP material system. Three types of PU foam samples which differ in their composition and also five commercially available TP blends systems, based on poly(carbonate), poly(styrene‐co‐maleic anhydride), poly(acrylonitrile‐butadiene‐styrene), and silicone acrylate rubber have been used. The slow reacting foam shows the best adhesion properties with all the TP materials. The climate treatments strongly effected the PU foam adhesion durability with poly(carbonate) containing TP materials (70–80% loss in adhesion), but nearly no effect with poly(styrene‐co‐maleic anhydride). The samples with lowered adhesion could be separated by peeling without visible foam residues on the TP surface. AFM, XPS, and surface tension studies have shown that the surface properties of the TP material are still governed by the PU foam. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 479–488, 2007 相似文献