莱芜黑猪肉中烟酸含量的测定

采用高效液相色谱法测定莱芜黑猪肉中烟酸的含量,并对提取方法及色谱条件等方面进行了改进,以Kromasil C_(18)柱为分离柱,甲醇–0.05mol/L磷酸二氢钾缓冲液(体积比5∶95)为流动相,柱温30℃,紫外检测器在波长261nm条件下检测,可以在4min左右完成分析。烟酸在1.0～25.0mg/L范围内有良好的线性关系(R=0.9998),相对标准偏差为0.62%(n=6),平均加标回收率为98.4%,检出限为2.0×10~(-4)g/kg,为准确测定莱芜黑猪肉中的烟酸含量提供了一种简便快捷的检测方法。     

小像元红外探测器读出电路设计研究

介绍了基于SMIC 0.18 μm 3.3 V工艺设计研究的第一款小像元红外探测器读出电路,间距10 μm,规模1024×1024。文章详细介绍了像素输入级以及列级、输出级运放的设计,为提高线性摆伏,设计选用了低阈值NMOS管nmvt 33,仿真分析证明低阈值管nmvt 33的噪声性能优于普通管n 33；版图设计对关键信号线和敏感点采取隔离处理措施,对像元间串扰进行了仿真分析,有效控制了信号串扰。电路经测试使用各项功能正常,最大电荷处理能力达到4.3 Me-,动态范围≥65 dB,读出速率达到10 MHz,性能指标满足设计要求。     

电子束和接触式曝光机的混合曝光技术

Ⅰ线光致抗蚀剂可以同时实用电子束和光学系统曝光，在50kV加速电压下，其曝光剂量为50-100μC/cm^2，曝光后在0.7%NaOH溶液内显影1分钟。其灵敏度比PMMA快5倍，分辩率为0.5μm。采用两方法制备CaAsPHEMT：一种用Ⅰ线光致抗蚀剂，对源、漏及栅全部都采用电子束曝光，制备了0.5μm栅长的GaAs PHEMT；另一种将源、漏及栅分割成两部分，其中精细部分由电子束曝光，其余部分由光学系统曝光，用这种方法制备了0.25μm栅长的GaAs PHEMT。Ⅰ     

Effects of modeling means on properties of monitoring models of spot welding quality

Analyzing and modeling the relation between monitoring information during welding and quality information of the joints is the foundation of monitoring resistance spot welding quality. According to the means of modeling, the known models can be divided into three large categories: single linear regression models, multiple linear regression models and multiple non-linear models. By modeling the relations between dynamic resistance information and welding quality parameters with different means, this paper analyzes effects of modeling means on performances of monitoring models of resistance spot welding quality. From the test results, the following conclusions can be drawn: By comparison with two other kinds of models, artificial neural network (ANN) model can describe non-linear and high coupling relationship between monitoring information and quality information more reasonably, improve performance of monitoring model remarkably, and make the estimated values of welding quality parameters more accurate and reliable.     

Effects of modeling means on properties of monitoring models o spot welding quality

Analyzing and modeling the relation between monitoring information during welding and quality information of the joints is the foundation of monitoring resistance spot welding quality.According to the means of modeling,the known models can be divided into three large categories:single linear regression models,multiple linear regression models and multiple nonlinear models.By modeling the relations between dynamic resistance information and welding quality parameters with different means,this paper analyzes effects of modeling means on performances of monitoring models of resistance spot welding quality. From the test results,the following conclustons can be drawn:By comparison with two other kinds of models,artificial neural network(ANN) model can describe non-linear and high coupling relationship between monitoring information and quality information more reasonably,improve performance of monitoring model remarkably,and make the estimated values of welding quality parameters more accurate and reliable.     

三峡施工供用电网电压不平衡现象分析

针对三峡施工供用电网中产生的电压不平衡的各种原因进行了分析，总结归纳出了导致电压不平衡的几种故障的一些主要现象和基本特征，并根据三峡施工供用电网35kV和6kV系统的实际运行情况，验证了在小接地电流系统中采用过补偿运行方式的优越性和重要性。     

关于发展小灵通定位业务的几点思考

随着社会的发展，人们的活动范围越来越大，而且越来越不确定。这就为通信业开展定位服务带来了无限商机。     

杀螨脒全残留气相色谱分析

本文研究杀螨脒在茶叶和土壤中全残留的气谱分析法。本法是将杀螨脒及其降解物分别用酸和碱水解力2,4-二甲苯胺,用氟丁酸酐衍生为多氟衍生物,用气相色谱,电子捕获检测器测定。最小检测量2×10~(-12)克。样品最低检测浓度0.001～0.0003ppm,方法的灵敏度、准确度和精密度均达农药残留分析技术要求。     

关于深冲薄钢板中的夹杂和成形性的商榷

对深冲薄钢板大生产的全工艺过程进行了跟踪，研究了ＷＹ０８ＡｌＡ薄钢板中Ａｌ＿２Ｏ＿３的形成，形态以及它们对冷轧成品的深冲性能和冲压小件的冲压成形废品率的影响。     

中国建筑防水市场现状和发展综述

分析了近年中国建筑防水材料行业发展所处的宏观环境;从产量、行业经济运行特点、科技创新、标准和规范、产业政策、存在问题等方面论述了2004年防水行业发展现状;披露了对北京地区2004年建筑防水工程市场所作的调查结果;介绍了中国建筑防水行业国际化进程中的企业动向;对今后几年防水行业的发展趋势作了预测.