Magneto-dielectric effect in Pb(Zr0·52Ti0·48)O3 filled nanoporous Ni 0 ·5Zn 0 ·5Fe 2 O 4 composite

Nanoporous Ni_0·5Zn_0·5Fe₂O₄ particles of diameter, ~ 9·5 nm, were synthesized by citric acid assisted thermal decomposition in an autoclave. The BET surface area measured was 80 m² g^???1 and the average pore diameter was 2·5 nm. By soaking the particles in a suitable precursor solution and then subjecting them to a heat treatment at 923 K for 3 h, Pb(Zr_0·52Ti_0·48)O₃ was grown within the nanopores. X-ray and electron diffraction studies confirmed the presence of both these phases. The nanocomposites showed ferromagnetic behaviour over the temperature range 2–300 K. No ferroelectric hysteresis loop could be found which was consistent with the earlier theoretical prediction of loss of ferroelectricity below a critical thickness of 2·4 nm. Good magneto-dielectric response of the order of 7% at a magnetic field of 9 kOe was recorded for the present system. This is believed to arise due to a negative magnetostriction coefficient of Ni_0·5Zn_0·5Fe₂O₄ which exerted a compressive strain on Pb(Zr_0·52Ti_0·48)O₃ thereby lowering the tetragonality in its crystal structure.     

VISCOMETRIC MEASUREMENT OF CHROMIUM(III)-POLYACRYLAMIDE GELS†

Gelled polymers are being used increasingly to modify the movement of injected fluids in secondary and enhaced oil recovery processes. A common gelation process involves the reduction of Cr(VI) to Cr(III) in the presence of polyacrylamide. The Cr(III) reacts or interacts with the polymer to form a gel network. Although correlations of gelation time with principal process variables have been obtained, viscometric data have not been reported during or after gelation. These data are needed for fluid flow calculations in surface equipment and estimation of flow behaviour in reservoir rocks.

A Weissenberg Rheogoniometer, with cone and plate geometry, was used to obtain viscometric data for the gelation of polyacrylamide and chromium (III). Solutions consisting of polyacrylamide polymer, sodium dichromate-dihydrate and sodium bisulfite were gelled under a steady shear field at constant temperature. The shear stress versus time profile for the galation process was interpreted to define a gelation time and to determine the apparent viscosity of the gelled fluid. The gelation time decreased as the applied shear rate increased up to about 14.25 sec^?1 and was affected by shear rate history. Viscometric properties of the gelled solutions were determined. Apparent viscosity of the gelled solutions decreased as the shear rate under which they were formed increased.

Post gelation studies indicated that gels exhibited a residual stress at zero shear rate and behaved as Bingham plastics under steady shear. Gels formed at low shear rates were more viscous than gels formed at high shear rates. However, the structure of these gels was susceptible to shear degradation.     

A method of obtaining the dual-input describing functions for a periodic input†

A combined analytic and graphic procedure is described for obtaining the dual-input describing functions for a class of non-linear elements subjected to a periodic input. The procedure is illustrated by considering the non-linearity to be a simple contactor involving hysteresis and the describing functions obtained for the element are presented.     

Simulation im Bereich der Produktionsplanung und -steuerung (PPS)

Up to now, within the area of PPC, simulation is mainly used for local applications, i. e., particular machines, production lines etc. Missing proceeding models as well as automated interfaces prevented especially small and medium sized producers from comprehensive applications to the whole production process. The paper shows ways to overcome these restrictions and outlines a concrete approach to the coupling of a PPC-System with a simulation tool.     

Detection of Salmonella spp. in Oysters Using Polymerase Chain Reactions (PCR) and Gene Probes

The polymerase chain reaction (PCR) DNA amplification method was used to identify oligonucleotide primers from a target gene, hns, to specifically detect SulmonelIu spp. in contaminated oysters. The primers for PCR amplification and a hybridizing oligonucleotide probe to detect the amplified DNA were specific for all Salmonella spp. tested. Modification of a procedure for extracting DNA from oyster tissue matrices followed by PCR amplification, and coupled with gene-probe hybridization detected <40 cells of seeded or naturally occurring Sulmonella spp./g of oyster meat samples without any enrichment step. The detection of SaZmonella spp. was reliable, sensitive, and required considerably less time than conventional microbiological culture methods.     

Electronic property investigations of single-walled carbon nanotube bundles in situ within a transmission electron microscope: an evaluation

We have evaluated a combined transmission electron microscopy (TEM)–scanning tunnelling microscopy (STM) (hence TEM-STM) sample holder for the investigation of the mechanical and electrical properties of individual bundles of single-walled carbon nanotubes (SWCNTs) together with their simultaneous observation, analysis and mechanical modification in the TEM. Current-voltage (I–V) measurements from bundles of SWCNTs were observed to change as the bundles were deformed both reversibly and irreversibly, although the observed behaviour was somewhat complex. Electron energy loss spectroscopy (EELS) analysis revealed measurable changes in the bonding of the carbon atoms within the graphene layers upon bundle deformation, with measurable changes in the π*/(π*+σ*) peak ratios observed at the carbon K-edge. Reversible deformation of the bundles was consistent with the sensitivity of σ bonding to deviations from nonplanarity, whereas irreversible deformation was consistent with the introduction of nonhexagonal defects into the graphene sheets.     

Fingerprint matching,spoof and liveness detection:classification and literature review

Fingerprint matching,spoof mitigation and liveness detection are the trendiest biometric techniques,mostly because of their stability through life,uniqueness and their least risk of invasion.In recent decade,several techniques are presented to address these challenges over well-known data-sets.This study provides a comprehensive review on the fingerprint algorithms and techniques which have been published in the last few decades.It divides the research on fingerprint into nine different approaches including feature based,fuzzy logic,holistic,image enhancement,latent,conventional machine learning,deep learning,template matching and miscellaneous tech-niques.Among these,deep learning approach has outperformed other approaches and gained significant attention for future research.By reviewing fingerprint literature,it is historically divided into four eras based on 106 referred papers and their cumulative citations.     

The influence of time elapsed after milking and lactation stage on the lactoperoxidase system of milk in Sahiwal cattle and Nili‐Ravi buffaloes

The effects of time elapsed after milking and lactation stage were assessed on the lactoperoxidase (LP) enzyme activity and concentrations of thiocyanate in Sahiwal cattle (N = 15) and Nili‐Ravi buffaloes (N = 15). The LP activity and thiocyanate concentrations decreased as the time elapsed after milking (P < 0.05) but the concentration of these components increased as the lactation advanced. The LP enzyme activity was sufficient until 12 h post milking but the thiocyanate concentration after 8 h decreased to an insufficient level to activate the LP System, hence additional thiocyanate would be beneficial from external sources. No difference was noted regarding the LPS activity in cattle and buffaloes at the time of collection and subsequently after storage. However, at the end of lactation, the thiocyanate concentration was lower in buffaloes than that in cattle. (P < 0.05).     

Failure mode of laser welds in lap‐shear specimens of high strength low alloy (HSLA) steel sheets

In this paper, the failure mode of laser welds in lap‐shear specimens of non‐galvanized SAE J2340 300Y high strength low alloy steel sheets under quasi‐static loading conditions is examined based on experimental observations and finite element analyses. Laser welded lap‐shear specimens with reduced cross sections were made. Optical micrographs of the cross sections of the welds in the specimens before and after tests are examined to understand the microstructure and failure mode of the welds. Micro‐hardness tests were also conducted to provide an assessment of the mechanical properties in the base metal, heat‐affected and fusion zones. The micrographs indicate that the weld failure appears to be initiated from the base metal near the boundary of the base metal and the heat‐affected zone at a distance away from the pre‐existing crack tip, and the specimens fail due to the necking/shear of the lower left load carrying sheets. Finite element analyses based on non‐homogenous multi‐zone material models were conducted to model the ductile necking/shear failure and to obtain the J integral solutions for the pre‐existing cracks. The results of the finite element analyses are used to explain the ductile failure initiation sites and the necking/shear of the lower left load carrying sheets. The J integral solutions obtained from the finite element analyses based on the 3‐zone finite element model indicate that the J integral for the pre‐existing cracks at the failure loads are low compared to the fracture toughness and the specimens should fail in a plastic collapse or necking/shear mode. The effects of the sheet thickness on the failure mode were then investigated for laser welds with a fixed ratio of the weld width to the thickness. For the given non‐homogenous material model, the J integral solutions appear to be scaled by the sheet thickness. With consideration of the plastic collapse failure mode and fracture initiation failure mode, a critical thickness can be obtained for the transition of the plastic collapse or necking/shear failure mode to the fracture initiation failure mode. Finally, the failure load is expressed as a function of the sheet thickness according to the governing equations based on the two failure modes. The results demonstrate that the failure mode of welds of thin sheets depends on the sheet thickness, ductility of the base metal and fracture toughness of the heat‐affected zone. Therefore, failure criteria based on either the plastic collapse failure mode or the fracture initiation failure mode should be used cautiously for welds of thin sheets.