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Aysel Buyuksagis Meltem Dİlek 《Protection of Metals and Physical Chemistry of Surfaces》2019,55(6):1182-1194
Protection of Metals and Physical Chemistry of Surfaces - The corrosion inhibition and adsorption characteristics of the extract obtained from the plant Papaver somniferum L. (PSL) by... 相似文献
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Nail Altunay Adil Elik Ramazan Gürkan 《Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment》2018,35(2):222-232
Acrylamide (AAm) is a carcinogenic chemical that can form in thermally processed foods by the Maillard reaction of glucose with asparagine. AAm can easily be formed especially in frequently consumed chips and cereal-based foods depending on processing conditions. Considering these properties of AAm, a new, simple and green method is proposed for the extraction of AAm from thermally processed food samples. In this study, an ionic liquid (1-butyl-3-methylimidazolium tetrafluoroborate, [Bmim][BF4]) as extractant was used in the presence of a cationic phenazine group dye, 3,7-diamino-5-phenylphenazinium chloride (PSH+, phenosafranine) at pH 7.5 for the extraction of AAm as an ion-pair complex from selected samples. Under optimum conditions, the analytical features obtained for the proposed method were as follows; linear working range, the limits of detection (LOD, 3Sb/m) and quantification (LOQ, 10Sb/m), preconcentration factor, sensitivity enhancement factor, sample volume and recovery% were 2.2–350 µg kg?1, 0.7 µg kg?1, 2.3 µg kg?1, 120, 95, 60 mL and 94.1–102.7%, respectively. The validity of the method was tested by analysis of two certified reference materials (CRMs) and intra-day and inter-day precision studies. Finally, the method was successfully applied to the determination of AAm levels in thermally processed foods using the standard addition method. 相似文献
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Aysel Kantürk Figen Evren Terzi Nural Yilgör Saip Nami Kartal Sabriye Pişkin 《Korean Journal of Chemical Engineering》2013,30(4):878-890
hermal degradation characteristics of Tetra Pak panel boards (TPPB) can be useful to improve usage of such panels as an alternative to wood-based products such as plywood, fiberboard, and particleboard. In the study, samples from the TPBBs manufactured from waste Tetra Pak packages (WTPP) were heated in a nitrogen atmosphere at different heating rates (10, 15 and 20 °C/min) using a thermal analysis system. The Coats-Redfern kinetic model was applied to calculate kinetic parameters. The degradation rate equations were then established. In addition, the kinetic compensation effect (KCE) was used to correlate the pre-exponential factor (k o ) with activation energy (E a ) and the existence of the KCE was accepted. TG-FT/IR analyses were applied to the TPPB degradation and then the FT-IR stack plot was used to analyze gas products (CO2, CH4, HCOOH, and CH3OH). Infrared vibrational frequencies and the micro, crystal structure of the TPPBs were investigated by Fourier transform infrared spectroscopy (FT-IR), Scanning electron microscope (SEM) and X-Ray diffraction analysis (XRD), respectively. 相似文献
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In this study, anhydrous sodium metaborate (NaBO2), an industrial and technologically important boron compound, synthesis from concentrated tincal (CT) was carried out. Experiments with different temperature and time were performed in the parametric investigation to map out the reaction mechanism. Crystalline phase characterization of metaborates products indicates that anhydrous NaBO2 synthesis from CT occurred at 400 °C with 5 h of reaction conditions. At the end of synthesis, the obtained anhydrous NaBO2 product can be used in many fields without having the calcination step due to the advantages of this method. 相似文献
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There has been a recent increase in research into the possible ways of protecting individuals from cancer by making changes in dietary habits. In this study raw and boiled juice and leaf and dried seeds of Urtica sp, Stachys annula, sage, rosehip, grape molasses and tarhana were not found mutagenic in S typhimurium TA 100. All of the foods decreased sodium azide mutagenicity in S typhimurium TA 100. Among the foods tested, raw Urtica sp (46.32%) and rosehip (44.03%) showed the highest antimutagenic effect followed by leaf of Urtica sp (41.25%), boiled juice of Urtica sp (37.22%), Stachys annula (36.42%), grape molasses (33.03%) and tarhana (28.60%), respectively. The antimutagenic activities of Urtica sp and rosehip were found to be significantly higher than the antimutagenic activity of tarhana (p<0.01). © 1999 Society of Chemical Industry 相似文献
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Determination of aflatoxins in peanut butter and sesame samples using high-performance liquid chromatography method 总被引:1,自引:0,他引:1
Gülderen?YentürEmail author Buket?Er Muzaffer?Gür ?zkan Aysel?Bayhan ?ktem 《European Food Research and Technology》2006,224(2):167-170
In this study, total number of samples analysed were 20 packages of sesame and 20 cans of peanut butter, which were collected from Ankara local markets, Turkey. Extraction and determination of aflatoxins have been made by immunoaffinity column technique and high-performance liquid chromatography (HPLC) method. Mean levels (±SE) of aflatoxins B1, B2, G1 were found to be 15.756±3.129 ng/g, 1.232±0.244 ng/g and 9.689±1.005 ng/g, respectively in peanut butter samples. Regarding the sesame samples, mean level of aflatoxin G1 was found to be 0.754±0.213 ng/g. Our data revealed that while aflatoxin levels found in sesame samples were within the Turkish Food Codex (TFC) values, for peanut butter samples, they were higher than the TFC values. 相似文献
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In the present study, a novel microwave assisted method has been developed for sodium metaborate dihydrate (NaBO2·2H2O) synthesis. Anhydrous NaBO2, a derivative of borax, is an industrially and technologically important boron compound used as a raw material for the thermochemical production of sodium borohydride (NaBH4). The effects of different microwave treatment conditions such as microwave power (90, 270 and 360 W) and irradiation time (1, 2, and 5 min) on the synthesis of NaBO2·2H2O were examined. After microwave irradiation at 270 W for 1 min, NaBO2 crystals with 2 molar equivalents of water were formed. Anhydrous NaBO2 was obtained following incubation at 400 °C for 33 min under calcination conditions. Then the resulting anhydrous NaBO2 powder was reacted with MgH2 under 60 bar hydrogen atmosphere at 470 °C, leading to successful production of NaBH4 with 93% yield. 相似文献
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Aysel T. Atimtay 《Clean Technologies and Environmental Policy》2001,2(4):197-208
World primary energy demand increases with increases in population and economic development. Within the last 25 years, total
energy consumption has almost doubled. In order to meet this demand, research into new sources of energy as well as improving
the efficiency of energy production technologies is being carried out. In both cases, the production of clean energy is very
important because of environmental concerns and regulations. Integrated gasification combined cycle (IGCC) technology seems
to be one of the most promising technologies for production of energy by using fossil fuels, especially coal. Hot gas desulfurization
is a crucial issue in the development of the IGCC system. This paper reviews the importance of clean energy production, the
IGCC technology and focuses on the development of several metal oxide-based sorbents used for desulfurization of the hot coal
gas in the IGCC system. 相似文献
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