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排序方式: 共有463条查询结果,搜索用时 15 毫秒
1.
Summary Well-defined living polymers of isobutyl vinyl ether were obtained in the polymerization initiated with ethylaluminum dichloride (EtAlCl2) in conjunction with a stoichiometric excess of dioxane (5–10 vol%) in n-hexane at 0°C. Under these conditions, the number-average molecular weight of the polymers increased in direct proportion to monomer conversion, while the molecular weight distribution stayed narrow (Mw/Mn = 1.1–1.25). In sharp contrast, the EtAlCl2-initiated polymerization in the absence of dioxane led to non-living polymers with a broad molecular weight distribution. It was concluded that the propagating carbocation is stabilized not by the counteranion but by an externally added basic compound (dioxane) that strongly interacts with the active end. 相似文献
2.
Fumiya Kurokawa Masaya Kishimoto Yuichi Tsujiura Hirotaka Hida Isaku Kanno 《Microsystem Technologies》2016,22(6):1275-1283
In this study, we fabricated multilayer ceramics (MLCs) composed of multilayered Pb(Zr,Ti)O3 (PZT) piezoelectric thin films with internal electrodes and evaluated their dielectric and piezoelectric properties. The stack of PZT ferroelectric layers (550 nm) and SrRuO3 (SRO, 80 nm) electrodes were alternatively deposited on Pt/Ti-coated silicon-on-insulator substrates by radio-frequency magnetron sputtering. The MLCs composed of one, three, and five PZT layers were fabricated by the alternate sputtering deposition of PZT ferroelectric layers and SRO electrodes through the movable shadow mask. The capacitances of MLCs were proportionally increased with the number of PZT layers, while their relative dielectric constants were almost same among the each MLC. The MLCs exhibited symmetric and saturated P–E hysteresis loops similar to the conventional PZT thin films. We estimated that the piezoelectric properties of MLCs by FEM simulation, and confirmed that the effective transverse piezoelectric coefficients (d 31,eff ) increased with the number of PZT layers. The piezoelectric coefficients calculated to be d 31,eff = ?2964 pC/N at 25 PZT layers, which is much higher than those of conventional single-layer piezoelectric thin films. 相似文献
3.
Nishikino M. Tanaka M. Ochi Y. Kishimoto M. Ishino M. Hasegawa N. Kado M. Sukegawa K. Kawachi T. Nagashima K. 《IEEE journal of selected topics in quantum electronics》2004,10(6):1382-1387
We have recently reported the successful development of a fully coherent X-ray laser (XRL) at 13.9 nm by an oscillator-amplifier configuration with two targets. In the experiment, a seed XRL beam from the first target is injected into a plasma amplifier at the second target. The observed XRL beam has full spatial coherence and 0.2 mrad of nearly diffraction-limited divergence. In order to improve the output fluence, the amplification properties of the XRL beam have been investigated using various plasma lengths of the second amplifier target. The output energy has been improved by a factor of ten, increasing the length of the gain region to 10 mm, resulting in about 0.2 /spl mu/J of output energy. 相似文献
4.
Based on finite-difference time-domain(FDTD) method,the wave propagation and localization in two-dimensional defect-containing piezoelectric phononic crystals are investigated when the mechanical-electrical coupling is taken into account.The characteristics of localized defect modes are studied,and the effects of the number and direction of defects on the defect modes and transmission coefficients are discussed.Numerical results of defect modes and transmission coefficients are presented for BaTiO3/polymer piezocomposite,and from which we can see that the number and direction of defects have pronounced effects on the defect modes and transmission coefficients.The results also show the existence of elastic wave localization in piezoelectric phononic crystals containing defects. 相似文献
5.
Abstract Under 24-GHz millimetre-wave irradiation heating ionic conductivity of zirconia base ceramics was up to 20 times higher than that of a conventionally-heated sample at the same temperature of 400 °C. The degree of enhancement could be altered by changing the stabilising atom from Y to Yb. Enhancement of ionic conduction was prominent in the setup condition of larger self-heating ratio and larger MMW absorbing materials. The isothermal improvement of ionic conductivity under MMW irradiation would be ascribed to the non-thermal effect. 相似文献
6.
Partial isothermal sections of the Bi-Fe-Ti system at 700 °C and 900 °C were constructed to investigate the reactivity of Fe with Bi-Ti liquid alloy. In the ternary system, three-phase equilibria such as liquid-Fe-Fe2Ti, liquid-Fe2Ti-Bi2FeTi4, and liquid-Bi9Ti8-Bi2FeTi4 were confirmed at both temperatures. The solubility of Fe in liquid Bi at these temperatures is negligibly small. On the other hand, it is notable that the solubility of Fe in liquid Bi containing Ti at 900 °C is much larger and reaches 2.3 mol pct. Then, we measured the electromotive force (emf) between Bi-20 mol pct Ti alloy and pure Ti at 700 °C in equimolar NaCl-KCl where 1 mol pct TiCl2 was added. From the result, the interaction parameter of the liquid phase in the Bi-Ti system and the standard molar Gibbs energies of formation of Bi9Ti8 and Bi2FeTi4 at 700 °C were estimated. 相似文献
7.
Isamu Ogura Naomi Hashimoto Mari Kotake Hiromu Sakurai Atsuo Kishimoto Kazumasa Honda 《Aerosol science and technology》2014,48(7):758-767
A simple sampling method to collect aerosol particles for transmission electron microscope (TEM) analysis was developed by R’mili and others in 2013. The method involves passing air through a holey carbon film-coated copper mesh TEM grid (holey carbon grid) and sampling particles by filtration. In this study, we proposed a modified calculation method to represent the collection efficiencies of holey carbon grids, taking into consideration the porosity of the copper mesh. We then evaluated the particle collection efficiencies of holey carbon grids both theoretically and experimentally. We tested the collection efficiency of two types of holey carbon grids, with nominal pore sizes of 1.2 and 0.6 μm, using particles of monodispersed polystyrene latex (PSL) and potassium chloride. The overall collection efficiency of each grid (Egrid) was determined by the downstream/upstream concentration ratio measured by condensation particle counters (CPCs). In addition, for PSL particles, the collection efficiency of the holey carbon film (Efilm) was determined by the ratio of the number of particles on the film (counted on a scanning electron microscope) to the number of inflow particles (counted by a CPC). We compared model calculations against the experimental results obtained in this study and those reported by R’mili and others in 2013. These data showed that the calculated Egrid values were in reasonably good agreement with the experimental Egrid values. However, although the model calculation indicated that Efilm ≈ Egrid, there was an inconsistency between the experimental Efilm and Egrid, which requires further investigation in order to determine its cause.
Copyright 2014 American Association for Aerosol Research 相似文献
8.
针对日本国鬼怒河流域小流量河流,通过对河床上附着生物膜的组成、底栖生物、细菌活性分析和AGP试验,研究了污水厂二级处理排放水对小流量河流生态的影响.研究表明,当污水厂二级处理排放水占河流流量比例较大时(研究河流所占比例为35%),同样会引发河流富营养化和影响河流水体的生态.因此,从保护水环境及其生态考虑,有必要对污水进行深度处理. 相似文献
9.
Grimshaw Andrew Morgan Mark Merrill Duane Kishimoto Hiro Savva Andreas Snelling David Smith Chris Berry Dave 《Computer》2009,42(2):27-34
To expand the use of distributed computer infrastructures as well as facilitate grid interoperability, OGSA has developed standards and specifications that address a range of scenarios, including high-throughput computing, federated data management, and service mobility. 相似文献
10.
Teruhisa Horita Haruo Kishimoto Katsuhiko Yamaji Manuel E. Brito Yueping Xiong Harumi Yokokawa 《Journal of power sources》2009,193(1):180-184
Reactivity of oxide scale on Fe-Cr alloy with Na-containing gases was examined to estimate the stability against sodium (Na): vapors of NaCl and Na2SO4 exposures with air flow at 1073 K. The identified reaction phases were Cr-Mn spinel, Cr2O3, and alloy from the X-ray diffraction of surface with no Na-reaction products. However, the protective oxide scales (Mn-Cr spinel and Cr2O3 layers) on the Fe-Cr alloy were partially decomposed by reacting with Na to form Na-compounds inside the oxide scale/alloy interfaces. In some parts, anomalous oxide scales were found around the oxide scale/Fe-Cr alloy interfaces, with forming Na-rich compounds: the compounds were distributed inner parts of oxide scales around oxide scale/alloy interfaces. The stability of oxide scales and degradation were discussed based on the observed distribution of elements. 相似文献