Revolving Vernier Mechanism Controls Size of Linear Homomultimer

A new kind of the Vernier mechanism that is able to control the size of linear assembly of DNA origami nanostructures is proposed. The mechanism is realized by mechanical design of DNA origami, which consists of a hollow cylinder and a rotatable shaft in it connected through the same scaffold. This nanostructure stacks with each other by the shape complementarity at its top and bottom surfaces of the cylinder, while the number of stacking is limited by twisting angle of the shaft. Experiments have shown that the size distribution of multimeric assembly of the origami depends on the twisting angle of the shaft; the average lengths of the multimer are decamer, hexamer, and tetramer for 0°, 10°, and 20° twist, respectively. In summary, it is possible to affect the number of polymerization by adjusting the precise shape and movability of a molecular structure.     

What Business Owners Expect From a Crisis Manager? A Competency Model: Survey Results From Czech Businesses

This competency model of a crisis manager has been developed based on cooperation with managers and experts in the field of crisis management. The brainwriting method was used to generate an overview of the competencies expected of a crisis manager. Using a mind map three basic groups of competencies were developed. The participants used Saaty's method to determine the significance of individual competencies. The different attributes of individual competencies according to the level of their development were established. Finally all individual competencies were assigned a target value which indicates the expected level of competence for the position of a crisis manager. The model of competencies is a practical tool for the establishment of crisis management system in a company.     

Determination of Fexofenadine in Tablets by Capillary Electrophoresis in Free Solution and in Solution with Cyclodextrins as Analyte Carriers

ABSTRACT

Capillary electrophoresis (CE) methods for the determination of fexofenadine (FEX) in commercial pharmaceuticals were developed. It was demonstrated that FEX could be effectively analyzed in free solution cationic CE at low pH. Another analytical approach studied was based on cyclodextrin (CD) modified CE where highly charged CD derivatives served as analyte carriers. In this way, the separation range was spread to physiological pH region and a CE analysis of FEX, present actually in its zwitterionic form, could be accomplished. Several parameters affecting the separations were studied, including the type and concentration of carrier ion, counterion, analyte carrier, and pH of the buffer. The methods based on the free solution CE and CD-modified CE were compared each other, validated, and applied for the determination of FEX in tablets.     

Spray-dry synthesis of β-Cu1.8Zn0.2V2O7 ceramic fine particles showing giant negative thermal expansion

We used spray-dry method to synthesize fine powder of β-Cu_1.8Zn_0.2V₂O₇ showing large negative thermal expansion (NTE) linearly to temperature over a wide temperature range. The NTE of β-Cu_1.8Zn_0.2V₂O₇ is produced by microstructures consisting of voids and anisotropic thermal deformation of crystal grains in ceramics. By reducing the size of the microstructures that produce NTE, large NTE equivalent to that of bulk was realized, even for ceramic particles of about 2 μm size. Comparison with particles produced using a conventional method demonstrates that the particle size distribution is narrow and that the particles are nearly spherical. This achievement is expected to pave the way to use of NTE materials in micrometer-scale control of thermal expansion.     

Magnetic Torque Measurements on Bi2201 Single Crystal in High Magnetic Fields

The magnetic field direction dependence of the magnetic torque in the superconducting state of Bi ₂ Sr _1.65 La _0.35 CuO ₆₊ (Bi2201) single crystal has been measured in several static magnetic fields up to 200 kOe. The applied field dependence of the anisotropy parameter, , defined by the square root of the effective mass ratio has been obtained by fitting the magnetic torque curves at 17 K by means of the effective mass model. For Bi ₂ Sr ₂ CaCu ₂ O ₈₊ (Bi2212), the values up to 210 kOe were reported previously. At each field, for Bi2201 is larger than that for Bi2212. Since the value decreases as the field increases both for Bi2201 and Bi2212, the reduction of by the application of the high magnetic field is considered to be common for Bi-based layered superconductors.     

Measurement method using coupled transmission lines for voltage transients on the distribution line

It is well known that voltage transients are caused by the operation of switchgears in a power system. The voltage transients travel along the power line as a traveling wave, and cause malfunction of electrical devices, communication systems, and the operational error of a control system. The voltage transients at the making operation of switchgear were examined to obtain the fundamental data for considering the immunity of communication systems used on a power system. However, it was difficult to observe the voltage transients using the potential transformer and the capacitance potential device because the transients were very rapid. Therefore, a measurement method using the coupled transmission line system is proposed to measure the high-speed and high-voltage transients, and the actual experimental results on the 6.9-kV power system are presented. This method enables the measurement of high-speed voltage transients in out of contact with the power system.     

In-Plane Anisotropy of the Upper Critical Field of La2−x Sr x CuO4 in the Underdoped and Overdoped Regimes

For La_2–x Sr _x CuO₄ single-crystals in the underdoped and overdoped regimes, we have measured the electrical resistivity along the c-axis, _c , under constant magnetic fields, changing the field direction in the ab-plane. At x=0.08, 0.12 and 0.16 in the underdoped and almost optimally-doped regimes, clear anisotropy of _c with the fourfold symmetry in the ab-plane has been observed. This symmetry is regarded as the fourfold symmetry of the upper critical field, H _c2, and explained as being mainly due to the anisotropy of the superconducting energy gap owing to the d_x ^{2-y 2} pairing. The magnitude of the fourfold component of H _c2, H _c2/H _c2, is largest in x=0.08 among the three crystals. At x=0.20 in the overdoped regime, no clear fourfold symmetry has been observed. It appears that the fourfold symmetry is easy to observe in the underdoped regime rather than in the overdoped regime.     

On Active Noise Control Systems With Online Acoustic Feedback Path Modeling

The presence of strong acoustic feedback degrades the convergence speed of the active noise control (ANC) filter, and in the worst case the ANC system may become unstable. A fixed feedback neutralization filter, obtained offline, can be used to neutralize the acoustic feedback. The feedback path, however, may be time varying, and we may need continual adjustments during online operation of the ANC system. This paper proposes a new method for online modeling of the acoustic feedback path in ANC systems. The proposed method uses three adaptive filters; a noise control filter, a feedback path modeling (FBPM) filter, and an adaptive noise cancelation (ADNC) filter. The objective of ADNC filter is to remove the disturbance from the desired response of FBPM filter. In comparison with the existing method, which works only for predictable noise sources, the proposed method can work, as well, with the broadband noise sources. The computer simulations are carried out for narrowband (predictable) (case I) and broadband (random) noise sources (case II). It is demonstrated that the proposed method performs better than the existing method in both cases     

Evolution of strength and structure during SPD processing of Ti–45Nb alloys: experiments and simulations

A β-phase Ti–45Nb alloy was processed by several severe plastic deformation (SPD) methods as high-pressure torsion, cold rolling and folding, and hydrostatic extrusion to enhance its strength by achieving an ultrafine grained structure without affecting the Young’s modulus being close to that of bone material. Mechanical properties during processing were monitored by direct torque and Vickers hardness measurements, while the micro-/nano-structural evolution was investigated by transmission electron microscopy and X-ray line profile analysis. Simulations of both mechanical and micro-/nano-structural data were performed on the basis of the SPD work-hardening model by Zehetbauer. The simulations not only found a good agreement with the deformation-specific evolution of strength and density of individual dislocations but also well reflected mesoscopic structural quantities such as the sizes of cell/grain interiors and walls without introducing additional fitting parameters.