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排序方式: 共有2328条查询结果,搜索用时 10 毫秒
1.
The crystallization process of hexagonal boron nitride in the presence of copper has been investigated. The positive effect of copper on the crystallinity of boron nitride was observed in the three studied systems of: nitrided boron, nitrided boron–carbon, and previously prepared turbostratic boron nitride. However, the presence of copper hindered the formation of boron carbonitride and produced graphite and boron nitride phases separately. Poor crystallinity was found as a conditio sine qua non for the existence of such a compound. Well-crystallized boron nitride had a very low spacing parameter 0.3328 nm and a regular hexagonal shape. 相似文献
2.
Apparent carbon aromaticities, fa, of some asphaltenes have been measured by n.m.r. in solution and compared with those obtained by the CP/MAS technique on solid samples. The aromaticities were also measured for several Alberta plains coals. From the 1H solution spectra and 13C solid nmr spectra of asphaltenes, some of their skeletal features, not obtainable from solution spectra only, have been suggested. 相似文献
3.
John P. Hilton ThaiHuu Nguyen Mihaela Barbu Renjun Pei Milan Stojanovic Qiao Lin 《Microfluidics and nanofluidics》2012,13(5):749-760
We present a bead-based approach to microfluidic polymerase chain reaction (PCR), enabling fluorescent detection and sample conditioning in a single microchamber. Bead-based PCR, while not extensively investigated in microchip format, has been used in a variety of bioanalytical applications in recent years. We leverage the ability of bead-based PCR to accumulate fluorescent labels following DNA amplification to explore a novel DNA detection scheme on a microchip. The microchip uses an integrated microheater and temperature sensor for rapid control of thermal cycling temperatures, while the sample is held in a microchamber fabricated from (poly)dimethylsiloxane and coated with Parylene. The effects of key bead-based PCR parameters, including annealing temperature and concentration of microbeads in the reaction mixture, are studied to achieve optimized device sensitivity and detection time. The device is capable of detecting a synthetically prepared section of the Bordetella pertussis genome in as few as 10 temperature cycles with times as short as 15?min. We then demonstrate the use of the procedure in an integrated device; capturing, amplifying, detecting, and purifying template DNA in a single microfluidic chamber. These results show that this method is an effective method of DNA detection which is easily integrated in a microfluidic device to perform additional steps such as sample pre-conditioning. 相似文献
4.
M. Kohl M. Odehnal V. Petříěek R. Tichý S. Šafrata 《Journal of Low Temperature Physics》1988,72(3-4):319-343
We describe an apparatus allowing the observation of the NMR static longitudinal component of nuclear magnetizationM
z
by a SQUID at low magnetic fields and atT=4.2 K in Plexiglas, Teflon, and CaF2. The higher order NMR Larmor lines at 2f
0, 3f
0, and 4f
0, wheref
0 is the Larmor frequency of the allowed NMR line, were measured. These lines correspond to a flip of two, three, and four spins, respectively, by one photon. The amplitudes of 2f
0 and 3f
0 lines and their field dependences show that the common assertion that the forbidden lines at 2f
0 and 3f
0 appear in the same order of perturbation theory and that their intensity decreases with static magnetic fieldB
0 asB
0
–2
is wrong. In fact, the third Larmor line 3f
0 appears at higher order than the second Larmor line 2f
0 and its intensity decreases asB
0
–4
. This is also shown by a theoretical calculation of its intensity. For the first time the NMR SQUID technique allowed the detection of the 4f
0 line, corresponding to the simultaneous flip of four spins by one photon. 相似文献
5.
We report the observation of the dc and ac Josephson effect and quasiparticle tunnelling in the high-temperature superconductor YBaCuO. The observation is made at 4.2 K. These effects were observed in a junction made by a niobium tip pressed against a high-T
c
sample of YBaCuO ceramic. We observed a clean dc Josephson effect with a critical currentI
c
2 A and the ac effect with Shapiro steps corresponding toV=(hf/2e)n. The nature of the junction is not clear; however, we suggest that all observed effects can be explained by assuming a singlet pairing state in the ceramic. We have also observed a very peculiar noise behavior along theV-I characteristic. 相似文献
6.
7.
The main aim of this work was to study the effects of particle size, particle volume fraction, and matrix strength on the
long fatigue crack growth resistance of two different grades of Al alloys (Al2124-T1 and Al6061-T1) reinforced with SiC particles.
Basically, it was found that an increase in particle volume fraction and particle size increases the fatigue crack growth
resistance at near threshold and Paris regimen, with matrix strength having a smaller effect. Near final failure, the stronger
and more brittle composites are affected more by static modes of failure as the applied maximum stress intensity factor (K
max) approaches mode I plane strain fracture toughness (K
IC). 相似文献
8.
This paper presents a decentralized observer with a consensus filter for the state observation of discrete-time linear distributed systems. Each agent in the distributed system has an observer with a model of the plant that utilizes the set of locally available measurements, which may not make the full plant state detectable. This lack of detectability is overcome by utilizing a consensus filter that blends the state estimate of each agent with its neighbors’ estimates. It is proven that the state estimates of the proposed observer exponentially converge to the actual plant states under arbitrarily changing, but connected, communication and pseudo-connected sensing graph topologies. Except these connectivity properties, full knowledge of the sensing and communication graphs is not needed at the design time. As a byproduct, we obtained a result on the location of eigenvalues, i.e., the spectrum, of the Laplacian for a family of graphs with self-loops. 相似文献
9.
Petr Švec Atul Thakur Eric Raboin Brual C. Shah Satyandra K. Gupta 《Autonomous Robots》2014,36(4):383-405
The capability of following a moving target in an environment with obstacles is required as a basic and necessary function for realizing an autonomous unmanned surface vehicle (USV). Many target following scenarios involve a follower and target vehicles that may have different maneuvering capabilities. Moreover, the follower vehicle may not have prior information about the intended motion of the target boat. This paper presents a trajectory planning and tracking approach for following a differentially constrained target vehicle operating in an obstacle field. The developed approach includes a novel algorithm for computing a desired pose and surge speed in the vicinity of the target boat, jointly defined as a motion goal, and tightly integrates it with trajectory planning and tracking components of the entire system. The trajectory planner generates a dynamically feasible, collision-free trajectory to allow the USV to safely reach the computed motion goal. Trajectory planning needs to be sufficiently fast and yet produce dynamically feasible and short trajectories due to the moving target. This required speeding up the planning by searching for trajectories through a hybrid, pose-position state space using a multi-resolution control action set. The search in the velocity space is decoupled from the search for a trajectory in the pose space. Therefore, the underlying trajectory tracking controller computes desired surge speed for each segment of the trajectory and ensures that the USV maintains it. We have carried out simulation as well as experimental studies to demonstrate the effectiveness of the developed approach. 相似文献
10.
Bohdan Schneider Jan Štokr Pavel Schmidt Marian Mihailov Stoil Dirlikov Nadezhda Peeva 《Polymer》1979,20(6):705-712
Infrared and Raman spectra of atactic PMMA and infrared spectra of stereoregular PMMA and of its four deuterated derivatives , were measured. They were used to assign the bands of stretching and deformation vibrations of CH2, CCH3 and OCH3 groups in the infrared and Raman spectra and to discuss the effect of stereoregularity on these bands in the infrared spectra. 相似文献