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1.
An on-line, steam distillation/purge and trap gas chromatographic procedure is described for determination of halogenated analytes in foods and beverages. Recoveries were generally >80% (versus aqueous standards) from vegetable oil, flour, root beer, cream (10% butter fat), and milk spiked at 1-3 micrograms/kg for each of the 32 analytes studied. Analytes ranged in volatility from vinyl chloride to 1,2,3,4-tetrachlorobenzene. Repeatabilities from aqueous standards were <10% for most analytes. For a 1 g food sample, method detection limits ranged from 0.02 to 0.2 micrograms/kg for the 32 analytes. Reduced recoveries for less volatile analytes, however, occurred when steam-distillable, nonpolar food components were carried to the sparger. This effect was observed for citrus beverages containing steam-volatile limonene, roasted and ground coffees, and some salad dressings. The method was applied to a variety of foods. 相似文献
2.
Jacquet Philippe Minet Pascale Mühlethaler Paul Rivierre Nicolas 《Wireless Personal Communications》1997,4(1):51-63
Radio LANs are emerging in the computing world. They are supported by distinct configurations: on the one hand radio LANs with base stations and a wired backbone, on the other hand radio LANs implementing Intra-forwarding. Adding a new node in a radio LAN with Intra-forwarding, increases the reliability, while this reliability decreases with ad hoc or hub configurations. This advantage of Intra-forwarding is quantified. Intra-forwarding, as defined in the HIPERLAN standard, is based on a hop-by-hop policy and link check procedures. It is shown how point-to-point packets and broadcast packets are forwarded. The three basic components of Intra-forwarding needed to build and update the Intra-forwarding database are described. The originality of this approach is the use of multipoint relays which enable better scalability. The correctness of the Intra-forwarding protocol is proved and its cost is evaluated. 相似文献
3.
Mostafa Moussaid Stphane Caillet Josphine Nketsia‐Tabiri Cheikh Boubekri Monique Lacroix 《Journal of the science of food and agriculture》2004,84(13):1657-1662
The study evaluated the effects of waxing, irradiation dose and post‐irradiation storage time on the essential oils in orange peel. Mature oranges (Maroc late) waxed or unwaxed were treated with 1 or 2 kGy radiation and stored for 9 weeks at 20 °C and 40–50% RH. Essential oils from the peel were extracted and analysed by GC. Results showed that D ‐limonene was significantly lower in waxed oranges; levels in samples treated with 2 kGy were higher than those in non‐irradiated or treated with 1 kGy. Linalool, methyl anthranilate and 3,7‐dimethyl‐2,6‐octadienal decreased as the dose increased. Levels of linalool increased with storage time but D ‐limonene was unaffected. These results may aid in guaranteeing the quality of orange essential oils during storage time. Copyright © 2004 Society of Chemical Industry 相似文献
4.
F Proulx J Lacroix IA Qureshi D Nadeau M Gauthier M Lambert 《Canadian Metallurgical Quarterly》1997,156(11):864-869
In order to characterize the role of carnitine during metabolic stress, we prospectively determined carnitine profiles in plasma and urine on admission, days 2, 5, 10 and 15, among 28 critically ill children free of any known conditions associated with secondary carnitine deficiency. More than 25% of plasma and 50% of urinary carnitine measurements were abnormal; 96% (27/28) of patients displayed on at least one occasion an abnormal [< -2 SD or > +2 SD] carnitine value in plasma. Three children had extremely low [< 10 micromol/l] free carnitine (FC) levels in plasma. Plasma esterified and FC levels on admission were not related to the risk of mortality [PRISM score], to muscle lysis [CK values], and to the caloric intake. Levels of FC and esterified carnitine in plasma were unrelated to those measured in urine. Conclusion: Abnormal plasma and urine carnitine measurements are frequently found in critically ill children; the biological significance of these perturbations remains unclear. Caution must be exercised before concluding that an abnormal carnitine value is indicative of an underlying hereditary metabolic disorder in this population. 相似文献
5.
DV Matei F Pascale A Clemente F Della Corte D Pucello F Grassetti 《Canadian Metallurgical Quarterly》1996,20(3):302-306
Since in vitro experiments had excluded interactions between Fe-gluconate (Fe-gluc) and magnesium-L-aspartate hydrochloride (MAH) in aqueous solutions the present in vivo studies seemed to be justified. Animal studies: Rats were kept on magnesium-(Mg)- and iron-(Fe)- sufficient and deficient diets. The intragastral administration of Fe-gluc significantly increased plasma Fe after 3 h, either given alone, or in combination with MAH (inducing hypermagnesemia). Same results were obtained when fortified diets were offered to Fe/Mg-deficient animals. Human studies: The combination of Fe-gluc (2 x 50 mg Fe per day, per os) plus MAH (2 x 7.5 mmol Mg per day, p.o.) was well tolerated by healthy volunteers. Single dose experiments revealed that Fe-gluc alone and in combination with MAH increased plasma Fe levels during 3 h to the same extent. Two groups of pregnant women with moderately reduced hemoglobin levels either received Fe-gluc (out-patients) or its combination with MAH (at least temporarily hospitalised because of preterm labor). Treatments were well tolerated. Hemoglobin levels did not further decrease, as expected without Fe supplements, during the course of pregnancy, thus indicating the therapeutic availability of the electrolytes in both study groups. Progesterone-induced constipation is frequently observed during pregnancy; hence stool softening reported by 50% of the women receiving Fe-gluc plus MAH (versus 33% in the Fe-gluc group) can be regarded as desirable effect. It is concluded that MAH does not interfere with the enteral absorption of Fe-gluc when both electrolytes are orally administered together. Taking both electrolytes together instead of 2 to 3 h apart from each other, as actually recommended, means a less complicated dosage regimen and probably improves compliance. 相似文献
6.
Jacques Hernigou Pascale Vertongen Joanne Rasschaert Philippe Hernigou 《International journal of molecular sciences》2021,22(8)
The value of bone marrow aspirate concentrates for treatment of human knee cartilage lesions is unclear. Most of the studies were performed with intra-articular injections. However, subchondral bone plays an important role in the progression of osteoarthritis. We investigated by a literature review whether joint, subchondral bone, or/and scaffolds implantation of fresh autologous bone marrow aspirate concentrated (BMAC) containing mesenchymal stem cells (MSCs) would improve osteoarthritis (OA). There is in vivo evidence that suggests that all these different approaches (intra-articular injections, subchondral implantation, scaffolds loaded with BMAC) can improve the patient. This review analyzes the evidence for each different approach to treat OA. We found that the use of intra-articular injections resulted in a significant relief of pain symptoms in the short term and was maintained in 12 months. However, the clinical trials indicate that the application of autologous bone marrow concentrates in combination with scaffolds or in injection in the subchondral bone was superior to intra-articular injection for long-term results. The tendency of MSCs to differentiate into fibrocartilage affecting the outcome was a common issue faced by all the studies when biopsies were performed, except for scaffolds implantation in which some hyaline cartilage was found. The review suggests also that both implantation of subchondral BMAC and scaffolds loaded with BMAC could reduce the need for further surgery. 相似文献
7.
Pascale Sabin Bouchra Benjelloun-Mlayah Michel Delmas 《Journal of the American Oil Chemists' Society》1997,74(5):481-489
Two sets of alkyd resins of variable oil lengths with the required properties for offset printing ink formulations, modified
by sunflower and rapeseed oil, were synthetized according to the “monoglyceride” process. The influence of the acyl composition
of the modifying vegetable oil and of the oil content on alkyds’ properties was determined by detailed chemical and rheological
characterization. Molecular structure, size, and molecule size distribution appeared to be linked to these two factors. A
comparative study with two usual linseed oil-modified alkyds led to determination of the more appropriate alkyds for applications
in offset varnishes. 相似文献
8.
Kobus Barnard Quanfu Fan Ranjini Swaminathan Anthony Hoogs Roderic Collins Pascale Rondot John Kaufhold 《International Journal of Computer Vision》2008,77(1-3):199-217
We present a new data set of 1014 images with manual segmentations and semantic labels for each segment, together with a methodology
for using this kind of data for recognition evaluation. The images and segmentations are from the UCB segmentation benchmark
database (Martin et al., in International conference on computer vision, vol. II, pp. 416–421, 2001). The database is extended by manually labeling each segment with its most specific semantic concept in WordNet (Miller et al.,
in Int. J. Lexicogr. 3(4):235–244, 1990). The evaluation methodology establishes protocols for mapping algorithm specific localization (e.g., segmentations) to our
data, handling synonyms, scoring matches at different levels of specificity, dealing with vocabularies with sense ambiguity
(the usual case), and handling ground truth regions with multiple labels. Given these protocols, we develop two evaluation
approaches. The first measures the range of semantics that an algorithm can recognize, and the second measures the frequency
that an algorithm recognizes semantics correctly. The data, the image labeling tool, and programs implementing our evaluation
strategy are all available on-line (kobus.ca//research/data/IJCV_2007).
We apply this infrastructure to evaluate four algorithms which learn to label image regions from weakly labeled data. The
algorithms tested include two variants of multiple instance learning (MIL), and two generative multi-modal mixture models.
These experiments are on a significantly larger scale than previously reported, especially in the case of MIL methods. More
specifically, we used training data sets up to 37,000 images and training vocabularies of up to 650 words.
We found that one of the mixture models performed best on image annotation and the frequency correct measure, and that variants
of MIL gave the best semantic range performance. We were able to substantively improve the performance of MIL methods on the
other tasks (image annotation and frequency correct region labeling) by providing an appropriate prior. 相似文献
9.
A. Ritacco R. Adam A. Adane P. Ade P. André A. Beelen B. Belier A. Benoît A. Bideaud N. Billot O. Bourrion M. Calvo A. Catalano G. Coiffard B. Comis A. D’Addabbo F.-X. Désert S. Doyle J. Goupy C. Kramer S. Leclercq J. F. Macías-Pérez J. Martino P. Mauskopf A. Maury F. Mayet A. Monfardini F. Pajot E. Pascale L. Perotto G. Pisano N. Ponthieu M. Rebolo-Iglesias V. Revéret L. Rodriguez G. Savini K. Schuster A. Sievers C. Thum S. Triqueneaux C. Tucker R. Zylka 《Journal of Low Temperature Physics》2016,184(3-4):724-732
10.
Daniel Cosmin Porumbel Jin-Kao Hao Pascale Kuntz 《Computers & Operations Research》2010,37(4):769-778
We present a search space analysis and its application in improving local search algorithms for the graph coloring problem. Using a classical distance measure between colorings, we introduce the following clustering hypothesis: the high quality solutions are not randomly scattered in the search space, but rather grouped in clusters within spheres of specific diameter. We first provide intuitive evidence for this hypothesis by presenting a projection of a large set of local minima in the 3D space. An experimental confirmation is also presented: we introduce two algorithms that exploit the hypothesis by guiding an underlying Tabu Search (TS) process. The first algorithm (TS-Div) uses a learning process to guide the basic TS process toward as-yet-unvisited spheres. The second algorithm (TS-Int) makes deep investigations within a bounded region by organizing it as a tree-like structure of connected spheres. We experimentally demonstrate that if such a region contains a global optimum, TS-Int does not fail in eventually finding it. This pair of algorithms significantly outperforms the underlying basic TS algorithm; it can even improve some of the best-known solutions ever reported in the literature (e.g. for dsjc1000.9). 相似文献