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排序方式: 共有223条查询结果,搜索用时 15 毫秒
1.
Quality of Crude Fish Oil Extracted from Herring Byproducts of Varying States of Freshness 总被引:1,自引:0,他引:1
ABSTRACT: Herring byproducts were stored at 2 and 15 °C for up to 72 h. Over time, significant increases of total volatile bases (TVB), histamine, putrescine, cadaverine, and tyramine were detected. However, only tyramine and TVB levels were temperature-dependent. The level of total polyunsaturated fatty acids (PUFAs) was constant. Longer byproducts storage gave rise to an oil with higher levels of free fatty acids, eicosapentaenoic acid (EPA), docosahexaenoic acid (DHA), and total PUFAs, while fluorescent compounds were lower. A higher storage temperature led to oil higher in α-tocopherol and EPA levels and lower in anisidine value. Surprisingly, the oil with the highest content of PUFAs was not produced from the freshest byproducts, and oil with low oxidation products can be extracted from stored byproducts. 相似文献
2.
I. Aidos N. Kreb M. Boonman J.B. Luten R.M. Boom A. Van Der Padt 《Journal of food science》2003,68(2):581-586
ABSTRACT: A pilot plant used for upgrading herring byproducts into fish oil was analyzed on its operational efficiency and product quality. The temperature of the heat exchanger and the speeds of the pump and the 3-phase decanter were varied according to a 23 fractional factorial design. The initial amount of oxidation products present in the crude oil, its storage stability, and the yields from the different obtained products were determined. Multivariate data analysis of the advanced screening stage showed that T had neither influence on the quality nor on the yield in contrast to D and MP (P < 0.05). Process optimization results showed that the quality of the oil was influenced by an interaction effect between the speed of the MP and the D. Oils processed with the highest MP speed were the most stable during storage. 相似文献
3.
C Jurinke B Z?llner HH Feucht D van den Boom A Jacob S Polywka R Laufs H K?ster 《Canadian Metallurgical Quarterly》1998,14(3):97-102
DNA preparations from three different groups of serum samples were examined for HBV-DNA via a nested polymerase chain reaction assay (lower detection limit: 10 viral genomes in 100 microliters serum): Group I consisted of 11 uninfected control sera, group II consisted of sera obtained from 11 HBV infected patients and group III consisted of 21 isolated anti-HBc positive samples. The 21 samples from group III were HBV-DNA negative according to a conventional non-nested PCR assay and hybridization with a 32P-labelled probe. Using nested PCR and mass spectrometry, HBV-DNA was detected in none of group I and in all of group II samples. In 11 out of 21 (52%) of the isolated anti-HBc positive sera from group III, HBV-DNA was detected. No correlation was observed between HBV-DNA positivity and anti-HBc titers. Matrix-assisted laser desorption/ionization time-of-flight (MALDI-TOF) mass spectrometry provided a fast, sensitive and non-radioactive assay for the detection of PCR products without the need for gel electrophoresis or hybridization with labelled probes. 相似文献
4.
The influence of nonsolvent, crystallinity of the polymer film, and addition of dodecane (a poor solvent for the polymer and for the nonsolvent) on the morphology of polylactides films has been investigated and was related to phase separation behavior. Both amorphous poly‐DL ‐lactide (PDLLA) and crystalline poly‐L ‐lactide (PLLA) were dissolved in dichloromethane, and subsequently films were made by immersion in nonsolvent baths. PDLLA gave dense films without any internal structure, since the structure was not solidified by crystallization or glassification. PLLA films show varying structure depending on the nonsolvent. With methanol, asymmetric morphologies were observed as a result from combined liquid‐liquid demixing and crystallization, while with water symmetric spherulitic structures were formed. As a next step, dodecane was added, which is not miscible with the nonsolvent, and we found it to have a strong influence on the morphology of the films. The PDLLA films with dodecane did not collapse: a closed cell structure was obtained. In PLLA films, dodecane speeds up phase separation and induces faster crystallization in the films, and the porosity, size of the pores, and interconnectivity increased. When the PLLA solutions were subjected to a heat pretreatment, crystallization could be postponed, which yielded a cellular structure around dodecane, which did not contain spherulites anymore. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 959–971, 2007 相似文献
5.
Global outsourcing is a growing trend among independent software vendors. In these projects like other distributed work, distances have negative effects on communication and coordination, directly impacting performance. We present a normative model designed to address this issue by improving communication and knowledge exchange. The model consists of six distinct practices and a tool blueprint, each coming with practical guidelines. It is based in part on two case studies of Dutch software vendors who have successfully outsourced part of their activities to an Eastern European outsourcing vendor, and validated by a panel of six experts from industry and the scientific community. It is concluded that knowledge exchange in global software outsourcing is a by‐product of efforts to enhance communication and coordination, rather than specific technical solutions. By committing to sharing knowledge, emphasizing transparency and integrating the outsourcing team into their organizations, customers from the product software business can realize the benefits of global outsourcing. 相似文献
6.
Verhelst SH Michiels PJ van der Marel GA van Boeckel CA van Boom JH 《Chembiochem : a European journal of chemical biology》2004,5(7):937-942
Aminoglycoside antibiotics, which are able to selectively bind to RNA, are considered to be an important lead in RNA-targeting drug discovery. In this study, surface plasmon resonance (SPR) was employed to explore the interaction of aminoglycosides with known tobramycin-binding RNA hairpins (aptamers) and an unrelated RNA hairpin. It was established that aminoglycosides have multiple interactions with RNA hairpins. Unexpectedly, the different hairpins showed comparable affinity for a set of related aminoglycosides. The observed absence of selectivity presents an extra hurdle in the discovery of novel aminoglycosides as specific drugs that target defined RNA hairpins. 相似文献
7.
Although many different methods for microencapsulation are known only some of them had been applied at industrial scale, due to complexity, lack of mechanical strength of the resulting capsules, and the costs related to their production. One of such methods is the electrostatic layer-by-layer (LbL) adsorption, which produce shells from oppositely charged polymers. The thickness of those shells can be tuned with nanometric precision, but to build enough strength for practical applications requires the adsorption of an impractical number of layers. We present here a method to produce strong microcapsules combining the assembly of a protein/pectin shell via electrostatic LbL adsorption with the adsorption of bigger charged colloidal particles. Those colloidal particles do not need any pretreatment to modify their wettability, as would be the case for a standard colloidosome route. In this way strong encapsulates with porous walls are obtained, which can be used as easy to load scaffolds. The pores in the walls can be closed through subsequent adsorption of more layers of protein and pectin. Since the assembly scheme occurs at pH 3.5 we expect the produced microcapsules to act as an effective delivery system in food products, protecting their contents from the acidity of the stomach and dissolving later at the small intestine. The proteins and pectins used as basic building blocks are food-grade and inexpensive. 相似文献
8.
Jimmy Perdana Martijn B. Fox Maarten A. I. Schutyser Remko M. Boom 《Food and Bioprocess Technology》2013,6(4):964-977
The inactivation of bioactive ingredients during spray drying is often matrix specific. Therefore, the design of new processes or the optimisation of existing spray drying processes is usually highly product specific and requires numerous experiments. Rapid experimentation methods that facilitate fast data generation are therefore desired. A novel method for drying single droplets to mimic spray drying is proposed. The approach involves droplet deposition on a hydrophobic flat surface followed by controlled drying. A heat and mass transfer model is applied to predict the drying history of the single droplets. The approach is successfully evaluated through studying the inactivation of β-galactosidase during drying. The heat and mass transfer model supplemented with inactivation kinetics provided reasonable prediction of the residual enzyme activity after drying. In addition, the inactivation kinetics could be directly extracted from single droplet experiments rather than using the kinetics from separate heating experiments. Finally, it was demonstrated that the inactivation kinetics found with the single-drop experiments could satisfactorily predict the residual activity of β-galactosidase dried with a laboratory-scale spray dryer. 相似文献
9.
Heinz-Bernhard Kraatz Milko E. van der Boom Yehoshoa Ben-David David Milstein 《Israel journal of chemistry》2001,41(3):163-172
The reaction of the PCP-type complex Pd(Me){2,6-(iPr2PCH2)2C6H3}( 3 ) with phenyl iodide results in the formation of Pd(I){2,6-(iPr2PCH2)2C6H3} ( 5 ), methyl iodide, toluene, and biphenyl. Formation of Pd(Ph){2,6-(iPr2PCH2)2C6H3}( 4 ) is observed during the reaction by 31P NMR. Reaction of 4 with aryl iodides results in the formation of 5 and Ph–Ph, Ph–Ar, and Ar–Ar, products indicative of a radical reaction. Under pseudo-first-order conditions, the rates of the reactions follow the order p-OMe > p-Me > H > p-NO2 > m-Cl. The reaction is likely to involve electron transfer from 4 to the aryl iodide followed by fast decomposition of a postulated radical cation [Pd(Ph){2,6-(iPr2PCH2)2C6H3}]+. ( 4 +.) to give a phenyl radical and [Pd{2,6-(iPr2PCH2)2C6H3}]+ ( 6 +). Facile decomposition of the aryl iodide radical anion generates an aryl radical and I−. Recombination of aryl radicals gives rise to mixed biaryls, and 6 + combines with I− to give 5 . 相似文献
10.
Guoliang Zhu Yongbing Dai Da Shu Yanping Xiao Yongxiang Yang Jun Wang Baode Sun Rob Boom 《Intermetallics》2011,19(7):1036-1040
First-principles calculations were employed to study the migration of vacancy in clean and Si-doped Al3Ti. The effect of Si doping on the formation of vacancy and the diffusion of doped-Si atom in the Al3Ti were also investigated. It is found that, under Al-rich condition, the formation energies of Al vacancies in Al3Ti with Si doping are decreased compared with those in clean Al3Ti. The preferred migration paths of vacancies are not changed when Si occupies Al site, but the migration energy barriers for the majority of paths are decreased after Si doping. The doped-Si atom on Al site prefers to diffuse via the nearest Al vacancy. 相似文献