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Polymerization of β,β′-(ethylenedithio)dipropionitrile 1 IUPAC name: 4,7-dithiadecane dinitrile. with formaldehyde in the presence of sulfuric acid was carried out in order to permit the synthesis of polymides containing thioether groups. The obtained poly(amide thioether)s were characterized; they coordinate mercury (II) with a high degree of selectivity. 相似文献
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Yi-Ou Li Tom Eichele Vince D. Calhoun Tulay Adali 《Journal of Signal Processing Systems》2012,68(1):31-48
In this work, we apply a novel statistical method, multiset canonical correlation analysis (M-CCA), to study a group of functional
magnetic resonance imaging (fMRI) datasets acquired during simulated driving task. The M-CCA method jointly decomposes fMRI
datasets from different subjects/sessions into brain activation maps and their associated time courses, such that the correlation
in each group of estimated activation maps across datasets is maximized. Therefore, the functional activations across all
datasets are extracted in the order of consistency across different dataset. On the other hand, M-CCA preserves the uniqueness
of the functional maps estimated from each dataset by avoiding concatenation of different datasets in the analysis. Hence,
the cross-dataset variation of the functional activations can be used to test the hypothesis of functional-behavioral association.
In this work, we study 120 simulated driving fMRI datasets and identify parietal-occipital regions and frontal lobe as the
most consistently engaged areas across all the subjects and sessions during simulated driving. The functional-behavioral association
study indicates that all the estimated brain activations are significantly correlated with the steering operation during the
driving task. M-CCA thus provides a new approach to investigate the complex relationship between the brain functions and multiple
behavioral variables, especially in naturalistic tasks as demonstrated by the simulated driving study. 相似文献
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Tulay Y. İnan Emel Yıldız Birsen Karaca Hacer Dogan Alican Vatansever Muhammed Nalbant Koray Eken 《Journal of materials science. Materials in medicine》2014,25(8):2027-2039
We produced UV curable lenses with properties blocking short wave UV light. In the UV-curable formulations, we used an oligomer (Ac-PEEK) with another urethan oligomer (Mw = 2000). Radically active, molecular weight controlled Ac-PEEK was obtained by reacting 2-hydroxyl ethyl methacrylate with molecular- weight- controlled and isocyanate terminated PEEK (Mn = 4500). We characterized all synthesized monomer, oligomer and optical materials with UV/Vis spectrophotometer with interferogram, elemental analyser, mass spectrophotometer, proton nuclear magnetic resonance, Fourier transform infrared spectroscopy, thermal gravimetric analyzer, differential scanning calorimeter, scanning electron microscopy and gas chromatography. Results suggested that newly synthesized oligomer with the structure of PEEK absorbs short wave UV-light. Ageing tests [ISO 11979-5, Ophthalmic implants—intraocular lenses (IOL)—Part 5: Biocompatibility] performed on the IOL materials were successful. High contact angle of the obtained lenses suggests that all lenses were hydrophobic and SEM results revealed that lenses are morphologically homogeneous. Based on all positive properties just mentioned, we safely conclude that the lenses produced in this study are very promising for IOL production. 相似文献
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The historic Hagia Sophia in Istanbul, which held the record as the world's largest domed building for some 800 years, is analysed with a finite element formulation, including the effects of thickness shear deformations and the term z/R, to understand its structural behaviour under the action of static loading. The structure, including all essential elements of the system, is modelled by using the same curved trapezoidal finite element with 40 degrees of freedom. Its structural behaviour and its structural load carrying system are demonstrated and the results are compared with those obtained earlier and also with those observed at the structure. 相似文献
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The Hagia Sophia, a 6th century masonry edifice in Istanbul, is analysed with a linear finite element model including thickness shear deformations, the terms z/R, and rotatory inertia effects with consistent mass matrix to provide insight to the structure's behaviour under earthquake loading. The structure, including the primary main dome and supporting system, is modelled by using a two-dimensional model composed of eight-node shell element. The dynamic characteristics of the system are obtained by using the Wilson-θ method, step-by-step integration method, and also by applying the available ground motion data to understand its general structural behaviour in the future earthquakes. 相似文献
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In this study, different vegetable‐fibre enriched yoghurts namely control (C), pumpkin (PY), carrot (CY), green pea (GY) and zucchini (ZY), were produced. It was observed that Streptococcus thermophilus and Lactobacillus delbrueckii subsp. bulgaricus counts were higher in yoghurts supplemented with vegetable purees, in accordance with the enhanced growth of lactic acid bacteria due to the fibres, phenolic compounds and organic acids present in the vegetables. Furthermore, vegetable puree supplementation affected the pH, titratable acidity, syneresis, colour (L*, a*, b*, ΔE values), texture (firmness, cohesiveness, consistency and viscosity index) and sensorial properties of the yoghurts. Firmness, consistency and viscosity indices were higher in the yoghurt produced with carrot puree, whereas the highest antioxidant capacity was detected in the pumpkin yoghurt, which corresponded to the highest total phenolic, ascorbic acid and total carotenoid contents. The results of the present study could lead to an innovative approach in the functional dairy product market for the development of dairy products enriched with vegetables that have nutritional and potential therapeutic characteristics. 相似文献