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以间乙酰氨基苯胺、3-氨基-4-甲氧基乙酰苯胺为原料,氯乙酸甲酯和氯乙酸乙酯为烷基化试剂,研究了催化剂种类、缚酸剂种类、反应时间和加料方式对反应的影响,并对合成的四个N,N-二乙酸酯基芳香胺系列染料中间体进行了结构表征。结果表明:Na Br和Na_2CO_3分别是催化该类反应合适的催化剂和缚酸剂。当芳香胺:氯乙酸酯:碳酸钠为1:4:1. 1(mol),在回流反应2h后加入10%的催化剂溴化钠和0. 5%抗氧化剂(m),再进行分水回流反应2h,得纯度99%(HPLC)、收率98%以上的N,N-二乙酸酯基芳香胺系列染料中间体。经紫外光谱、红外光谱、核磁共振氢谱和质谱分析,所合成的四个N,N-二乙酸酯基芳香胺系列染料中间体为目标产物。 相似文献
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The volatile oil of leaves and barks of Calycopteris floribunda was examined by gas chromatography-mass spectrometry (GC-MS). 52 volatile chemical components in leaves were identified.
The antimicrobial assay of oils in the leaves and barks was carried out by disk diffusion method in vitro. The major components (mass fraction) in leaves are caryophyllene oxide (13.79%), n-hexadecanoic acid (11.91%) and β-caryophyllene (10.45%). Ten constituents are identified accounting for about 99.98% of the total volatile oil in the bark.
Among these components, n-hexadecanoic acid (59.18%), linolic acid (12.70%) and butyl octyl phthalate (8.21%) are the major constituents. The oils
exhibit strong antimicrobial activity and display more potent against bacteria than fungi. 相似文献
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通过对照学习新、旧《水法》,结合南宁市的一些实际情况,就如何贯彻落实新《水法》,在做好新《水法》宣传、搞好中长期规划、加大基础设施建设投入、做好节水工作,加大水利工程改革力度、完善法规配套建设、建设高素质水政队伍,加大执法力度等方面工作内容提出了建议。 相似文献
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