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由于银与高定向热解石墨(highly oriented pyrolytic graphite,HOPG)面间的相互作用很小,银在HOPG表面上的生长通常采取三维的Volmer-Weber模式,得到空间分布不均匀的银团簇。本文分别采用加热氧化和氩离子轰击来改变HOPG衬底的表面结构,并用扫描隧道显微镜(STM)研究了银在它们上面的生长过程。实验结果表明:在氩离子轰击过的HOPG表面上,可以得到大小基本一致、空间分布均匀的银纳米团簇,实现了银团簇的控制生长.氩离子轰击导致了平整的HOPG表面产生缺陷,这些缺陷对银原子的扩散进行限制并成为优先成核中心,最终形成均匀的银纳米团簇。 相似文献
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Well-aligned carbon nitrogen nanotube films have been synthesized successfully on meso-porous silica substrates by microwave plasma chemical vapor deposition (MWPCVD) method. Studies on their morphology, structure, and composition by scanning electron microscopy (SEM), transmission electron microscopy (TEM), and energy dispersive X-ray spectroscopy (EDX), respectively, indicate that these nanotubes consist of linearly polymerized carbon nitrogen nanobells, and the nitrogen atoms have been doped into carbon netweork to form a new structure C1-xNx( x = 0.16±0.01). X-ray photoelectron spectroscopy (XPS) results of the samples further demonstrate that carbon bonds cova-lently with nitrogen in all the carbon nitrogen nanotube films. 相似文献
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