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首先提出射频反应磁控溅射中薄膜沉积速率同O2流量和溅射功率关系的理论计算模型;其次根据这一理论计算模型,在O2/Ar气氛中,利用射频反应磁控溅射制备氧化铁镍薄膜;最后分别采用台阶仪、X射线衍射(XRD)、X射线光电子能谱(XPS)、电子扫描镜(SEM)和电化学工作站对薄膜进行了表征,并分析了在制备过程中O2含量、工作压强和溅射功率对薄膜的沉积速率、结构、组分和表面形貌的影响.实验验证了所提出的理论计算模型以及Ni3 的存在;得到了膜厚与晶型以及工作压强与形貌的关系;电化学测试结果为:在电流密度为8 mA/cm2时的过电势为284 mV. 相似文献
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ZnO nanocrystals doped with trivalent europium ions (Eu3+) and dysprosium ions (Dy3+) were synthesized by the pre- cipitation method. The structural and optical properties of the samples are investigated by the X-ray diffraction (XRD) and photoluminescence (PL). The results show that rare earth ions are incorporated into the lattice of ZnO, and the combination of blue, green and red emissions can be obtained. Specially, the emission can be obtained even under the nonresonant excitation of 320 nm, which is explained based on the energy transfer. The concentration quenching mechanism is also presented in this paper. 相似文献
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One dimension (1D) ordered titanium dioxide (TiO2) nanostructured photocatalysts sensitized by quantum dots (QDs) are fabricated. Their morphologies, crystal structures and photocatalytic properties are characterized by scanning elec-tron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD) and ultraviolet-visible-near infrared (UV-vis-NIR) absorption spectroscopy, respectively. Compared with the original TiO2 nanostructure, the nanostructured TiO2 sensitized by QDs exhibits a good photocatalytic activity for the degradation of methyl orange (MO). The QDs with core-shell structure can reduce the photocatalytic ability due to the higher potential barrier of carrier transport in ZnS shell layer. The results indicate that the proposed photocatalyst shows promising potential for the application in organic dye degradation. 相似文献
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合成了一种新型的共掺杂稀土Eu-Gd配合物Gd0.5Eu0.5(TTA)3Dipy,将其作为红光发射材料制备了结构为ITO/PVK:Gd0.5Eu0.5(TTA)3Dipy/PBD/Al的有机电致发光薄膜器件,得到了单色性好的红色有机电致发光器件,器件的开启电压为9 V,在16 V时达到最大亮度109 nit.研究了Eu-Gd配合物与PVK共掺杂体系的激发光谱和光致发光谱,结果发现两者间存在着能量转移,表明Gd3 的存在促进了PVK到Eu3 的能量传递. 相似文献
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比较多种检测技术的优缺点;对埋地油气长输钢质管道腐蚀状况进行评价,以便及时有效地维护管道,避免油气输送事故发生,延长管道使用寿命。 相似文献
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