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Hydrolysis of titanium alkoxide and effects of hydrolytic polycondensation parameters 总被引:7,自引:0,他引:7
Bulent E. Yoldas 《Journal of Materials Science》1986,21(3):1087-1092
Titanium alkoxides hydrolyse vigorously with water producing polycondensates whose equivalent oxide content varies from 70% to over 90%. This variation reflects the average molecular size and the nature of the terminal bonds. Hydrolysis conditions also affect the molecular and particle morphologies modifying the crystallization and sintering behaviour of oxide materials derived from polycondensates. It is also possible to form clear polymer solutions under excess water hydrolysis with the addition of certain acids. Investigations show that there is a window in the acid concentration which provides long-term solution stability. The gels formed from these clear solutions shrink in their liquor under certain conditions and the introduction of hydrogen peroxide into the liquor (surrounding the gel) causes vigorous gel shrinkage. 相似文献
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Bulent I. Dervisoglu 《Journal of Electronic Testing》1991,2(1):107-115
The architecture and some of the specific features of a Scan and Clock Resource (SCR) chip are described. This chip is currently being used in a high-end workstation product to provide access to the testability features of the individual chips and/or printed circuit boards. Using a board-level controller to gain access to the testability features of system components and interfacing the controller to a diagnostics processor (or external tester) is emerging as a common strategy for designing testable digital systems. Based upon experience gained from such an application, controller features that are deemed useful are discussed.This paper is an enhanced version of the author's earlier paper titled Towards a Standard Approach for Controlling Board-Level Test Functions, presented at the IEEE International Test Conference, ITC'90, Washington D.C., September 1990. 相似文献
4.
Peri SR Akgun B Satija SK Jiang H Enlow J Bunning TJ Foster MD 《ACS applied materials & interfaces》2011,3(9):3375-3383
Tailoring the structure of films deposited by plasma-enhanced chemical vapor deposition (PECVD) to specific applications requires a depth-resolved understanding of how the interface structures in such films are impacted by variations in deposition parameters such as feed position and plasma power. Analysis of complementary X-ray and neutron reflectivity (XR, NR) data provide a rich picture of changes in structure with feed position and plasma power, with those changes resolved on the nanoscale. For plasma-polymerized octafluorocyclobutane (PP-OFCB) films, a region of distinct chemical composition and lower cross-link density is found at the substrate interface for the range of processing conditions studied and a surface layer of lower cross-link density also appears when plasma power exceeds 40 W. Varying the distance of the feed from the plasma impacts the degree of cross-linking in the film center, thickness of the surface layer, and thickness of the transition region at the substrate. Deposition at the highest power, 65 W, both enhances cross-linking and creates loose fragments with fluorine content higher than the average. The thickness of the low cross-link density region at the air interface plays an important role in determining the width of the interface built with a layer subsequently deposited atop the first. 相似文献
5.
Songül Cakmakci Engin Gundogdu Ali A. Hayaloglu Elif Dagdemir Mustafa Gurses Bulent Cetin Deren Tahmas‐Kahyaoglu 《International Journal of Food Science & Technology》2012,47(11):2405-2412
The objective of this study is to characterise the gross chemical and microbiological status and identify the volatile compounds of mouldy Civil cheeses. A total of forty‐one samples were surveyed, and gross compositional status of the cheeses was (as mean values): 6.5 for pH, 6.2% for fat‐in‐dry matter, 51.8% for moisture and 15.3% for water‐soluble nitrogen (as% of total nitrogen). Chemical composition of the cheese samples varied widely. Mouldy Civil cheese has similar pH values and moisture contents when compared with blue‐type cheeses, but it has distinct feature for fat contents. The microbiological counts of the samples were found to be high and some samples contained coliform bacteria. A total of 95 volatiles, including esters (28), acids (6), ketones (12), aldehydes (3), alcohols (15), terpenes (10), sulphur compounds (3) and miscellaneous (18), were identified in the volatile fractions of the cheeses, and principal volatile groups were esters, alcohols and ketones. 相似文献
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Songul Cakmakci Ali A Hayaloglu Elif Dagdemir Bulent Cetin Mustafa Gurses Deren Tahmas‐Kahyaoglu 《International Journal of Dairy Technology》2014,67(4):594-603
Four different types of mould‐ripened Civil cheese were manufactured. A defined (nontoxigenic) strain of a Penicillium roqueforti (SC 509) was used as the secondary starter with and without addition of the whey cheese (Lor); in parallel, secondary starter‐free counterparts were manufactured. Chemical composition, microbiology and proteolysis were studied during the ripening. The incorporation of whey cheese in the manufacture of mould‐ripened Civil cheese altered the gross composition and adversely affected proteolysis in the cheeses. The inoculated P. roqueforti moulds appeared to grow slowly on those cheeses, and little proteolysis was evident in all cheese treatments during the first 90 days of ripening. However, sharp increases in the soluble nitrogen fractions were observed in all cheeses after 90 days. Microbiological analysis showed that the microbial counts in the cheeses were at high levels at the beginning of ripening, while their counts decreased approximately 1–2 log cfu/g towards the end of ripening. 相似文献
8.
Iranian Polymer Journal - Surface of Al2O3 nanoparticles was modified with a silane coupling agent, and aramid fiber-reinforced epoxy nanocomposites were produced using these particles. Three... 相似文献
9.
Hot rolled steel (HRS) is used extensively in the automotive, agricultural and appliance industries. The corrosive response of HRS was investigated after it had been exposed to various surface treatments, prior to powder coating. The behaviour of three conversion coatings: zinc phosphate (ZnP), iron phosphate (FeP) and zirconium (Zr)-based nano-scaled, on HRS was studied. HRS is naturally covered with iron oxide scale and this was removed from the surface by mechanical and chemical processes, prior to the application of surface treatment and organic coatings. The following tests on differently treated panels were conducted to evaluate corrosion performance: adhesion tests such as, crosshatch, pull-off, and conical bending, SEM, XPS, salt spray and electro-chemical impedance studies were also performed. Good correlations were recorded showing that zinc phosphate conversion coating gave the best performance, and zirconium-based nano-structured conversion coating, was superior to that of iron phosphate conversion coatings on HRS. 相似文献
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