尼龙66高强力轻型帘布的开发与应用

神马尼龙66高强力轻型帘布在保持帘布高强力、尺寸稳定性、耐热性、耐疲劳、耐冲击的良好特性的前提下，采用SNT高强度工业丝生产技术，充分挖掘工业丝的强力优势，把富余的强力通过进一步降低纤维密度转化为帘布面积优势的扩大，从而提高轮胎生产的帘布出胎率，使轮胎生产厂享受尼龙66帘布品质的同时，实现降低成本的目的。     

分散剂FDN对G级油井水泥作用机理探讨

采用液相电导法和酸度法研究了分散剂FDN对G级油井水泥水化速度的影响。发现FDN促进水泥的早期水化,但吸附-络合作用及磺酸根离子对Ca(OH)_2核晶过程的“毒化”作用使后期水化速度减慢。本研究证实ζ电位升高是FDN广生分散作用的主要因素。当FDN的吸附达饱和时,ζ电位达最大值,水泥浆的分散程度最大。     

Effect of polymerization conditions on o‐phenylenediamine and o‐phenetidine oxidative copolymers

A series of new o‐phenylenediamine (OPD)/o‐phenetidine (PHT) copolymers with partly phenazine‐like structures has been successfully synthesized at three polymerization temperatures by chemically oxidative polymerization in four different polymerization media. The molecular structures and properties of the resulting OPD/PHT polymers were investigated by IR, UV–vis and high‐resolution ¹H NMR spectroscopies, and DSC, in order to ascertain the effect of reaction temperature, comonomer ratio and acid medium. The copolymerization mechanism of OPD with PHT monomers has been proposed. It is found that the statistical OPD/PHT copolymer obtained at a temperature of 118 °C has a higher degree of polymerization than that obtained at 12–17 °C. The OPD content in the copolymers calculated from NMR spectroscopic analysis is higher than that in the feed OPD content, whereas the OPD content calculated from element analysis is slightly lower than the feed OPD content. It can be predicted that denitrogenation takes place in the OPD units during the polymerization process at OPD/PHT molar ratios of 90/10 and 100/0. These OPD/PHT copolymers exhibit a much better solubility than the OPD homopolymer, hence suggesting an incorporation of PHT units into the phenazine structure of the homopolymer. The thermal behavior of the copolymers was also studied. Copyright © 2004 Society of Chemical Industry     

Towards a Dual-Tip STM Application in Mesoscopic Electron Transport

A new design for a dual-tip scanning tunneling microscope (STM) is presented. The design is a variation on the mechanically controllable break-junction with two electron beam-induced deposition nano-tips. The new design enables one to scan surfaces simultaneously with two probes having a nano-gap separation. By collecting the lateral current flowing between the tips, the transconductance map can then be compared with the STM images for local characterizations of the electron transport. Since the lateral beam carries the property of the density of states of the surface at momentum space, the dispersion of the electronic structure should give an orientation and position dependence of the local transconductance current. In addition, the reduced terminal separation, on the order of the characteristic mesoscopic length scales, is likely to be sensitive to a variety of typically observed interactions and interference effects.     

金属及合金中钛的光度分析近况

综述了金属及合金中钛的光度测定方法新近进展情况。