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The composition and chemical bonding of the first atoms across the interface between Si(0 0 1) and the gate dielectrics determine the quality of gate stacks. An analysis of that hidden interface is a challenge as it requires high sensitivity in both elemental and chemical state information. We used synchrotron radiation (SR) based photoelectron spectroscopy and, in particular, X-ray absorption spectroscopy in total electron yield and total fluorescence yield at the Si2p and the O1s edges to address this issue. We report on results for Hf oxide prepared by ALD and compare to Pr2O3/Si(0 0 1). For Hf oxide thin films we find evidence for the silicate formation at the interface as derived from the characteristic features in the X-ray absorption spectra at the Si2p and the O1s edges. Resonant photoelectron spectroscopy is used to analyze the absorption band in detail. Following the resonant profiles of initial and final states we deduce from the resonant behaviour a charge donation via a Si-induced charge transfer. 相似文献
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Mingchao Wang Huanhuan Shi Panpan Zhang Zhongquan Liao Mao Wang Haixia Zhong Friedrich Schwotzer Ali Shaygan Nia Ehrenfried Zschech Shengqiang Zhou Stefan Kaskel Renhao Dong Xinliang Feng 《Advanced functional materials》2020,30(30)
2D conjugated metal‐organic frameworks (2D c‐MOFs) are emerging as a novel class of conductive redox‐active materials for electrochemical energy storage. However, developing 2D c‐MOFs as flexible thin‐film electrodes have been largely limited, due to the lack of capability of solution‐processing and integration into nanodevices arising from the rigid powder samples by solvothermal synthesis. Here, the synthesis of phthalocyanine‐based 2D c‐MOF (Ni2[CuPc(NH)8]) nanosheets through ball milling mechanical exfoliation method are reported. The nanosheets feature with average lateral size of ≈160 nm and mean thickness of ≈7 nm (≈10 layers), and exhibit high crystallinity and chemical stability as well as a p‐type semiconducting behavior with mobility of ≈1.5 cm2 V?1 s?1 at room temperature. Benefiting from the ultrathin feature, the nanosheets allow high utilization of active sites and facile solution‐processability. Thus, micro‐supercapacitor (MSC) devices are fabricated mixing Ni2[CuPc(NH)8] nanosheets with exfoliated graphene, which display outstanding cycling stability and a high areal capacitance up to 18.9 mF cm?2; the performance surpasses most of the reported conducting polymers‐based and 2D materials‐based MSCs. 相似文献
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Synthesis of 2,4-Bisalkyl(aryl)amino-6-cyanamino-s-triazines Reaction of 2,4-bisalkyl(aryl)amino-6-chloro-s-triazines with disodiumcyanamide to 2,4-bisalkyl(aryl)amino-6-cyanamino-s-triazines ( 3a – g ) strongly depends on the solvent used. In dimethylformamide by-products predominate. The best results are found in dimethylsulphoxide. 相似文献
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A New In Situ Microscopy Approach to Study the Degradation and Failure Mechanisms of Time‐Dependent Dielectric Breakdown: Set‐Up and Opportunities
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Zhongquan Liao Martin Gall Kong Boon Yeap Christoph Sander Oliver Aubel Uwe Mühle Jürgen Gluch Sven Niese Yvonne Standke Rüdiger Rosenkranz Markus Löffler Norman Vogel Armand Beyer Hans‐Jürgen Engelmann Peter Guttmann Gerd Schneider Ehrenfried Zschech 《Advanced Engineering Materials》2014,16(5):486-493
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Marianna Erbano Carlos Augusto Ehrenfried Maria Élida Alves Stefanello Élide Pereira Dos Santos 《Microscopy research and technique》2012,75(12):1737-1744
Salvia lachnostachys Benth., Lamiaceae, is a endemic species from southern Brazil. The essential oil of its leaves and flowers is mainly constituted by aliphatic compounds, such as dodecanoic acid, with sesquiterpenes as minor constituents. This work evaluated the morphology, anatomy, microchemistry, and phytochemistry of S. lachnostachys to provide advanced knowledge of Brazilian plants with medicinal potential. Light and scanning electron microscopy techniques were used in the anatomical and microchemical studies. Compounds were isolated by chromatographic techniques, identified by analysis of their NMR spectra and compared with published data. S. lachnostachys can be distinguished from other related species mainly by its petiolate leaves, terminal inflorescence, persistent bracts, and villous‐glandular corolla. The stem and leaves of S. lachnostachys display anatomical characteristics common to the family Lamiaceae. However, this species can be distinguished from other family members by the morphology and the presence of eglandular and glandular trichomes, as well as the organization of the vascular bundles of the petiole. The phytochemical results revealed that S. lacnostachys produces oleanolic and ursolic acids in addition to the diterpene fruticuline A, which is a rare compound, previously found only in Salvia fruticulosa Benth. and S. corrugata Vahl. Ursolic and oleanolic acids are bioactive triterpenes that exhibit antiatherosclerotic, anticancer, antihypertensive, antinflammatory, antileukemic, antimutagenic, antioxidant, antiproliferative, and antiviral activities, and fruticuline A has antibacterial activity. Microsc. Res. Tech. © 2012 Wiley Periodicals, Inc. 相似文献