-150℃四级自复叠制冷系统的实验与分析

搭建了一种四级自复叠制冷系统,采用由R600a、R134a、R23、R14、R50和R740等6种工质组成的非共沸混合制冷剂,经过调试与实验,成功得到了-150℃的柜内温度。讨论了该低温箱体的降温特性、压缩机的运行特性和混合工质的节流特性。研究表明,压缩机的吸、排气压力和温度关乎系统能否安全稳定的运行,每级毛细管的长度关乎系统的降温特性。     

响应面法优化腐乳生产中的培菌条件

在单因素试验基础上,利用响应面法优化腐乳生产的培菌条件。响应面分析结果表明,最佳培菌条件是:温度28℃,时间72.7 h,接种量10.2%。     

氨基树脂表面活化提高固定化核酸酶P1连续催化性能

考察了固定化酶常用载体-氨基树脂几何结构及表面活化过程对固定化核酸酶P₁性能的影响,并进行了动力学和连续催化稳定性研究。FESEM、BET及FTIR等表征发现,氨基树脂具有大量酶可利用的孔,在固定化过程中核酸酶P₁主要利用的孔径范围为4～30 nm。相对游离的核酸酶P₁而言,所得固定酶耐酸、耐热性增强;米氏动力学研究表明各组固定酶对底物的亲和力下降,最大反应速率下降;后交联组的重复利用性相对物理吸附、化学交联组明显增强。优化的固定化条件为：酶和载体比例为3：20（质量比）,酶浓度为0.8 g·L^-1,酶液pH为6.0,固定时间为10 h,在优化条件下所得固定酶的单位载体酶活为10013 U·g^-1。同时设计及优化柱连续反应器操作条件,确定反应温度为65℃,进料流量为0.75 ml·min^-1,使得产品的核苷酸浓度维持30 g·L^-1（水解率为60%）以上的累计时长达120 h,有利于核酸酶P₁连续生产核苷酸的工业化应用。     

孔雀石绿分光光度法测定双酚A

在酸性介质中,双酚A对羟基自由基氧化孔雀石绿的反应具有抑制作用,据此建立了测定双酚A含量的分光光度法。在最佳实验条件下,体系的吸光度变化值与双酚A浓度呈线性关系,其线性范围为8.14×10–8~7.02×10–7 mol/L。线性回归方程为ΔA=0.0184+0.452c(×10–6mol/L),线性相关系数为0.9862,检出限为2.44×10–8 mol/L。应用本法测定5种塑料制品中双酚A的含量,回收率在96%~106%之间,RSD在1.5%~3.8%之间。     

酵母分离株分子鉴定及其挥发性香气成分检测分析

测定了8类不同食品来源的12株酵母分离株26S rDNA D1/D2序列,与Genbank登陆序列比较分析,12株分离酵母鉴定为:3株酿酒酵母,2株戴尔有孢圆酵母、1株马克斯克鲁维氏酵母、1株喜仙人掌毕赤酵母、1株鲁西坦念珠菌、1株膜噗毕赤酵母、2株Kudriavzevii毕赤酵母,1株疑似新种。选用固相微萃取-气质联用(SPME-GC/MS)方法,完成了各分离株挥发性成分的检测。结果表明,酵母发酵后的香气组分主要为酯类,包括乙酸乙酯、辛酸乙酯、乙酸苯乙酯、癸酸乙酯等,其中菌株A1发酵后产生多种含量较高的挥发性组分及独有组分己酸乙酯。结果表明,酵母产生的香气组分、含量与酵母分离来源、种类有关,这可能与不同酵母代谢途径的差异相关。     

Access probability optimization for streaming media transmission in heterogeneous cellular networks

FemtoCaching technology, aiming at maximizing the access probability of streaming media transmission in heterogeneous cellular networks, is investigated in this paper. Firstly, five kinds of streaming media deployment schemes are proposed based on the network topology and the relationship between users and streaming media. Secondly, a matching algorithm for adaptive streaming media deployment is proposed, where the FemtoCaching can be adjusted dynamically. Thirdly, a joint problem is formulated combined with the channel assignment, the power allocation, and the caching deployment. To address this problem, we propose a joint optimization algorithm combining matching algorithm and genetic algorithm to maximize the access probability of streaming media transmission. Simulation experiments demonstrate that: (1) the average access probability of all users accessing streaming media in the network based on the proposed algorithm compared with recent works can be greatly improved, and (2) the performance increases with increasing the number of channels and the storage capacity of micro base stations, but decreases with increasing the number of users.

     

RANGE AMBIGUITY DISTRIBUTION CHARACTERISTIC OF SPACEBORNE SAR AND ITS DESIGN CONSIDERATION

A new approach is proposed which can satisfy the range ambiguity requirement while keep the antenna width not to be enlarged and get the high quality image also. Here the chirp slope of the transmitted linear frequency modulated pulses is reversed alternately. Therefore, during the range compression significant portion of the ambiguous return which is due to the mismatching with the signal reference function is suppressed. The suggested method provides significant improvement in range ambiguity ratio and can be utilized in attaining wider swath.     

CBR: An Effective Clustering Approach for Time Series Events

Neural Processing Letters - As technology advances, a large number of time series data have emerged in all walks of life. Clustering is a key technique for analysing time series data. However, most...     

分子筛吸附脱除芳烃中的环状烯烃

以Y型分子筛为吸附剂脱除甲苯中的环状烯烃化合物（二聚环戊二烯,DCPD）。采用NH3-TPD测试方法分析了USY和HY分子筛的酸性中心性质。通过间歇吸附实验考察了USY和HY分子筛对甲苯中DCPD的吸附脱除能力以及温度对USY分子筛吸附能力的影响,结果表明,USY分子筛的烯烃吸附量是HY分子筛的1.68倍;当温度由30℃升至50℃时,USY分子筛的吸附速率增大。采用固定床连续实验考察了温度、体积空速和原料中烯烃浓度对USY分子筛吸附效果的影响,当温度为80℃、空速为0.133h?1时,分子筛的穿透吸附量最大;分子筛处理具有较高初始浓度的原料时得到较高的穿透吸附量,且对工业焦化甲苯溶液的处理效果明显,具有较好的工业应用前景。TGA热重分析结果表明,USY分子筛对DCPD的选择性吸附能力强于甲苯。