Comparative study of crystallization processes in Sb2Te3 films using laser and thermal annealing techniques

Adherent and pin-hole free amorphous Sb₂Te₃ thin films have been obtained by vacuum evaporation at substrate temperatures ≤25 °C. The films have been crystallized by thermal and laser annealing, and the crystallization processes monitored as a function of annealing temperature and laser scan speed. A comparative study of topography reveals disk-shaped crystallized areas in thermal crystallization and dendrite growth in the laser induced process. The crystallized films in both cases contain a single Sb₂Te₃ phase. Activation energy of 2 eV for crystallization, determined using differential scanning calorimetery indicates good room temperature stability of the amorphous states.     

Object-oriented intelligent computer-integrated design, processplanning, and inspection

The methodology for developing intelligent integrated computer-aided design and manufacturing systems based on object-oriented principles is discussed. The ways in which the application of these principles affects the nature of these systems are reviewed. The implementation of an automated, intelligent, and flexible computer-integrated-manufacturing (CIM) system prototype using an object-oriented programming environment (Smalltalk-80, Version 4.0) is detailed. A CIM system includes CAD, a process planner, and an inspection planner. Each of these components is discussed individually     

Thermal gas effusion from diamond-like carbon films

Good-quality diamond-like carbon films (6 at.% H₂, 2400 kgf/mm² microhardness, 2.7 eV bandgap, higly insulating) have been obtained by the DC glow discharge decomposition of acetylene. Mass spectroscopic thermal effusion measurements were carried out on the films deposited under different deposition conditions. Analyses of hydrogen in conjunction with hydrocarbon effusing species yield information on the microstructure and nature of C---H bonding configurations. It is shown to be a useful analytical tool to study hydrogenated amorphous carbon films of different microstructures varying from polymer-like to diamond-like.     

Single point incremental forming: state-of-the-art and prospects

Incremental sheet metal forming in general and Single Point Incremental Forming (SPIF) specifically have gone through a period of intensive development with growing attention from research institutes worldwide. The result of these efforts is significant progress in the understanding of the underlying forming mechanisms and opportunities as well as limitations associated with this category of flexible forming processes. Furthermore, creative process design efforts have enhanced the process capabilities and process planning methods. Also, simulation capabilities have evolved substantially. This review paper aims to provide an overview of the body of knowledge with respect to Single Point Incremental Forming. Without claiming to be exhaustive, each section aims for an up-to-date state-of-the-art review with corresponding conclusions on scientific progress and outlook on expected further developments.     

Thermodynamic properties of alumina-saturated iron-carbon-bismuth alloys

Using direct and indirect equilibration methods, the solubilities of iron in molten bismuth and those of bismuth in molten iron-carbon alloys have been measured over the temperature range 1473-1873 K. The Henrian behaviour of bismuth in molten ferrous alloys allows the calculation of its activity coefficient, which in turn facilitates modelling as a function of temperature and carbon content, using the unified interaction parameter formalism developed by Pelton and Bale. The modelling results generate the expression: . A model has also been developed expressing bismuth content in molten iron-carbon alloys as a function of temperature and composition: .     

Empirical validation of object-oriented metrics for predicting fault proneness models

Empirical validation of software metrics used to predict software quality attributes is important to ensure their practical relevance in software organizations. The aim of this work is to find the relation of object-oriented (OO) metrics with fault proneness at different severity levels of faults. For this purpose, different prediction models have been developed using regression and machine learning methods. We evaluate and compare the performance of these methods to find which method performs better at different severity levels of faults and empirically validate OO metrics given by Chidamber and Kemerer. The results of the empirical study are based on public domain NASA data set. The performance of the predicted models was evaluated using Receiver Operating Characteristic (ROC) analysis. The results show that the area under the curve (measured from the ROC analysis) of models predicted using high severity faults is low as compared with the area under the curve of the model predicted with respect to medium and low severity faults. However, the number of faults in the classes correctly classified by predicted models with respect to high severity faults is not low. This study also shows that the performance of machine learning methods is better than logistic regression method with respect to all the severities of faults. Based on the results, it is reasonable to claim that models targeted at different severity levels of faults could help for planning and executing testing by focusing resources on fault-prone parts of the design and code that are likely to cause serious failures.     

Developing a framework for analyzing IS sourcing

This paper develops a framework for the consideration of internal markets as an alternative to information systems (IS) outsourcing. It is based on an assessment of the pros and cons of both outsourcing and of insourcing based on the internal markets approach. It is formulated in terms of the operational, tactical, and strategic impacts of the choice among the alternatives. The framework, and the propositions that are developed from it, should be useful both for researchers, who can use it for developing testable research hypotheses, and for practitioners, who may use it as a basis for developing a comprehensive set of criteria for the evaluation of these sourcing options.     

Influence of tool material on dynamics of drilling of GFRP composites

Drilling trials have been carried out on glass Fibre reinforced plastics (GFRP) with plain high speed steel (HSS), TiN coated HSS and tipped tungsten carbide drills. Most of the defects in drilling of composites are due to thrust force experienced by the workpiece. The parametric influence on cutting force was experimentally evaluated. The experimental results show that the defects toleranced drilling can be attained by proper selection of cutting parameters and tool material. This is substantiated by monitoring flank wear, hole shrinkage and acoustic emission during drilling.     

Dielectric spectroscopic studies on polypyrrole glucose oxidase films

An investigation was made into the dielectric spectroscopic characteristics of p-toluene sulfonate (PTS) doped polypyrrole (PPY) films in the presence and absence of immobilized glucose oxidase (GOX) in three different configurations: Al-PTS-PPY-Al-PTS-PPY/GOX-Al, and Al-PTS-PPY/GOX/β-D -glucose-Al, respectively. Measurement of dielectric loss and capacitance yielded valuable information about the dielectric properties of GOX immobilized in PTS doped PPY films. The effect of both the temperature and varying βD -glucose concentrations on the mobility of the charge carriers in these films was also systematically studied. © 1996 John Wiley & Sons, Inc.