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排序方式: 共有102条查询结果,搜索用时 15 毫秒
1.
Maurya Atul Kumar Gogoi Rupam Sethi Sushanta K. Manik Gaurav 《Journal of Materials Science》2021,56(30):16976-16998
Journal of Materials Science - Fly ash (FA) particles were surface modified with cetyltrimethylammonium bromide (Ctab) and hybridized with graphene oxide (GO) and carboxymethyl cellulose (CMC)... 相似文献
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The copper(II)‐catalyzed decarboxylative coupling reactions of arylglyoxylic acids with isatins afford 4H‐benzo[d][1,3]oxazin‐4‐ones via decarbonylation and concurrent C–N, C–O bond formation.
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Aliphatic hyperbranched poly(urethane-urea)s with different weight percentages of branch generating moiety were synthesized by a one pot A2 + BC2 approach. Isophorone diisocyanate was used as the A2 type monomer, while a tri-functional dihydroxyamine compound synthesized from ?-caprolactam and diethanol amine acted as the BC2 monomer. Evidence supporting the hyperbranched structure of the synthesized poly(urethane-urea) was obtained from 1H NMR spectra. FTIR study confirmed the nature and extent of hydrogen bonding present in this novel macromolecule. A Gaussian band fitting procedure of the IR band at amide-I region showed that the extent of hydrogen bonding increases with the increase of weight percentage of the tri-functional compound. The tensile strength, elongation at break, impact resistance, scratch hardness and gloss followed an increasing trend with the same. The thermal degradation of the hyperbranched poly(urethane-urea) was found to be dependent on the weight percentage of the BC2 type moiety. The kinetics of thermal degradation studied by the Ozawa method showed that the activation energy required for thermal degradation of hyperbranched polymer is higher than its linear polyurethane analog. The synthesized polymer was found to be biodegradable by Pseudomonas aeruginosa bacteria. The study showed superiority of the hyperbranched structure over the linear one. Thus the results indicated the potential usage of the studied hyperbranched poly(urethane-urea) as an advanced surface coating material. 相似文献
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Junali Handique Joly Gogoi Jayashree Nath Swapan Kumar Dolui 《Polymer Engineering and Science》2020,60(1):140-150
This investigation reports the effective use of the Diels–Alder (DA) click reaction in the preparation of self-healing bio-based dendritic methacrylates having reactive furfuryl functionality. Bio-based methacrylates were synthesized by modifying tannic acid with glycidyl methacrylate and furfuryl functionality was introduced by atom transfer radical polymerization with varied amount of furfuryl methacrylate monomer. The thermoreversible network was successfully achieved by DA and retro-DA reaction between the furfuryl groups and a bifunctional maleimide crosslinker, bismaleimide. This process was studied by nuclear magnetic resonance spectroscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis, and solvent exposure tests. Differential scanning calorimetry analysis was used to determine the endothermic retro-DA reaction in the DA adduct. The self-healing property of the above crosslinked material was demonstrated by monitoring the repair of a scratch in the polymer film upon heating and cooling. This was analyzed by scanning electron microscopy. POLYM. ENG. SCI., 60:140–150, 2020. © 2019 Society of Plastics Engineers 相似文献
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Harshita Gogoi V. Nirosha Anjali Jayakumar Keerthana Prabhu Meghna Maitra 《Energy Sources, Part A: Recovery, Utilization, and Environmental Effects》2018,40(1):39-44
In the present study, pre-treated paper mill sludge (PMS) was evaluated extensively as a substrate for production of acetone-butanol-ethanol using Clostridium sporogenes NCIM 2337. The PMS was subjected to three types of pre-treatment methods namely alkali, mechanical, and thermal treatment and was analyzed by SEM. The pre-treatment of PMS by alkali was observed to be more effective over the other pre-treatment methods. The alkali pre-treated sludge was then made to undergo fermentation, which showed the conventional process of acidogenesis followed by solventogenesis. The acetone, butanol, and ethanol concentration for 15% alkali pre-treated PMS was estimated to be maximum. 相似文献
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Layers of naturally occurring clay minerals are rearranged to prepare highly sensitive multiresponsive clay–clay bilayer membrane (CCBM). The CCBM introduced here responds to the minuscule changes in the surrounding environments including temperature, humidity, and presence of solvent vapors by morphing in specific manners. Strips cut from CCBM exhibit up to 588 N kg?1 force output when exposed to temperature fluctuations. Inheriting the natural stability of clay minerals, CCBM demonstrates extreme robustness, heating up to 500 °C, cooling with liquid N2 and exposure to corrosive chemical vapors did not deteriorate its bending performance. Mechanistic studies suggest that shape transformations of CCBM are driven by the unequal response of its components to external stimuli. 相似文献
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A study was conducted to evaluate the nutritional potential of four commonly available, unexplored aquatic weeds namely, Salvinia cuculata, Trapa natans, Lemna minor and Ipomoea reptans from northeast India for ascertaining their suitability for utilization as supplementary fish feed with the aim to reduce the cost of commercial feeds. Results of proximate analysis showed that the crude protein content of the aquatic weeds ranged between 11.0% and 32.2% (w/w), whereas crude fibre and ash contents varied between 4.2% and 20% (w/w), and 13.3% and 31.2% (w/w), respectively. Protein to energy ratio (P/E) of these weeds ranged between 30.7 mg/kcal and 95.3 mg/kcal and the highest value was displayed by I. reptans. All these aquatic weeds contained high amounts of vitamins E and C and mineral elements required for the normal growth and development of fish. 相似文献
10.
Development and characterization of pseudolatex based transdermal drug delivery system of diclofenac. 总被引:1,自引:0,他引:1
Suresh P. Vyas Partha Jyoti Gogoi Sanjay K. Jain 《Drug development and industrial pharmacy》1991,17(8):1041-1058
A transdermal drug delivery system of diclofenac was developed for prolonged and controlled release of diclofenac. The designed system essentially based on polymeric pseudolatex dispersion. The formulation variables that could effect the formulation stability vis a vis drug release were studied. To achieve the desired release rate, different combination of hydrophilic and hydrophobic polymer were used for the preparation of pseudolatex system. The designed system exhibited linear relationship between drug release (Q) V/s square root of time (t0.5). The product having skin permeability rate 0.188 mg/h/cm was selected for the in vitro anti-inflammatory activity and in vivo evaluation. The system could maintained a constant and effective plasma level for 24 hours. The effective drug plasma concentration was monitored periodically. The study revealed that designed pseudolatex transdermal drug delivery system of diclofenac could be used successfully with improved performance and hold promise for further studies. 相似文献