离子液体中α,β-不饱和化合物的绿色合成

芳香醛和活泼亚甲基化合物为原料,在离子液体中进行Knoevenagel缩合反应。本工艺避开了传统方法中在加入催化剂的有机溶剂中进行Knoevenagel缩合反应的步骤,采用离子液体为反应提供环境和催化,具有操作简单、成本低、对设备无特殊要求和环境友好的优点。     

Structural,morphological, dielectric and magnetic properties of Zn-Zr co-doping yttrium iron garnet

In this study, yttrium iron garnet co-doped with Zn and Zr atoms with a chemical formula Y₃Zn_xZr_xFe_(5−2x)O₁₂ (x = 0.0-0.3) has been successfully prepared by the solid-state reaction method. The effects of doping concentration on the microstructure, crystal structure, magnetic properties, and dielectric properties of Y₃Zn_xZr_xFe_(5−2x)O₁₂ were investigated. The microstructure analysis indicates that co-doping of YIG with Zn and Zr can effectively reduce the grain size of the ceramic. The crystal structure results reveal that the doping concentration of Zn–Zr has substantial influence on the lattice parameters of YIG, such as, increases the lattice constant, crystal cell size, and interplanar spacing. However, the second phase of ZrO₂ appears once x ≥ 0.15. Additionally, the dielectric properties of YIG ferrite can be regulated using this Zn–Zr co-doping method. Zn–Zr co-doping can improve the dielectric stability and reduce the dielectric loss at high temperature. The magnetization measurement shows that the saturation magnetization is stabilized at x < 0.15, and the magnetic loss is decreased with the increase in the doping concentration. Overall, the findings show that the ceramic with x = 0.1 exhibits better properties included high saturation magnetization (24.607 emu/g), low magnetic loss (0.0025 @ 1 MHz), and relatively low dielectric loss (496 @ 400°C).     

Effect of Biochar as Reductant on Magnetizing-roasting Behavior of Pyrite Cinder

The effect of biochar substituted for anthracite as reductant on magnetizing-roasting pyrite cinder was investigated.The key of magnetizing-roasting is the gasification reaction between reductants and CO2.Since biochar could react with CO2 more rapidly at lower temperature,the reactivity of biochar is better than that of anthracite.The gasification of biochar could produce reducing condition ofφCO/(φCO+φCO2)about 10%-20% between 700-800 ℃,which is in accord with the atmosphere and temperature of Fe2O3 reduction.So it is beneficial to the reduction of iron mineral of pyrite cinder.Compared with anthracite,biochar could decrease the roasting temperature from825 to 750 ℃ and roasting time from 20 to 15min,which shows that a better effect of magnetization could be obtained in the condition of lower temperature and shorter time.Using biochar as reductant,iron concentrate extracted from pyrite cinder as about 64%iron grade could be produced,and the recovery is over 90% under the condition of above 90% grinding particle less than 0.045 mm and magnetic intensity of 0.124-0.194 T.     

CDMA 1x EV-DO覆盖模型的分析与仿真

结合经过校正后的适合于本地无线环境的OKUMURA-HATA传播模型，建立起一种新的本地化基于1x EV—DO系统数据业务吞吐量分析的覆盖预测仿真模型，可应用于1xEV—DO系统的网络规划及系统性能分析。     

克拉2气田水处理装置设计浅析

介绍了克拉2气田中央处理厂一期气田水处理装置的处理工艺特点和流程。针对气田水的最终去向，分析气田水的水质特点，提出合理的处理方案，既符合环保要求，达到保护环境的目的，又简化了工艺，节约了投资。     

连续波半主动雷达制导空空导弹截获跟踪距离计算

分析了连续波半主动雷达制导导弹导引头工作电磁环境和对武器系统攻击区的影响，建立了热噪声和杂波干扰环境下导引头截获距离方程，分析推导了直波泄漏干扰，地杂波干扰的计算公式，并在此基础上给出了导弹允许攻击区计算公式。     

锑酸消除含氚废空气中的氚

用锑酸作消气材料 ,压制成消氚电极 ,在适当外加条件下 ,考察了锑酸作消氚材料直接将含氚废空气中的氚除去的可能性。对消氚过程中料气中氚的浓度及水分对消氚结果的影响进行了考察 ,给出了消气片中氚的物料平衡。结果表明 :在 3 2L含氚空气中 ,用锑酸制成的消氚材料 ,在 2 0 0min左右可将原料气氛中 80 %以上的氚去除     

几种典型凸轮裹包执行机构的从动系统运动规律的理论分析

详细分析了裹包执行机构的正弦型和正切型从动系统的运动规律，用数学方法对运动规律进行了详尽的理论分析。     

勘探工程综合配套技术在巴音都兰凹陷隐蔽油气藏勘探中的应用

巴音都兰凹陷巴Ⅰ、巴Ⅱ号隐蔽油气藏的勘探以前期综合评价技术为基础,立足现有技术资料,在勘探系统工程中形成了全三维地震资料处理、薄互层录井、油气层保护、MFE二开助排为代表的隐蔽油气藏综合配套技术。文中对各项配套技术进行了论述,简要评价了应用效果,认为该套技术对二连盆地隐蔽油气藏的勘探针对性强、有效实用,较好地解决了勘探工程实施中存在的关键技术问题,可为类似领域的油气勘探提供技术借鉴。