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1.
The copreheat-treatment of non-fusible and slightly fusible coals with A240 and hydrogenated A240 under high temperature-short contact-time conditions around 500 °C has been examined in an attempt to produce a formed coke with better anisotropic development. These conditions shortened the copreheat-treatment time and provided better anisotropic development in the resultant coke after carbonization. Effectiveness of short contact-time has been discussed in terms of the extent of depolymerization of coal molecules suitable for anisotropic development, this being related to coal liquefaction under similar conditions. 相似文献
2.
Yi Kai Zhou Sung Woo Choi Shigeya Kimura Shuichi Emura Shigehiko Hasegawa Hajime Asahi 《Journal of Superconductivity and Novel Magnetism》2007,20(6):429-432
GaGdN layers were grown at temperatures below 300°C by radio-frequency plasma-assisted molecular beam epitaxy on sapphire
substrates. GaGdN samples with high Gd concentration as high as 12.5% were obtained by lowering the growth temperature. X-ray
diffraction results showed no obvious secondary phase, which means that the phase separation can be suppressed by the growth
at low temperatures. All samples, including those grown at room temperature, showed ferromagnetic characteristics. Photoluminescence
emission was observed, though spectra exhibit broad and sharp luminescence bands related to many kinds of defects. It is suggested
that electrons coming from defects, especially, nitrogen vacancy, stabilize ferromagnetism, and that the carrier-induced ferromagnetism
occurs in the low-temperature-growth GaGdN. 相似文献
3.
Segregation in sputtered Co-Cr films 总被引:1,自引:0,他引:1
The segregation growth process in sputtered Co-Cr films is investigated by examining the effect of substrate temperature on the segregated microstructure and magnetic properties. In sputtered Co-25at%Cr films, segregation occurs below 560°C, and both the saturation magnetization and the perpendicular anisotropy constant show a maximum around a substrate temperature of 300°C, where a specific microstructure, called a CP (chrysanthemum-like pattern) structure, is observed. The results suggest that the CP structure becomes observable in the highly segregated state and generates high perpendicular anisotropy. A new segregation growth model is derived from the results of the CP structure observations. Using this model, it is possible to explain the continuous transition of the magnetization mode between the continuous and the particulate modes. 相似文献
4.
Toshiaki Nishihata Mayumi Ishizaka Sigeharu Yokohama Alice C. Martino Roger E. Gordon 《Drug development and industrial pharmacy》1993,19(20):2679-2698
The effects of particle size and food on the absolute bioavailability of U-78875 in dogs after oral administration of either a suspension or tablet dosage form were investigated. A reduction of particle size caused a significant increase in bioavailability along with an increase in dissolution rate. Additionally, both suspension and tablet dosage forms administered after food caused an increase in bioavailability. Thus, to accelerate drug dissolution, a reduction of U-78875 particle size from the unmilled state is important for the optimization of formulation compositions. To increase the bioavailability of U-78875, postprandial dosing should be considered. 相似文献
5.
In this study, current collecting efficiency of the micro tubular solid oxide fuel cell (SOFC) was estimated to determine optimum size of the micro tubular SOFC. Two models for collecting current from single terminal (ST) and double terminal (DT) of anode tube were proposed and used to calculate the current collecting efficiency as functions of anode thickness, tube length and operating temperature. It was shown that design of the cell geometry and current correcting method are significantly important to achieve high performance micro tubular SOFC stacks. The efficiency loss estimated from the DT model was about 2–4-fold lower than those of obtained from the ST model. The DT model was shown to be more effective for higher operating temperature and the tube length. 相似文献
6.
Tomohito Kameda Kazuya Horikoshi Shogo Kumagai Yuko Saito Toshiaki Yoshioka 《中国化学工程学报》2021,28(12):2993-3001
In this paper, we propose that the urinary toxins from the wastewater be adsorbed on an adsorbent such as spherical activated carbon and the latter be regenerated by subjecting it to high temperatures to recycle activated carbon and also to recycle the water used in dialysis. We studied the adsorption of artificial waste dialysate, which is a mixed solution of urea, creatinine, and uric acid, and the separate solutions for each of these and found that their extents of adsorption onto the spherical activated carbon material were nearly identical. The amount of adsorption was approximately 1.4 mg·g-1 for urea, 18 mg·g-1 for creatinine, and 20 mg·g-1 for uric acid. The urea, creatinine, and uric acid adsorbed onto the spherical activated carbon decomposed on heat treatment at 500℃, and the adsorption capacity of the spherical activated carbon was regenerated. Our study successfully demonstrated that the spherical activated carbon can be recycled in the waste dialysate treatment process. 相似文献
7.
A high-performance liquid chromatographic method, using post-column detection with diphenyl-1-pyrenyl-phosphine (DPPP), was
developed for the quantitative and qualitative determination of isomeric lipid hydroperoxides (OOH). The OOH eluted from a
normal-phase column were passed through a photodiode array detector and then mixed with DPPP solution in a reaction coil heated
at 80°C. DPPP oxide formed by the reaction with OOH was determined by monitoring the fluorescence intensity at 380 nm and
excitation at 352 nm. The conjugated diene OOH (13-cis, trans- and 9-cis, trans-OOH) and nonconjugated OOH (12-cis-trans- and 10-cis, trans-OOH) from photosensitized oxidation of methyl linoleate were determined in a molar ratio of 31∶29∶19∶21, respectively. However,
only the two conjugated hydroperoxides were detected by ultraviolet absorption at 234 nm. Further applications were carried
out for the determination of OOH of methyl oleate and methyl linolenate. This method proved to be useful for the determination
of the OOH containing both conjugated and nonconjugated diene structures. 相似文献
8.
Ken Shimomai Noboru Higashida Toshiaki Ougizawa Takashi Inoue Bernd Rudolf Jörg Kressler 《Polymer》1996,37(26):5877-5882
The miscibility of poly(methyl methacrylate) (PMMA) and styrene-acrylonitrile random copolymers (SAN) blends was investigated on the basis of the Flory—Orwoll—Vrij equation of state theory. To obtain the equation of state parameters (P*, V*sp, T*: characteristic parameters), the pressure—volume—temperature (PVT) behaviour was measured for PMMA and a series of SANs with various acrylonitrile contents. The exchange energy parameter Xij was also calculated by fitting the theory to some phase diagrams of PMMA/SAN blends. The Flory—Huggins interaction parameter χ was separated into two contributions based on the equation of state theory for mixtures: the exchange energy term χinter and the free volume term χfree. Both the temperature and copolymer composition dependences of χinter and χfree were estimated by calculations using the equation of state parameters. There exists a region in which χinter is negative, leading to a miscibility window in PMMA/SAN blends. However, the immiscibility at high temperatures in the blends cannot be explained only by χinter; it is caused by the free volume contribution, χfree. The miscibility window behaviour in PMMA/SAN blends may be explained within the framework of the equation of state theory. 相似文献
9.
Tsugio Sato Kenji Dosaka Toshiaki Yoshioka Akitsugu Okuwaki Kazuo Torii Yoshiro Onodera 《Journal of the American Ceramic Society》1992,75(3):552-556
Amorphous CeO2 –ZrO2 gels were prepared by coprecipitation in ammonia solutions. The onset of crystallization of the gels, from calcining in air, was 420°C, while 200° to 250°C in the presence of water and organic solvents such as methanol and ethanol. The sintering behaviors of CeO2 –ZrO2 powders were sensitive to the crystallizing conditions, since hard agglomerates formed when the precipitated gels were crystallized by normal calcination in air, whereas soft agglomerates formed when they were crystallized in water or organic solvents. CeO2 –ZrO2 powders crystallized in methanol and water at 250°C were sintered to full theoretical density at 1150° and 1400°C, respectively, whereas that crystallized by calcination in air at 450°C was sintered to only 95.2% of theoretical density, even at 1500°C. 相似文献
10.
This paper presents a novel pattern matching technique that is robust to illumination changes and the occlusion problem. The technique is based on the matching of gradient orientations in place of traditional image features such as intensities or gradients. Gradient orientations depend on the texture in an image. They are known to be insensitive to changes of image intensities that are often caused by time-varying illuminations or the auto-gain control (AGC) function of the camera. Moreover,the proposed method employs a voting strategy in the process of matching gradient orientations. The method works remarkably well even when a large part of the pattern is occluded with a foreign object. Consequently, the proposed method is robust to both irregular lighting conditions and the occlusion problem. 相似文献