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1.
Alaa?S.?Abd-El-AzizEmail author Nelson?M.?Pereira Waleed?Boraie Erin?K.?Todd Tarek?H.?Afifi Wes?R.?Budakowski Ken?J.?Friesen 《Journal of Inorganic and Organometallic Polymers and Materials》2005,15(4):497-509
The synthesis of the title complexes was achieved via the reaction of
-p-dichlorobenzene-
-cyclopentadienyliron cations with 4,4′-bis(4-hydroxyphenyl)valeric acid to produce the diiron complexes which were then reacted with a number of arylazo dyes to give cationic bis(cyclopentadienyliron)arene complexes containing the arylazo dyes. These iron-containing monomers were subsequently polymerized via nucleophilic aromatic substitution using 1,8-octanedithiol, 4,4′-thiobisbenzenethiol, or bisphenol A to produce the desired coloured cationic organoiron polymers. The weight – average molecular weights were estimated to range from 11,800 to 31,600. UV–vis studies conducted in dimethylformamide (DMF) showed that the metallated polymers exhibited
of 412–491 nm. Addition of HCl to the polymer solution caused a bathochromic shift into the range of 515–530 nm. Thermogravimetric analysis (TGA) revealed that the iron moieties were cleaved between 205 and 248 °C while the polyether/thioether backbone degraded between 380 and 613 °C. Differential scanning calorimetry (DSC) showed that the polymers exhibited glass transition temperatures (Tg) ranging from 106 to 184°C.This paper is dedicated to Professor Richard J. Puddephatt in recognition of his outstanding contribution to the field of metal-containing polymers. 相似文献
2.
A combination of soft lithography and lift-off processing is presented for the fabrication of sulfonated polyaniline (SPAN) microstructures. A soft lithography based micromolding process was used to pattern sacrificial layers using a thermoplastic polymer. SPAN was then polymerized in situ to coat the patterned substrate. The sacrificial layer was removed by lift-off in an organic solvent, leaving the patterned SPAN on the substrate. This process was performed on several rigid and flexible substrates including glass, silicon, and polyimide. The film thickness and roughness were measured as a function of reaction time using atomic force microscopy. Patterns were also imaged using scanning electron microscopy. This process provides a cost effective and versatile method of patterning SPAN and has potential applications in a number of conducting polymer devices. 相似文献
3.
Gosink LJ Anderson JC Bethel EW Joy KI 《IEEE transactions on visualization and computer graphics》2008,14(6):1715-1722
The visualization and analysis of AMR-based simulations is integral to the process of obtaining new insight in scientific research. We present a new method for performing query-driven visualization and analysis on AMR data, with specific emphasis on time-varying AMR data. Our work introduces a new method that directly addresses the dynamic spatial and temporal properties of AMR grids that challenge many existing visualization techniques. Further, we present the first implementation of query-driven visualization on the GPU that uses a GPU-based indexing structure to both answer queries and efficiently utilize GPU memory. We apply our method to two different science domains to demonstrate its broad applicability. 相似文献
4.
C. J. Thompson D. Hansford D. L. Munday S. Higgins C. Rostron G.A. Hutcheon 《Drug development and industrial pharmacy》2013,39(8):877-884
Ibuprofen was conjugated at different levels to a novel polyester, poly(glycerol-adipate-co-ω-pentadecalactone) (PGA-co-PL), via an ester linkage to form a prodrug. The conjugates were characterized by differential scanning calorimetry (DSC), nuclear magnetic resonance (NMR), infrared (IR), gel permeation chromatography (GPC), ultraviolet (UV), and high-performance liquid chromatography (HPLC). The conjugates had a molecular weight between 18 and 24 kDa, and there was a suppression of the free hydroxyl groups within the conjugated polymer. DSC scans showed a lowering of the melting point (Tm) when compared with the polyester alone and a difference in the number and area of Tm peaks. Drug release studies showed an initial burst release (13–18%) followed thereafter by very slow release (maximum 35% after 18 days). Continuous work may produce ester-linked conjugates that are sufficiently labile to allow for complete release of ibuprofen over the time period studied. 相似文献
5.
Athanasios Kotsiopoulos Geoffrey S. Hansford Randhir Rawatlal 《American Institute of Chemical Engineers》2012,58(8):2428-2440
A dynamic analysis of chalcopyrite bioleaching was performed in continuous flow systems. In contrast to a previous batch analysis1 in which the influence of particle surface area on reaction rate was not accounted for, the unsteady‐state change in particle surface area was integrated into the dynamic analysis by application of the modified PBM.2 The current study extends the analysis to include the influence of convective flow on the system. It is demonstrated that the analysis can be used to determine feasible control strategies for operating near the steady‐state maximum rate that is stable. Two strategies were evaluated for the purpose of increasing the leaching rates, showing that an increased rate of 56% is feasible. Analysis on experimental data showed that increased rates can be achieved by controlling the biomass concentration and ferric:ferrous ion ratio at an optimum by increasing the solids loading [m/v] in the reactor. © 2011 American Institute of Chemical Engineers AIChE J, 58: 2428–2440, 2012 相似文献
6.
Daniela M. Ushizima Hrishikesh A. Bale E. Wes Bethel Peter Ercius Brett A. Helms Harinarayan Krishnan Lea T. Grinberg Maciej Haranczyk Alastair A. Macdowell Katarzyna Odziomek Dilworth Y. Parkinson Talita Perciano Robert O. Ritchie Chao Yang 《JOM Journal of the Minerals, Metals and Materials Society》2016,68(11):2963-2972
7.
Wes Hansford 《电子产品世界》2007,(9):144-146
引言 一部分集成电路的NRE(一次性工程费用)被控制的越来越紧,但是另一部分却并非如此,典型的掩模组的价格急剧上升. 相似文献
8.
Chander Shekhar Sharma Amanda Ates Poulson Joseph Kamlesh A. Soni M. Wes Schilling Aaron Kiess 《International Journal of Food Science & Technology》2013,48(7):1410-1415
The efficacy of lauric arginate (LAE) on Salmonella survivability in ground chicken containing 9.8% fat was determined under refrigerated storage. The effect of LAE treatments on total aerobes, pH and objective colour were also assessed in ground chicken. LAE was highly effective against Salmonella in 0.1% peptone with no detectable survivors following treatment with 200 ppm and 400 ppm of LAE. No difference existed (P > 0.05) in the growth of Salmonella and total aerobes after treatment with 200 and 400 ppm of LAE in ground chicken inoculated with a four strain mixture of Salmonella. At these concentrations, LAE did not exhibit any treatment effect on the pH and colour of ground chicken (P > 0.05). In conclusion, although LAE possesses strong inhibitory (P < 0.05) effect against Salmonella in suspension in 0.1% peptone water, no inhibitory (P > 0.05) effect on growth of Salmonella was observed in ground chicken at the currently approved levels of 200 ppm of LAE. 相似文献
9.
10.
In this work, the fluid flow and mass transfer due to the presence of an electric field in a rectangular channel is examined. We consider a mixture of water or another neutral solvent and a salt compound, such as sodium chloride, for which the ionic species are entirely dissociated. Results are produced for the case in which the channel height is much greater than the electric double layer (EDL) (microchannel) and for the case in which the channel height is of the order of the width of the EDL (nanochannel). Both symmetric and nonsymmetric velocity, potential, and mole fraction distributions are considered, unlike previous work on this problem. At small electrolyte concentrations, the Debeye-Huckel picture of the electric double layer is recovered; at larger concentrations, the Gouy-Chapman picture of the electric double emerges naturally. The numerical results presented here agree with analytical solutions of a singular perturbation analysis, which is valid as the channel height increases. In the symmetric case for the electroosmotic flow so induced, the velocity field and the potential are similar. In the asymmetric case corresponding to different wall potentials, the velocity and potential can be vastly different. The fluid is assumed to behave as a continuum, and the volume flow rate is observed to vary linearly with channel height for electrically driven flow, in contrast to pressure-driven flow, which varies as height cubed. This means that very large pressure drops are required to drive flows in small channels. However, useful volume flow rates may be obtained at a very low driving voltage. 相似文献