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1.
研究了具有新型结构的双膦胺镍配合物N,N-双(二苯膦基)-对甲氧基苯胺二氯化镍-甲基铝氧烷(PNP-N i-MAO)催化体系对苯乙烯聚合的催化性能,考察了聚合温度、n(A l)∶n(PNP-N i)、PNP-N i的浓度和苯乙烯的浓度对催化活性、苯乙烯转化率、聚苯乙烯相对分子质量及其分布的影响,并用核磁共振和凝胶色谱对聚苯乙烯的结构进行了表征。实验结果表明,在聚合温度25℃、聚合时间1h、n(A l)∶n(PNP-N i)=300、c(苯乙烯)=2.3m ol/L、c(PNP-N i)=0.4mm ol/L、甲苯为溶剂的适宜条件下,苯乙烯的转化率可达95%以上,催化活性达到5×105g/(m ol.h)左右。核磁共振和凝胶色谱表征结果显示,所得聚苯乙烯为无规结构,重均相对分子质量约为1×104,相对分子质量分布Mw/Mn约为2。  相似文献   
2.
西北口面板堆石坝蓄水7年变形分析   总被引:9,自引:0,他引:9  
西北口坝是我国第一座混凝土面板堆石坝,是原水利电力部试验坝,是国家“七五”科技攻关项目.1991年下闸试蓄水运行至今已有7年.7年的监测成果表明,西北口混凝土面板堆石坝蓄水运行后仍有较大的变形发生,笔者通过资料分析初步认为是徐变引起的.  相似文献   
3.
This paper sketches the contours of the evolving international/monetary system and examines the various roles of the intemediation mechanisms. Then it examines the extent to which the financial system is independent from the “real economy” and the various ways in which it impacts it. The paper discusses some views in good currency on the dynamics of the technology-trade-finance nexus and shows how the financial system influences organization, location and technology choices in meso-innovation systems. The final section of the paper looks at the policy implications that might be derived from the analysis and suggests some directions for the future research.  相似文献   
4.
本文给出了一种椭圆弧长的作图求解方法,即由作图求得椭圆弧长的近似值。通过对100个椭圆弧长的求解结果表明,由此方法求得的椭圆弧长的误差甚小,从而在相当高的精度范围内,提供了一种工程中适用并且简单易行的求解椭圆弧长的方法。  相似文献   
5.
The vortex-induced vibration of a flexible circular cylinder is investigated at a constant Reynolds number of 1 000.The finite-volume method on moving meshes is applied for the fluid flow, and the Euler-Bernoulli beam theory is used to model the dynamic response of a flexible cylinder.The relationship between the reduced velocity and the amplitude response agrees well with the experimental results.Moreover, five different vibrating modes appear in the simulation.From the comparisons of their vortex structures, the strength of the wake flow is related to the exciting vibrating mode and different vortex patterns arise for different vibrating modes.Only 2P pattern appears in the first vibrating mode while 2S-2P patterns occur in the other vibrating modes if monitoring at different sections along the length of the cylinder.The vibration of the flexible cylinder can also greatly alter the three-dimensionality in the wake, which needs further studies in our future work, especially in the transition region for the Reynolds number from 170 to 300.  相似文献   
6.
In this paper, a unified approach to the design of a nonlinear excitation controller/power system stabilizer for a synchronous generator/infinite bus power system is presented. The approach is based on a form of state feedback linearization, known as input–output feedback linearization, which provides an exact semi-global state transformation that is valid for a large class of operating points of the power system. With this transformation, the terminal voltage becomes a linear function of the control input. The excitation controller/power system stabilizer is then synthesized by using linear controller design techniques. The controller is proven to provide small signal stability and to provide local asymptotic tracking of admissible constant reference signals for a large class of operating points. A procedure is given to tune the controller gains to provide significant damping of the power angle oscillations.  相似文献   
7.
Transmission Control Protocol (TCP) provides mechanisms for reliable data communications. Although it works well in wired networks, it fails to offer satisfactory performance in lossy and wireless environments. And in the multi-hop wireless infrastructure, packet delivery suffers high cumulative loss rate if traveling over multiple wireless hops. The Selective acknowledgment (SACK) is one header option that might be used to combat segment corruptions in air channels. In this paper, an alternative set of flow control mechanisms is proposed to handle high packet loss rate in a wireless medium. Using a measurement-based mechanism, sustainable segment delivery is achievable through a novel size-reduction method. Multiple segment retransmission mechanisms are introduced to reduce successive timeout events. One single byte loss is sufficient to waste all other bytes in a file received at a destination. That is, a good TCP flow control mechanism should provide a high successful file transmission completion rate, and this is set as our design goal. Through thorough simulations, our proposed multi-segment retransmission designs perform with higher successful file transfer rate and fewer timeout events than NewReno and SACK under a wide range of packet loss probabilities.  相似文献   
8.
User innovation is the key to the development and vitality of technology. As Huatong Sun wrote, “expanding the scope of localization practices and linking user localization efforts” to design cycles—including pedagogical design—will help bridge the gap between what teachers/designers create and what skills users/students need and want. This article theorizes the role of modern composition students and teachers as co-constructors of productive spaces for learning critical inquiry based on students’ statuses as digital natives. It focuses on a class of first-year composition students who reshaped an assignment to fit their own needs within the physical classroom and also enacted a shift to a virtual classroom. While doing so, they provided ways for each class member to individualize space within that digital environment, and they focused their project on examining the ways in which social networking forums colonize their daily lives. This article argues that by letting student innovation drive pedagogical practice—just as social media creators let user innovation drive the digital structures they produce—composition teachers can be assured of having a text for critique that blurs the lines between “private” student underlife and “public” classroom practice and legitimizes the creation of student-produced learning spaces. Using critical and cyberfeminist theories as lenses, this article draws conclusions about the future of computer usage in composition pedagogy based on students’ abilities to re-appropriate physical and digital classroom space.  相似文献   
9.
This paper considers the distributed model predictive control (DMPC) of systems with interacting subsystems having decoupled dynamics and constraints but coupled costs. An easily-verifiable constraint is introduced to ensure asymptotic stability of the overall system in the absence of disturbance. The constraint introduced has a parameter which allows for the performance of the DMPC system to approach that controlled by a centralized model predictive controller. When the subsystems are linear and additive disturbance is present, the added constraint ensures the state of each subsystem converges to its respective minimal disturbance invariant set. The approach is demonstrated via several numerical examples.  相似文献   
10.
Design reuse oriented partial retrieval of CAD models   总被引:1,自引:0,他引:1  
As a huge number of 3D CAD models is generated each year, retrieval of 3D CAD models is becoming more and more important for achieving design reuse. However, the existing methods for partial retrieval of 3D CAD models are very few and far from the requirements of design reuse. In this paper, we present an approach to partial retrieval of 3D CAD models for design reuse. The criteria for determining whether a subpart of 3D CAD models is reusable for design is defined first. Based on the criteria defined, all the design reusable subparts involved in the 3D CAD models in the library are automatically extracted and stored in the library as reference models. Moreover, each design reusable subpart in the library is represented by all its local matching regions in a hierarchical way so as to support multi-mode partial retrieval. In our approach, three partial retrieval modes including normal retrieval, exact retrieval and relaxed retrieval are defined to meet various partial retrieval requirements of design reuse such as the incomplete and vague queries during the early design stage. And the multi-mode partial retrieval is achieved by performing multi-mode matching and similarity assessment between the query and the design reusable subparts in the library indexed by bitmap. Experimental results are presented to demonstrate the effectiveness of the approach.  相似文献   
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