Creep and Stress Rupture Behavior of an Advanced Silicon Nitride: Part I, Experimental Observations

Cylindrical buttuohead specimens of an advanced silicon nitride were tested in uniaxial tension at temperatures between 1422 and 1673 K. In the range 1477 to 1673 K, creep deformation was reliably measured using high-temperature contact probe extensometry. Extensive scanning and transmission electron microscopy has revealed the formation of lenticular cavities at two-grain junctions at all temperatures (1422–1673 K) and extensive triple-junction cavitation occurring at the higher temperatures (1644–1673 K). Cavitation is believed to be part of the net creep process. The stress rupture data show stratification of the Monkman–Grant lines with respect to temperature. Failure strain increased with increase in rupture time or temperature, or decrease in stress. Fractography showed that final failure occurred by subcritical crack growth in all specimens.     

A case for information theory-based modelling of human multitasking performance

Technological advances have led to increased prevalence of human multitasking. Traditionally, multitasking performance is measured for each individual task, utilising multiple performance metrics. Recently, the human operator informatic model (HOIM) has been developed as a quantitative model of human–machine interaction capable of measuring multitasking performance with a single metric. In this study, we investigated the performance effects of both a different number of tasks and five different task combinations while maintaining a constant level of overall difficulty. Results indicate that, at a constant difficulty level, neither number of tasks nor task combination significantly affects multitasking performance, indicating the reliability of input baud rate as a measure of system complexity. No task interaction effects were found among the different tasks. This study demonstrates the application of information theory for modelling of human multitasking performance and makes a case for the use of the HOIM in future studies of human information processing.     

Nanocrystallization and Phase Transformation in Monodispersed Ultrafine Zirconia Particles from Various Homogeneous Precipitation Methods

Monodispersed ultrafine (nano- to micrometer) zirconia precursor powders were synthesized by three different physicochemical methods: (I) forced hydrolysis, (II) homogeneous precipitation in inorganic salt solutions, and (III) hydrolysis/condensation of alkoxide. The forced hydrolysis method produced monoclinic nanocrystalline particles (cube shaped) of nanometer scale, which depended largely on the initial salt concentration. Methods II and III, both involving the use of alcohol as a solvent, exhibited a faster particle formation rate and generated amorphous ultrafine (submicrometer) monodispersed microspheres, indicating that the presence of alcohol may have stimulated particle nucleation due to its low dielectric property (and, thus, the low solubility of nucleus species in mixed water-alcohol solutions). Nucleation and growth of the particles in solutions are discussed based on the measurements obtained by small-angle X-ray scattering (SAXS) and dynamic light scattering (DLS). High-temperature X-ray diffraction (HTXRD) and TGA/DTA studies elucidated the differences in phase transformation for different types of powders. The most interesting finding was the nonconventional monoclinic nanocrystal nucleation and growth that occurred prior to transformation to the tetragonal phase (at 1200°C) during the heat treatment of the nanocrystalline powders produced by the forced hydrolysis.     

Integrated Saltwater Desalination and Energy Storage through a pH Neutral Aqueous Organic Redox Flow Battery

Here, a pH neutral aqueous organic redox flow battery (AORFB) consisting of three electrolytes channels (i.e., an anolyte channel, a catholyte channel, and a central salt water channel) to achieve integrated energy storage and desalination is reported. Employing a low cost, chemically stable methyl viologen (MV) anolyte, and sodium ferrocyanide catholyte, this desalination AORFB is capable of desalinating simulated seawater (0.56 m NaCl) down to 0.023 m salt concentration at an energy cost of 2.4 W h L^?1 of fresh water—competitive with current reverse osmosis technologies. Simultaneously, the cell delivers stored energy at 79.7% efficiency with a cell voltage of 0.85 V. Furthermore, the cell is also capable of higher current operation up to 15 mA cm^?2, providing 4.55 mL of fresh water per hour. Combining energy storage and water desalination into such a bifunctional device offers the opportunity to address two growing global issues from one hardware installation.     

无人机飞行数据的可视化技术

在分析无人机领域飞行数据特征的基础上,设计了与数据相对应的可视化图形元,完成了基于ＰＣ机低成本硬件系统的飞行数据的可视化。在软件设计过程中,使用前后台编程技术,解决了地图航迹视图显示调图过程中出现的冻结问题;采用色彩优化算法,实现了彩色地图的伪彩色逼真显示。该系统经过实际飞行的验证,成为小型无人机公共地面控制系统的重要组成部分     

Microstructure and Crystallography of Titanium Nitride Whiskers Grown by a Vapor–Liquid–Solid Process

Titanium nitride whiskers having diameters of 0.5 to 1.5 μm and aspect ratios in the range of 20 to 50 have been produced by a new commercially scalable vapor–liquid–solid process. Electron microscopy studies have shown that most of the whiskers can be classified into two types based upon structure and morphology. The whiskers of one type are single crystals and have a growth direction of (100). Whiskers of the second type are comprised of two crystals having a common (110) growth direction. Both types have smooth surfaces and relatively few internal defects. Additionally, a small percentage of whiskers have considerable internal structure related to significant magnesium impurities.     

Neutron Diffraction Measurements of the Residual Stresses in Al2O3-ZrO2 (CeO2) Ceramic Composites

High-resolution neutron powder diffraction was used to study the residual stresses in Al₂O₃-ZrO₂ (12 mol% CeO₂) ceramic composites containing 10, 20, and 40 vol% ZrO₂ (CeO₂). The diffraction data were analyzed using the Rietveld structure refinement technique. The analysis shows that for all samples, the CeO₂-stabilized tetragonal ZrO₂ particles are in tension and the Al₂O₃ matrix is in compression. For both the ZrO₂ particles and the Al₂O₃ matrix, the average lattice strains are anisotropic and increase approximately linearly with a decrease in the corresponding phase content. It is shown that these features can be qualitatively understood by taking into consideration the thermal expansion mismatch between the ZrO₂ and Al₂O₃ grains. Also, for all composite samples, the diffraction peaks are broader than the instrumental resolution, indicating that the strains in these samples are inhomogeneous. From an analysis of the refined peak shape parameters, the average root-meansquare strain, which describes the distribution of the inhomogeneous strain field, was determined. Finally, the average residual stresses were evaluated from the experimentally determined average lattice strains and compared with recent results of X-ray measurements on similar composites.     

Stress-induced structural changes in La-doped BiFeO3–PbTiO3 high-temperature piezoceramics

High-temperature piezoelectric polycrystalline ceramics of the system (1 ? x)(Bi_1?yLa_y)FeO₃-xPbTiO₃ (BF–PT), which are mixed phase in their consolidated state, have been investigated by in situ neutron diffraction during the application of uniaxial compressive stress. It is suggested that the achievable strain in BF–PT is largely generated by straining of the rhombohedral phase. The results of the neutron diffraction measurements are compared and discussed with respect to the measured macroscopic ferroelastic constitutive behavior for various compositions of BF–PT.     

丰城赣江大桥水上钻孔定位测量

丰城赣江大桥工程地质勘察水上钻孔定位施工放样是采用方向法前方交会.用电磁波测距三角高程测量来测定其孔口标高.从误差传播定律的角度,论证了该施测方案的正确性,同时也论述了要达到高精度放样的最佳图形是布设成两底角为锐角的等腰三角形.